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Mid-Michigan
3340 Ranger Road
Lansing, MI 48906
Ph. 517-321-3331
Fax 517-323-7228 pme@pmenv.com Metro Detroit
22655 S. Chrysler Drive
Hazel Park, MI 48030
Ph. 248-336-9988
Fax 248-336-9989 pmehazelpark@pmenv.com West Michigan
1441 Arboretum Dr. SE,
Suite 200
Grand Rapids, MI 49546
Ph. 616-285-8857
Fax 616-285-8026 pmegr@pmenv.com ISO 9001 REGISTERED

CATEGORY-N BASELINE ENVIRONMENTAL
ASSESSMENT OF THE FORMER ACTIVE HOMES
MANUFACTURING BUILDING LOCATED AT 7876
VAN DYKE, MARLETTE, LAPEER COUNTY,
MICHIGAN
June 2, 2006

May 19, 2006

District Supervisor
Remediation and Redevelopment Division
Lansing District Office
Constitutional Hall
North Tower, 4th Floor
525 W. Allegan Street
Lansing, Michigan 48909

RE:

Category-N Baseline Environmental Assessment of Former Active
Homes Manufacturing Building
Located at 7876 Van Dyke, Marlette, Lapeer County, Michigan
PM Environmental, Inc., Project No. 22-692A

Dear District Supervisor:
Enclosed is one copy of the above-referenced document prepared in accordance with the March 11,
1999 “Instructions for Preparing and Disclosing Baseline Environmental Assessments by PM
Environmental, Inc., on behalf of Outlook Properties LLC. An affidavit signed by Mr. Bob Gilling, for a Disclosure Baseline Environmental Assessment has been included. If you have any questions regarding the information in this report, please contact our office at (248) 336-9988.
Sincerely,
PM Environmental, Inc.

Rachael Koch
Project Consultant

Steve Price
Vice President of Due Diligence

Enclosure

22655 S. Chrysler Dr.
Hazel Park, MI 48030
Office: 248.336.9988
Fax: 248.336.9989

3340 Ranger Road
Lansing, MI 48906
Office: 517.485.3333
Fax: 517.323.7228.

5380 Cascade Suite 200
Grand Rapids, MI 49546
Office: 616.285.8857
Fax: 616.285.8026

PM ENVIRONMENTAL, INC. PROJECT NO. 22-692A
BASELINE ENVIRONMENTAL ASSESSMENT
CATEGORY N BASELINE ENVIRONMENTAL
ASSESSMENT CONDUCTED PURSUANT TO
SECTION 20126(1)(c) OF 1994 PA 451, PART 201, AS
AMENDED, AND THE RULES PROMULGATED
THEREUNDER
Location:
Former Active Homes Manufacturing Building
7876 Van Dyke
Marlette, Lapeer County, Michigan
Prepared For:
Mr. Bob Gilling
1090 Doris Road
Auburn Hills, Michigan

CATEGORY N BASELINE ENVIRONMENTAL
ASSESSMENT CONDUCTED PURSUANT TO SECTION
20126(1)(c) OF 1994 PA 451, PART 201, AS AMENDED,
AND THE RULES PROMULGATED THEREUNDER
FOR
THE
FORMER
ACTIVE
HOMES
MANUFACTURING BUILDING LOCATED 7876 VAN
DYKE, MARLETTE, LAPEER COUNTY, MICHIGAN
48444

May 19, 2006
Prepared By:
PM Environmental, Inc.
TABLE OF CONTENTS
22655 S. Chrysler Dr.
Hazel Park, MI 48030
Office: 248.336.9988
Fax: 248.336.9989

3340 Ranger Road
Lansing, MI 48906
Office: 517.485.3333
Fax: 517.323.7228.

5380 Cascade Suite 200
Grand Rapids, MI 49546
Office: 616.285.8857
Fax: 616.285.8026

Category-N Baseline Environmental Assessment of the Former Active Homes Manufacturing Building
Located at 7876 Van Dyke, Marlette, Lapeer County, Michigan
PM Environmental, Inc., Project No. 22-692A; May 19, 2006

Baseline Environmental Assessment
1.0
2.0
3.0

4.0

5.0
6.0
7.0
8.0
9.0

Identification of Author and Date BEA was Conducted and Date BEA was Completed .. 1
Introduction......................................................................................................................... 1
Property Description & Intended Hazardous Substance Use ............................................. 2
3.1
Property Description ............................................................................................... 2
3.2
Intended Hazardous Substance Use ........................................................................ 3
Known Contamination ........................................................................................................ 3
4.1
Soil and Groundwater Sampling and QA\QC Procedures...................................... 3
4.1.1 Soil Boring Advancement........................................................................... 5
4.1.2 Quality Assurance and Quality Control...................................................... 6
4.2
Geology and Hydrogeology.................................................................................... 6
4.3
Chemical Analysis .................................................................................................. 7
4.4
Analytical Results ................................................................................................... 7
4.5
Abandoned Containers............................................................................................ 8
Likelihood of Other Contamination.................................................................................... 8
5.1
Potential Additional Impact on the Subject Site Property ...................................... 8
Alternative Approaches ...................................................................................................... 8
Conclusions......................................................................................................................... 8
References........................................................................................................................... 9
Attachments ...................................................................................................................... 10

ii

Category-N Baseline Environmental Assessment of the Former Active Homes Manufacturing Building
Located at 7876 Van Dyke, Marlette, Lapeer County, Michigan
PM Environmental, Inc., Project No. 22-692A; May 19, 2006

LIST OF TABLES
Table 1: Summary of Cleanup Criteria Comparison for Soils – Polynuclear Aromatic
Compounds (PNAs)
Table 2: Summary of Cleanup Criteria Comparison for Soils – Polychlorinated Biphenyls
(PCBs), Cadmium, Chromium and Lead
Table 3: Summary of Cleanup Criteria Comparison for Soils –Volatile Organic Compounds
(VOCs)
LIST OF FIGURES
Figure 1:
Figure 2:
Figure 3:

Site Vicinity Map
Subject Site and Adjoining Properties
Soil Boring Locations with Analytical Results

LIST OF APPENDICES
Appendix A:
Appendix B:
Appendix C:
Appendix D:
Appendix E:
Appendix F:

Resumes
Previous Site Assessment Reports
Site Photographs
Laboratory Reports
Boring Logs
GPR Survey

iii

Category-N Baseline Environmental Assessment of the Former Active Homes Manufacturing Building
Located at 7876 Van Dyke, Marlette, Lapeer County, Michigan
PM Environmental, Inc., Project No. 22-692A; May 19, 2006

1.0

Identification of Author and Date BEA was Conducted and Date BEA was Completed

This Category N Baseline Environmental Assessment (BEA) was prepared by Ms. Rachael Koch,
Project Consultant, Mr. Douglas McVey, Technical Operations Manager, and Mr. Steve Price, Vice
President of Due Diligence, PM Environmental, Inc., 22655 S. Chrysler Drive, Hazel Park,
Michigan. The BEA was conducted on May 15, 2006, and was completed on May 19, 2006.
Resumes for the environmental professionals involved in this BEA are included in Appendix A.
2.0

Introduction

PM Environmental, Inc., (PME) has been retained by the potential purchaser, Bob Gilling, Outlook
Properties, LLC, Auburn Hills, Michigan, to provide environmental consulting services related to the development of a Category N BEA for the Former Active Homes Manufacturing Building, located at 7876 Van Dyke, Marlette, Lapeer County, Michigan. The subject site is further described as located in Township 10 North (T.10N), Range 12 East (R.12E), Section 25, Marlette, Lapeer
County, Michigan. A site vicinity map is presented in Figure 1. A scaled site map depicting the subject site, adjoining properties and soil/groundwater sample locations is presented in Figure 2.
A Phase I Environmental Site Assessment (ESA) was completed for the subject site by PME in June
2005. The following on-site recognized environmental conditions (RECs) were identified in the
2005 Phase I ESA:


The subject site building has operated as a mobile home manufacturing facility. PME observed a staging area of the 55-gallon drums and ASTs, containing waste oil and unlabeled substances. This staging area was located within the northeastern portion of the manufacturing building. PME observed staining around the 55-gallon drums and AST storage and within expansion joints. The waste management practices of the historical occupants are unknown.



The integrity of the floor drains in the buildings is unknown. The potential failure of the drainage system (i.e., cracks, leaks) to have occurred over time, and the current and historical usage of hazardous substances has been identified as a REC.



PME was unable to determine the natural gas availability for the subject site area, the possibility exists that an alternative-heating source was utilized. PME has not identified a previous fuel source for heating through reasonably ascertainable standard and other historic sources consulted. The original date of development at the site was approximately 1950; therefore, the subject site may have utilized an AST or UST for heating oil storage, which represents a REC. The possibility exists for an orphan fuel oil UST to be present at the subject site.



Based on the usage of the building as a manufacturing facility, the use and storage of petroleum based substances and the unknown waste management practices represent a
PM Environmental, Inc.
Page 1

Category-N Baseline Environmental Assessment of the Former Active Homes Manufacturing Building
Located at 7876 Van Dyke, Marlette, Lapeer County, Michigan
PM Environmental, Inc., Project No. 22-692A; May 19, 2006

concern in regards to the septic system. The potential exists for the interior floor drains to lead to the septic system. PME was unable to identify the location of the septic field.
PME did not identify any off-site RECs.
Site assessment activities were completed by PME on the subject site property on April 27, 2006. A total of ten (10) soil borings (SB-1 through SB-10) were advanced to assess the RECs identified in the Phase I ESA and to assess whether the subject site should be classified as a facility as specified in Section 20120a(1)(a) or (17) in Part 201 of the Natural Resources and Environmental Protection
Act (NREPA), P.A. 451 of 1994 (Part 201). Soil boring locations were based on RECs that were documented in the June 2005 Phase I ESA (Appendix B).
Analytical results from the sampling completed by PME indicate soil contaminant concentrations of chromium that exceed the current Part 201 Residential/Commercial Groundwater Surface Water
Interface (GSI) Cleanup Criteria. Based upon these analytical results, the property identified as
Former Active Homes Manufacturing Building, Located at 7876 Van Dyke, Marlette, Lapeer
County, Michigan, is considered a facility.
The purpose of this BEA is to describe the condition of the subject site at the time of transfer and establish a basis to distinguish existing contamination from any new release in accordance with
Michigan Administrative Code R 299 5901-5919.
The intended use of the subject site by the purchaser is to remain unoccupied until a future use is determined. Therefore, a Category N BEA is the appropriate BEA. The future owner will be prohibited to use, store, or manage hazardous substances in quantities that exceed those typically used for residential or office purposes.
3.0

Property Description & Intended Hazardous Substance Use
3.1

Property Description

The subject site property is approximately 34.12 acres of land, containing the main manufacturing building, located on the western portion of the subject site. In addition, an office building is located west of the main building. The main building was originally constructed in approximately 1950, with several additions built throughout the years, and contains a total of approximately 378,420square feet of floor space. The current office building was constructed in 1996 and contains approximately 7,656-square feet of floor space, which is divided into offices and bathrooms.
Unpaved parking areas are located to the north and west of the subject site buildings. Overgrown vegetation is located east and south of the subject site building. There is a metal canopy located east of the main building. In addition, there is a water tower located east of the building. The remainder of the subject site is vacant/undeveloped land.

PM Environmental, Inc.
Page 2

Category-N Baseline Environmental Assessment of the Former Active Homes Manufacturing Building
Located at 7876 Van Dyke, Marlette, Lapeer County, Michigan
PM Environmental, Inc., Project No. 22-692A; May 19, 2006

Photographs of the subject site and the adjoining properties were taken on May 19, 2005, by Ms.
Rachael Koch, Project Consultant, during a site inspection (Appendix C).
The subject site building is connected to natural gas, which is supplied by SEMCo. PME was unable to determine the natural gas availability for the subject site area, and the possibility exists that an alternative-heating source was utilized. The original date of development at the site was approximately 1950; therefore, the subject site may have utilized a UST for heating oil storage.
PME interviewed a representative of Burnside Township. The representative of this department indicated that the subject site is not currently connected to municipal water service. PME was unable to locate a water well at the subject site. Burnside Township does not have records pertaining to water well installation. The Township representative indicated that the subject site is not currently connected to municipal sewer service. PME was unable to locate the septic field at the subject site. Burnside Township does not have records pertaining to the septic tank installation. In addition, Mr. Lupo, Burnside Township Assessor informed PME the subject site had a septic backup and a portion of the building was closed off, and temporary restrooms were installed. The potential exists for the interior floor drains to lead to the septic system. The surrounding adjoining properties are occupied by agricultural land.
The subject site consists of one (1) parcel, identification number 4405-128-003-00 and 4405-128006-00, 7938 (7876) Van Dyke, Marlette, Burnside Township, Michigan.
The subject site is zoned Light Industrial according to the Burnside Township.
3.2

Intended Hazardous Substance Use

The intended use of the subject site by the purchaser is to remain unoccupied until a future use is determined. No significant hazardous substance use will occur on the subject site, which will be the basis for distinguishing the existing contamination from a new release. Therefore, a Category N
BEA is appropriate.
Based on this information, there will be no significant hazardous substance use at the subject site and this stipulated condition is the basis for being able to distinguish existing contamination from a new release. Therefore, a Category-N is the appropriate BEA.
4.0

Known Contamination
4.1

Soil and Groundwater Sampling and QA\QC Procedures

On April 27, 2006, PME initiated field activities that consisted of advancing ten (10) soil borings
(SB-1 through SB-10), to investigate potential contamination from the RECs associated with historic on site operations. Sampling was conducted using hydraulic probe or hand auger methods to a maximum depth of 15.0 feet below ground surface (bgs). Soil samples were collected for chemical analysis based on visual staining, olfactory evidence, and/or elevated photoionization detector (PID)
PM Environmental, Inc.
Page 3

Category-N Baseline Environmental Assessment of the Former Active Homes Manufacturing Building
Located at 7876 Van Dyke, Marlette, Lapeer County, Michigan
PM Environmental, Inc., Project No. 22-692A; May 19, 2006

readings. Analytical results are summarized in Tables 1 through 3, along with Michigan Department of Environmental Quality (MDEQ) Part 201 cleanup criteria. Sample locations with summary results are presented in Figure 3. Complete laboratory reports are presented in Appendix D. The selection of soil boring locations was based on the RECs as follows:


Soil boring SB-1 was advanced in the north portion of the main building to assess the historical waste management practices. This boring was advanced to a depth of 15.0 feet bgs. One (1) soil sample was collected at 1.0-2.0 feet bgs. The soil sample collected was submitted for laboratory analysis of volatile organic compounds (VOCs), polynuclear aromatic compounds (PNAs), polychlorinated biphenyls (PCBs), cadmium, chromium and lead. •

Soil boring SB-2 was advanced in the north-central portion of the main building to assess the 55-gallon drum and AST storage area. This boring was advanced to a depth of 15.0 feet bgs. One (1) soil sample soil sample was collected at 2.0-3.0 feet bgs. The soil sample collected was submitted for laboratory analysis of VOC, PNAs, PCBs, cadmium, chromium and lead.



Soil boring SB-3 was advanced in the north-central portion of the main building to assess the 55-gallon drum and AST storage area. This boring was advanced to a depth of 15.0 feet bgs. One (1) soil sample was collected at 2.0-3.0 feet bgs. The soil sample collected was submitted for laboratory analysis of VOC, PNAs, PCBs, cadmium, chromium and lead.



Soil boring SB-4 was advanced in the north-central portion of the main building to assess the 55-gallon drum and AST storage area. This boring was advanced to a depth of 15.0 feet bgs. One (1) soil sample was collected at 2.0-3.0 feet bgs. The soil sample collected was submitted for laboratory analysis of VOC, PNAs, PCBs, cadmium, chromium and lead.



Soil boring SB-5 was advanced in the north-central portion of the main building to assess the historical waste management practices and surrounding floor drains. In addition, this boring also addresses the former septic field if the septic field existed north of the original building. This boring was advanced to a depth of 15.0 feet bgs. One (1) soil sample was collected at 1.0-2.0 feet bgs. The soil sample collected was submitted for laboratory analysis of VOC, PNAs, PCBs, cadmium, chromium and lead.



Soil boring SB-6 was advanced in the central portion of the main building to assess the historical waste management practices and surrounding floor drains. In addition, this boring also addresses the former septic field if the septic field existed north of the original building. This boring was advanced to a depth of 15.0 feet bgs. One (1) soil sample was collected at 1.0-2.0 feet bgs. The soil sample collected was submitted for laboratory analysis of VOC, PNAs, PCBs, cadmium, chromium and lead.



Soil boring SB-7 was advanced in the central portion of the main building to assess the
PM Environmental, Inc.
Page 4

Category-N Baseline Environmental Assessment of the Former Active Homes Manufacturing Building
Located at 7876 Van Dyke, Marlette, Lapeer County, Michigan
PM Environmental, Inc., Project No. 22-692A; May 19, 2006

historical waste management practices and surrounding floor drains. In addition, this boring also addresses the former septic field if the septic field existed north of the original building. This boring was advanced to a depth of 15.0 feet bgs. One (1) soil sample was collected at 2.0-3.0 feet bgs. The soil sample collected was submitted for laboratory analysis of VOC, PNAs, PCBs, cadmium, chromium and lead.


Soil boring SB-8 was advanced in the south-central portion of the main building to assess the historical waste management practices and surrounding floor drains. This boring was advanced to a depth of 15.0 feet bgs. One (1) soil sample was collected at 1.0-2.0 feet bgs.
The soil sample collected was submitted for laboratory analysis of VOC, PNAs, PCBs, cadmium, chromium and lead.



Soil boring SB-9 was advanced in the southeast portion of the main building to assess the historical waste management practices and surrounding floor drains. This boring was advanced to a depth of 15.0 feet bgs. One (1) soil sample was collected at 5.0-6.0 feet bgs.
The soil sample collected was submitted for laboratory analysis of VOC, PNAs, PCBs, cadmium, chromium and lead.



Soil boring SB-10 was advanced in the southwest portion of the main building to assess the historical waste management practices and surrounding floor drains. This boring was advanced to a depth of 15.0 feet bgs. One (1) soil sample was collected at 1.0-2.0 feet bgs.
The soil sample collected was submitted for laboratory analysis of VOC, PNAs, PCBs, cadmium, chromium and lead.

Additionally, PME subcontracted Worksmart Inc. to complete a ground penetrating radar survey on the property, which was completed on April 27, 2006. The GPR survey was conducted along the southern portion of the main building. No anomalies were detected that were indicative of an orphan
USTs. Therefore, it is unlikely that an orphan UST is present on the subject property. Refer to
Appendix F for a copy of the geophysical report.
4.1.1

Soil Boring Advancement

The soil borings were advanced by PME to the desired depth using hydraulic probe or hand auger methods. Soil sampling was performed for soil classification, verification of subsurface geologic conditions, and for the purpose of investigating the potential of soil or shallow groundwater contamination at the subject site. Soil samples were generally collected on a continuous basis using a 4 or 5-foot long, macro-core sampler in the case of a hydraulic probe, or a hand auger equipped with a 2.25-inch diameter, stainless-steel bucket. Soil boring logs are presented in Appendix E.
Soil collected from two-foot sample intervals was screened using a PID to determine if VOCs were present. Soil from specific depths was placed in plastic bags and allowed to volatilize. The headspace within each bag was then monitored with the PID. The PID is able to detect trace levels of organic compounds in the air space within the plastic bag. The PID utilizes a 10.2 electron volts
PM Environmental, Inc.
Page 5

Category-N Baseline Environmental Assessment of the Former Active Homes Manufacturing Building
Located at 7876 Van Dyke, Marlette, Lapeer County, Michigan
PM Environmental, Inc., Project No. 22-692A; May 19, 2006

(eV) lamp. Therefore, the PID can only detect organic vapors with an ionization potential less than or equal to 10.2 eV. PID field-screening results are documented on soil boring logs presented in
Appendix E.
Selected soil samples were submitted by PME for laboratory analysis of VOCs, PNAs, PCBs, cadmium, chromium and lead to RTI Laboratories, Inc., Livonia, Michigan. Soil samples submitted for VOC analysis were preserved in the field with methanol. Complete laboratory reports are presented in Appendix D.
4.1.2

Quality Assurance and Quality Control

During drilling operations the drilling equipment was cleaned to minimize the possibility of cross contamination. These procedures included cleaning equipment with high-pressure, steam-cleaning methods or a phosphate free solution and rinsing with distilled water after each sample collection.
All drilling and sampling equipment were cleaned in this manner, prior to field activities and between each boring location.
Soil and groundwater samples collected by PME were placed in new glass collection jars, packed on ice, and transported to RTI Laboratories, Inc., Livonia, Michigan for chemical analysis (Section 4.3), under chain of custody procedures and within applicable holding times. Soil samples analyzed for
VOCs were preserved in the field with methanol in accordance with USEPA Method 5035, modified. 4.2

Geology and Hydrogeology

A review of the 7.5 Minute, Marlette, Michigan Quadrangle Map (Figure 1), prepared by the United
States Geological Survey (USGS), dated 1963 indicates that the ground surface of the site is generally flat. The site is approximately 845 feet elevation, relative to the National Geodetic
Vertical Datum (NGVD).
According to information available from the United States Department of Agriculture, Soil Survey of Lapeer County, Michigan (published January 1972), soil types in the subject site area are generally characterized by Capac fine sandy loam, 0 to 2 percent slopes, which is characterized by sparse areas of deciduous tree forest litter from 0 to 2 inches bgs, otherwise, grayish brown to yellow sandy loam from 0 to 12 inches bgs, grayish brown to yellowish brown clay loam from 12 to 34 inches bgs, and gray loam from 34 + inches bgs.
Based on boring logs (Appendix E), the subsurface geology generally consists of approximately 5.0 feet of sand followed by a clay unit to depths ranging from 5.0 to 15.0 feet bgs, the maximum depth explored. Groundwater was not encountered within any of the ten (10) soil borings advanced by
PME.

PM Environmental, Inc.
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Category-N Baseline Environmental Assessment of the Former Active Homes Manufacturing Building
Located at 7876 Van Dyke, Marlette, Lapeer County, Michigan
PM Environmental, Inc., Project No. 22-692A; May 19, 2006

4.3

Chemical Analysis

A total of ten (10) soil samples were collected by PME on the subject site, and submitted for laboratory analysis of VOCs, PNAs, PCBs, cadmium, chromium and lead to evaluate the RECs identified in the June 2005 Phase I ESA. The compounds analyzed and USEPA methods are summarized in the following table. Laboratory MDLs are presented in the laboratory reports in
Appendix D.
Target Analytes and USEPA Methods for Soil
COMPOUNDS
VOCs

8260

PNAs

8270

PCBs

8082

Metals
4.4

SOIL

6020

Analytical Results

Tables 1 through 3 present a summary of the soil analytical results above laboratory method detection levels (MDLs) obtained by PME.
Analytical results indicate that the soil at the subject site has been impacted by toluene in SB-1 and cadmium and lead in various soil samples, at levels above the method of detection limit but below the most restrictive Part 201 Tier I Residential/Commercial/Industrial Cleanup Criteria. Chromium was detected in all borings that exceed the current Part 201 Residential/Commercial Groundwater
Surface Water Interface (GSI) Cleanup Criteria.
Analytical results for all other analytes detected in the soil samples were compared to Michigan
Department of Environmental Quality Operational Memorandum No.1 Part 201 Cleanup Criteria, issued December 10, 2004. Soil analytical results were compared to the Residential and
Commercial I Soil Drinking Water Protection (DWP), Soil Volatilization to Indoor Air Inhalation
(SVII), Groundwater Surface Water Interface Protection Criteria (GSIP), and Soil Direct Contact
(SDC) Cleanup Criteria.
A location where a hazardous substance is present “in excess of the concentrations which satisfy the requirements of subsection 20120a(1)(a) or (17)” is a “facility” pursuant to Part 201. Section
20120a(1)(a) requirements are the cleanup criteria for unrestricted residential usage. Geologic information assessed during the completion of the subsurface investigation indicates that the applicable criteria for subject site soil and groundwater are the Part 201 DWP, GSIP, SVII, SDC,
PM Environmental, Inc.
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Category-N Baseline Environmental Assessment of the Former Active Homes Manufacturing Building
Located at 7876 Van Dyke, Marlette, Lapeer County, Michigan
PM Environmental, Inc., Project No. 22-692A; May 19, 2006

DW, GSI, GVII, and GDC.
Review of analytical results summarized in Table 2 indicates contaminant concentrations of chromium, above the Part 201 Tier I GSIP Cleanup Criteria, which demonstrate that the subject property is a facility under Part 201 of P.A 451, as amended, and the rules promulgated thereunder. Copies of the analytical results are included in Appendix D.
4.5

Abandoned Containers

During the May 2005 site reconnaissance, PME observed one (1) 250-gallon and two (2) 500-gallon
ASTs within secondary containment. Additionally, PME observed several 55-gallon drums located within secondary containment. PME was unable to identify the contents of the ASTs and 55-gallon drums, with the exception of two (2) 55-gallon drums labeled “waste oil” and “engine-diesel fuel”.
The staging area of the ASTs and 55-gallon drums is located within the northern portion of the manufacturing building. The ASTs and 55-gallon drums were abandoned and need to be properly disposed of. PME observed limited staining on the concrete floor surrounding the AST and 55gallon drum storage.
5.0

Likelihood of Other Contamination
5.1

Potential Additional Impact on the Subject Site Property

The likelihood exists that other hazardous substances may be present on the property besides those identified during this BEA. Analytical results indicate that the soil at the subject site has been impacted by toluene, cadmium and lead at levels above the laboratory MDLs but below the applicable Part 201 Residential/Commercial/Industrial Cleanup Criteria. Chromium was detected in all borings that exceed the current Part 201 Residential/Commercial Groundwater Surface Water
Interface (GSI) Cleanup Criteria.
In summary, based on the historical usage of the subject site as manufacturing facility, the potential exists for other VOCs, PNAs, metals, PCBs and/or hazardous materials to be present on the subject site in areas not specifically investigated by PME.
6.0

Alternative Approaches

Not applicable.
7.0

Conclusions

Analytical results from the sampling completed by PME indicate soil contaminant concentrations of chromium that exceed the current Part 201 Residential/Commercial GSIP Cleanup Criteria. Based upon these analytical results, the site is considered a “facility” as specified in Section 20120a(1)(a) or (17) in Part 201.
PM Environmental, Inc.
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Category-N Baseline Environmental Assessment of the Former Active Homes Manufacturing Building
Located at 7876 Van Dyke, Marlette, Lapeer County, Michigan
PM Environmental, Inc., Project No. 22-692A; May 19, 2006

The intended use of the subject site by the purchaser is to remain unoccupied until a future use is determined. No significant hazardous substance use will occur on the subject site, which will be the basis for distinguishing the existing contamination from a new release. Therefore, a Category N
BEA is appropriate.
Based on this information, there will be no significant hazardous substance use at the subject site and this stipulated condition is the basis for being able to distinguish existing contamination from a new release. A Category-N BEA is sufficient to meet the needs of the proposed future property use.
8.0

References

MDEQ Operational Memorandum No. 1 “Part 201 Cleanup Criteria and Part 213 Risk-based
Screening Levels,” Revised December 10, 2004;
MDEQ Operational Memorandum No. 11 “Criteria to Eliminate the Potable Drinking Water
Pathway,” November 4, 1997;
MDEQ Operational Memorandum No. 2 “Sampling and Analysis,” October 22, 2004, Effective
February 1, 2005;
MDEQ Instructions for Preparing and Disclosing Baseline Environmental Assessments and
Section 7a Compliance Analyses, Effective March 11, 1999;
Phase I Environmental Site Assessment for Former Active Homes Manufacturing Building - 7876
Van Dyke, Marlette, Lapeer County, Michigan, prepared by PME, dated May, 2005

PM Environmental, Inc.
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Category-N Baseline Environmental Assessment of the Former Active Homes Manufacturing Building
Located at 7876 Van Dyke, Marlette, Lapeer County, Michigan
PM Environmental, Inc., Project No. 22-692A; May 19, 2006

9.0

Attachments

Copies of the following report or information that were used as the basis of this assessment are attached: Appendix A: Resumes
Appendix B: Phase I Environmental Site Assessment for Former Active Homes Manufacturing
Building - 7876 Van Dyke, Marlette, Michigan, prepared by PME, May, 2005.
Appendix C: Site Photographs
Appendix D: Laboratory Reports
Appendix E: Boring Logs
Appendix F: GPR Survey
REPORT PREPARED BY:
PM Environmental, Inc.

REPORT REVIEWED BY:
PM Environmental, Inc.

Rachael Koch
Project Consultant

Douglas E. McVey, C.P.G.
Technical Operations Manager
PM Environmental, Inc.

Steve Price
Vice President of Due Diligence

PM Environmental, Inc.
Page 10

Figures

Appendix A

PROFESSIONAL RESUME

PM ENVIRONMENTAL, INC.

Rachael Koch
PROJECT CONSULTANT
EDUCATION

EXPERIENCE

B.S. Environmental Science

Ms. Koch is a Project Consultant for PM
Environmental, Inc. Her responsibilities include site investigation activities, data collection, primary client contact, and preparation and review of reports and proposals for Phase I and Phase II
Environmental Site Assessments. Areas of expertise include:

Eastern Michigan University

CERTIFICATION
• XRF-Lead Inspection
• Certified Asbestos Building Inspector
Accreditation #A34085

• Staff Researcher for Phase I
Environmental Site Assessments.
• Data collection, site investigation, and preparation of Phase I Environmental Site
Assessments.
• Data collection, site investigation, and preparation of Transaction Screen Site
Assessments.
• Experience in implementation and completion of various site assessment standards and professional protocol and commercial lending requirements (ASTM
E-1527-00, ASTM E-1528-00).
• Data collection and evaluation for Phase
II environmental assessment reports.
• Data collection & evaluation of Baseline
Environmental Assessment Reports
• Limited lead containing soil and water sampling. • Limited bulk asbestos containing building material sampling.
• Demolition inspections for commercial & industrial properties.
• Wet-Chem., laboratory analysis.
• Data collection and evaluation for Air
Quality. (Including USEPA Method 1-4,
5, 10, 202)

01/24/2006

PM Environmental, Inc.

PROFESSIONAL RESUME

PM ENVIRONMENTAL, INC.

Steven E. Price
VICE PRESIDENT AND SENIOR TECHNICAL MANAGER
EDUCATION

EXPERIENCE



Peer/Senior Technical review for Due
Care Analysis for Category N, D, and S
Baseline Environmental Assessments in accordance with Natural Resources and Environmental Protection Act,
P.A. 451 of 1994, Part 201 and 213.

B.S. Industrial and Environmental Health Mr. Price is a Vice President and Senior
Management, Minor in Biology, Ferris Technical Manager for PM Environmental,
State University
Inc. His responsibilities include project management and supervision, evaluation and assessment of contaminated sites, coordination
CERTIFICATION
of field activities, preparation of reports, and • Peer/Senior Technical review of
Phase I environmental site assessment
OSHA 1910.120 Hazardous Waste senior technical review. Areas of expertise include: projects using ASTM Standard
Training
1527-00.
American Red Cross Standard First Aid & • Extensive experience in real estate portfolio analysis for evaluation of environmental risk • Peer/Senior Technical review for Phase
Adult CPR associated with single and multi property
II and III environmental site transactions for the lending industry. assessment projects.
Certified Asbestos Building Inspector
Accreditation
• Involved in the collateral and exposure • Peer/Senior Technical review for
# A11991 analysis for over 4,000 real estate leaking underground storage tank transactions; including single and multi
(LUST) projects, including for risk
PROFESSIONAL ACTIVITIES commercial, industrial and multi state evaluation for the lending industry. properties. Michigan Association of Environmental
• Expertise in compliance with the
Professionals
• Lead environmental risk manager for several
Natural Resources and Environmental single and multi state, multi property
Protection Act, P.A. 451 of 1994, Parts
Environmental Bankers Association participation/syndication transactions;
201, 211, 213, and 215. including acting as Agent bank and coordination with participating bank • Technical review of land use based environmental risk managers. corrective action plans.


Experience in extensive bank branch real • Experienced with Local, State, and estate portfolio, including environmental risk
Federal regulatory acts. analysis/reduction relating to asbestos containing materials, lead based paint, mold, • Technical review of feasibility studies and environmental due diligence during for the remediation of soil and acquisition and divestment of branch groundwater. locations.
• Technical review of generic and site• Experience in the management of specific risk assessments. environmental due diligence associated with the foreclosed properties.
• Experienced with on-site management of the containment and recovery of
• Peer/Senior Technical review baseline dense non-aqueous phase liquids environmental assessments (BEA) projects
(DNAPLs).
including Category N, D, and S Baseline
Environmental Assessments in accordance with the
Natural
Resources and Environmental Protection Ace, P.A. 451 of
1994, Part 201 and 213.

11/4/04

PM Environmental, Inc.

Appendix B

PM ENVIRONMENTAL, INC., PROJECT NUMBER 22-692
PHASE I ENVIRONMENTAL SITE ASSESSMENT

Location:
Former Active Homes Manufacturing Building
7876 Van Dyke
Marlette, Michigan
Prepared For:
Mr. Martin Pasquinelli
Structure and Site
32375 Plumwood
Beverly Hills, Michigan

PHASE I ENVIRONMENTAL SITE ASSESSMENT
OF THE FORMER ACTIVE HOMES
MANUFACTURING BUILDING LOCATED AT
7876 VAN DYKE
MARLETTE, MICHIGAN
June 23, 2005
Prepared by:
PM Environmental, Inc.
22655 South Chrysler Drive
Hazel Park, Michigan, 48030

22655 S. Chrysler Dr.
Hazel Park, MI 48030
248-336-9988

3340 Ranger Road
Lansing, MI 48906
517-485-3333

1441 Arboretum Dr. SE Ste. 200
Grand Rapids, MI 49546
616-285-8857

Phase I ESA of the Former Active Homes Manufacturing Building Located at
7876 Van Dyke, Marlette, Michigan
PME Project No. 22-692; June 23, 2005

EXECUTIVE SUMMARY
PM Environmental, Inc., (PME) has completed a Phase I Environmental Site Assessment (ESA) of the Former Active Homes Manufacturing Building located at 7876 Van Dyke, Marlette,
Lapeer County, Michigan (hereafter referred to as the “subject site”). The Phase I ESA was completed in general accordance with the American Society for Testing and Materials (ASTM)
Standard Practice for Environmental Site Assessments: Phase I ESA Process (ASTM
Designation: E-1527-2000).
THE REPORT WAS PREPARED FOR THE EXCLUSIVE USE OF RTJ GROUP, LLC,
WHO MAY RELY ON THE REPORT’S CONTENTS.
The scope of this Phase I ESA included a review of reasonably ascertainable aerial photography, city directories, Sanborn Fire Insurance Maps, local tax assessment records, local fire department records, local building department records, and local health department records. The scope also included a review of any previous site investigations, the current topographical map, and regulatory databases. A visual inspection of the subject site property and of the adjoining properties was also completed. A limited visual inspection for Asbestos Containing Materials was completed. Michigan Department of Environmental Quality (MDEQ) files for the subject site and any properties that PME has determined to be a potential Recognized Environmental
Condition (REC) to the subject site were also reviewed. Additionally, interviews with knowledgeable site contacts were conducted. No subsurface investigation of the property was undertaken as part of this Phase I ESA.
The subject site property is approximately 34.12 acres of land, containing the main manufacturing building, located on the western portion of the building. In addition, an office building is located west of the main building. The main building was originally constructed in approximately 1950, with several additions built throughout the years, and contains a total approximately 378,420-square feet of floor space. The current office building was constructed in
1996 and contains approximately 7,656-square feet of floor space, which is divided into offices and bathrooms. Unpaved parking areas are located to the north and west of the subject site buildings. Overgrown vegetation is located east and south of the subject site building. There is a metal canopy located east of the main building. In addition, there is a water tower located east of the building. The remainder of the property is vacant/undeveloped land.
Reasonably ascertainable records for the subject site extended back to approximately 1941. Data failure occurred prior to that date. Standard and other historical sources were able to document that the first developed use of the subject site occurred in at least 1950, with the construction of the main manufacturing building, with several additions throughout the years. The subject site has operated as a modular home manufacturer since development in 1950. In approximately
2003, the operations were abandoned and the subject site building has been unoccupied since.
The current office building was constructed in 1996, which replaced the original office. PME was unable to determine the initial construction date of the historical office building. Prior to development, in 1950, the subject site was utilized as an agricultural field.

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Phase I ESA of the Former Active Homes Manufacturing Building Located at
7876 Van Dyke, Marlette, Michigan
PME Project No. 22-692; June 23, 2005

PME has not identified any previous site investigations for the subject site property.
The subject site building is connected to natural gas, which is supplied by SEMCo. PME was unable to determine the natural gas availability for the subject site area, and the possibility exists that an alternative-heating source was utilized. The original date of development at the site was approximately 1950; therefore, the subject site may have utilized an underground storage tank
(UST) for heating oil storage. The subject site currently utilizes a water well and septic system.
No sites were identified in the state and federal regulatory database.
Historical RECs
A historical REC, as defined in the ASTM Standard, is a REC that was previously identified and has been adequately addressed, and no longer represents a REC. PME has not identified any historical RECs in association with the subject site.
Non CERCLA Related Concerns
PME observed suspect friable ACM including suspended 12” by 12” ceiling tiles and damaged drywall (locker rooms and offices within the main manufacturing building) and spray applied surfacing on walls (eastern portion of the main manufacturing building). PME observed suspect non-friable ACM including linoleum flooring and drywall walls. PME was unable to locate a boiler room and did not have access to the office building and therefore, cannot comment on the presence of ACM within the boiler room or the office building. PME recommends a full asbestos inspection prior to any renovations or demolition.
PME observed excessive mold throughout the manufacturing area of the main building, due to water damage. PME recommends addition investigation of the mold throughout the building.
No sensitive ecological areas were observed on the subject site property, including potential wetlands. PME observed a pad-mounted transformer located to the west of the subject site building. The transformer, which is likely owned by Detroit Edison (DTE), did not contain a label indicating
PCB content; however, the transformer appeared to be good condition with no evidence of leaks.
Environmental Non Compliance
No environmental non-compliance issues were identified.
Potential Areas of Concern
No PAOC’s were identified.
Current RECs

ii

Phase I ESA of the Former Active Homes Manufacturing Building Located at
7876 Van Dyke, Marlette, Michigan
PME Project No. 22-692; June 23, 2005

In the professional opinion of PME, an appropriate level of inquiry has been made into the previous ownership and uses of the property consistent with good commercial and customary practice in an effort to minimize liability, and no evidence or indication of on-site RECs has been revealed, except for the following:


The subject site building has operated as a mobile home manufacturing facility. PME observed a staging area of the 55-gallon drums and ASTs, containing waste oil and unlabeled substances. This staging area was located within the northeastern portion of the manufacturing building. PME observed staining around the 55-gallon drums and
AST storage and within expansion joints. The waste management practices of the historical occupants are unknown.



The integrity of the floor drains in the buildings is unknown. The potential failure of the drainage system (i.e. cracks, leaks) to have occurred over time, and the current and historical usage of hazardous substances has been identified as a REC.



PME was unable to determine the natural gas availability for the subject site area, the possibility exists that an alternative-heating source was utilized. PME has not identified a previous fuel source for heating through reasonably ascertainable standard and other historic sources consulted. The original date of development at the site was approximately 1950; therefore, the subject site may have utilized an AST or UST for heating oil storage, which represents a REC. The possibility exists for an orphan fuel oil
UST to be present at the subject site.



Based on the usage of the building as a manufacturing facility, the use and storage of petroleum based substances and the unknown waste management practices represent a concern in regards to the septic system. The potential exists for the interior floor drains to lead to the septic system. PME was unable to identify the location of the septic field.

These RECs have been brought to the attention of the client within the requirements of the
ASTM Standard Designation E-1527-2000. Additional site assessment activities may be warranted, and could be completed for approximately $12,375.00.

iii

Phase I ESA of the Former Active Homes Manufacturing Building Located at
7876 Van Dyke, Marlette, Michigan
PME Project No. 22-692; June 23, 2005

The summary presented above is general in nature and should not be considered apart from the entire text of the report, which contains the qualifications, considerations and subject site details mentioned herein. Details of findings and conclusions are elaborated upon in this report.
This report has been reviewed for its completeness and accuracy. Please feel free to contact our office at (248) 336-9988 to discuss this report.
REPORT PREPARED BY:
PM Environmental, Inc.

REPORT REVIEWED BY:
PM Environmental, Inc.

Rachael Koch
Project Consultant

Steve Price
Vice President of Due Diligence

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Phase I ESA of the Former Active Homes Manufacturing Building Located at
7876 Van Dyke, Marlette, Michigan
PME Project No. 22-692; June 23, 2005

LIMITATIONS
This Phase I Environmental Site Assessment (ESA) was prepared in general accordance with the
American Society for Testing and Materials (ASTM) Standard Practice for Environmental Site
Assessments: Phase I ESA Process (ASTM Designation: E-1527-00.
THE REPORT WAS PREPARED FOR THE EXCLUSIVE USE OF RTJ GROUP, LLC,
WHO MAY RELY ON THE REPORT’S CONTENTS.
There are no deletions from the ASTM Standard. Additions to the ASTM Standard include a limited visual inspection for asbestos containing materials.
PM Environmental, Inc. (PME) performed its services in conformance with the care and skill ordinarily used by other reputable environmental consulting firms practicing under similar conditions, at the same time, and in the same or similar locality. In preparing the assessment report, PME may have relied on information obtained from or provided by others. PME makes no representation or warranty regarding the accuracy or completeness of this information gathered through outside sources or subcontracted services. No warranty, guarantee, or certification of any kind, expressed or implied, at common law or created by statute, is extended, made, or intended by rendering these environmental consulting services or by furnishing this written report. No single page of this report should be relied upon alone rather only the report in its entirety. Environmental conditions and regulations are subject to constant change and reinterpretation. One should not assume that any on-site conditions and/or regulatory statutes or rules will remain constant in the future, after PME has completed the scope of work for this project. Furthermore, because of the facts stated in this report are subject to professional interpretation, differing conclusions could be reached by other professionals.
Contaminants may be hidden in subsurface material, covered by pavement, vegetation, or other substances. Additionally, contamination may not be present in predictable locations. The most that PME can do is prepare a logical assessment program to reduce the client's risk of discovering unknown contamination. This risk may be reduced by more extensive exploration on the site. Even with additional exploration, it is not possible to completely eliminate the risk of discovering contamination on-site. It cannot be assumed that samples collected and conditions observed are representative of an area that has not been sampled and/or tested. Tests and other data collected for the report were obtained only for the sole purposes stated in this report, and they should not be used for purposes or reasons other than those intended.
Present on the subject site was a building, asphalt paved areas, dense vegetation, and exterior storage, which limited PME’s observation of the ground surface. PME cannot make any conclusions regarding the potential for visible signs of contamination at areas covered by the aforementioned items. PME can further evaluate these covered areas at a later date when the land/surface cover is not present.
ASTM Standard Practice E-1527-00 defines all appropriate inquiry. ASTM’s definition is aimed at providing an industry standard in an effort to guide legal interpretation of the Comprehensive
Environmental Response, Compensation and Liability Act’s (CERCLA’s) “innocent land owner v Phase I ESA of the Former Active Homes Manufacturing Building Located at
7876 Van Dyke, Marlette, Michigan
PME Project No. 22-692; June 23, 2005

defense.” Even with ASTM’s definition, the level of investigation necessary to demonstrate
“due diligence” or “all appropriate inquiry” has not been legislatively defined by federal, state, or local law; therefore, PM Environmental, Inc., cannot warrant that the work undertaken for this report will satisfy “due diligence,” “all appropriate inquiry,” or any other similar standard under any federal, state, or local law.
Due to changing environmental regulatory conditions and potential on-site or off-site activities occurring after this assessment, the client may not presume the continuing applicability to the site of the conclusions in this assessment for more than 180 days after the report’s issuance date.
Any reports, field data, field notes, laboratory testing, calculations, estimates or other documents prepared by or relied upon by PME are the property of PME. If any of these documents are released or obtained by a party other than the client, PME may not discuss the project with that party unless the original contracted client notifies PME of the same and PME is authorized to disclose the information and to discuss the project with others. PME further states that it disclaims any duty of any kind or nature to any person or entity other than the client in preparing this report, except as otherwise agreed with the client.
PME does not assume liability for any losses or damages that the client or third party incur due to the results or conclusions provided in this assessment.

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Phase I ESA of the Former Active Homes Manufacturing Building Located at
7876 Van Dyke, Marlette, Michigan
PME Project No. 22-692; June 23, 2005

TABLE OF CONTENTS
SECTION 1.0 – SITE OVERVIEW............................................................................................... 1
SECTION 2.0 – HISTORICAL REVIEW ..................................................................................... 1
Section 2.1: Chain of Title .................................................................................................. 2
Section 2.1.1: Environmental Liens........................................................................ 2
Section 2.2: Aerial Photographs and Sanborn Map Coverage............................................ 2
Section 2.3: City Directories............................................................................................... 3
Section 2.4: Interviews with Knowledgeable Site Contacts ............................................... 4
Section 2.4.1: Interview with Owner ...................................................................... 4
Section 2.4.2: Interview with “key site manager” .................................................. 4
Section 2.4.3: Interview with Occupants ................................................................ 4
Section 2.4.4: Interview with Local Government Officials.................................... 5
Section 2.4.4a: Local Fire Department ....................................................... 5
Section 2.4.4b: Local Health Department................................................... 5
Section 2.4.5: Interview with Others ...................................................................... 5
Section 2.5: Building Department/Assessing Records ....................................................... 5
Section 2.5.1: Zoning Department Records............................................................ 5
Section 2.6: Previous Site Investigations............................................................................ 6
Section 2.6.1: List of Previous Reports .................................................................. 6
Section 2.6.2: Summary of Previous Investigations ............................................... 6
Section 2.6.3: PME’s Opinion of Adequacy of Previous Investigations................ 6
SECTION 3.0 - SITE INSPECTION.............................................................................................. 6
Section 3.1: Name of Inspector(s), Date and Time of Inspection....................................... 6
Section 3.1.1: Weather............................................................................................ 6
Section 3.1.2: Physical Setting................................................................................ 6
Section 3.1.3: Current Property Use ....................................................................... 7
Section 3.1.4: Intended Property Use ..................................................................... 7
Section 3.1.5: Utilities............................................................................................. 7
Section 3.1.5a: Municipal Water/Water Wells ........................................... 7
Section 3.1.5b: Sanitary Sewer/Septic System ........................................... 7
Section 3.1.5c: Storm Sewer/Storm Water Detention Ponds...................... 7
Section 3.2: Description of Site Building ........................................................................... 7
Section 3.2.1: Description of Current Business Operations ................................... 8
Section 3.2.2: Current Interior Hazardous Material Usage/Storage ....................... 8
Section 3.2.3: Current Interior Waste Streams ....................................................... 8
Section 3.2.4: Historical Interior Waste Streams.................................................... 8
Section 3.2.5: Interior Pits, Drains, Sumps and Drywells ...................................... 9
Section 3.3: Description of the Remainder of the Property (Excluding Site Buildings) .... 9
Section 3.3.1: Exterior Site Operations................................................................... 9
Section 3.3.2: Exterior Pits, Ponds, and Lagoons ................................................... 9
Section 3.3.3: Exterior Waste Storage .................................................................... 9
Section 3.3.4: Solid Waste Storage and Disposal ................................................... 9
Section 3.4: Agricultural Waste.......................................................................................... 9
Section 3.5: Underground Storage Tanks and Aboveground Storage Tanks ................... 10
Section 3.5.1: USTs .............................................................................................. 10 vii Phase I ESA of the Former Active Homes Manufacturing Building Located at
7876 Van Dyke, Marlette, Michigan
PME Project No. 22-692; June 23, 2005

Section 3.5.2: ASTs/55-Gallon Drums ................................................................. 10
Section 3.6: Potential PCB Containing Materials............................................................. 10
Section 3.7: Electromagnetic Fields ................................................................................. 11
Section 3.8: Oil and Gas Wells ......................................................................................... 11
Section 3.9: Topography................................................................................................... 11
Section 3.9.1: Drainage Patterns........................................................................... 11
Section 3.9.2: General Soil Profile ....................................................................... 11
Section 3.9.3: Geology.......................................................................................... 12
Section 3.9.4: Depth to Groundwater & Local Groundwater Flow...................... 12
Section 3.10: Adjoining Properties ................................................................................... 12
SECTION 4.0 - ASBESTOS CONTAINING MATERIALS (ACM) INSPECTION ................. 13
Section 4.1: Identification of Certified Asbestos Inspector .............................................. 13
Section 4.2: Suspect Friable and Non-Friable ACM ....................................................... 14
Section 4.3: Analytical Results of Suspect Friable and Non-Friable ACM .................... 14
SECTION 5.0 - REGULATORY FILE REVIEW ....................................................................... 14
Section 5.1: NPL............................................................................................................... 14
Section 5.2: CERCLIS/NFRAP ........................................................................................ 15
Section 5.3: State Master Lists.......................................................................................... 15
Section 5.4: TSDFs ........................................................................................................... 15
Section 5.5: RCRA Generator of Hazardous Waste ......................................................... 15
Section 5.6: ERNS ............................................................................................................ 15
Section 5.7: LUSTs........................................................................................................... 15
Section 5.8: Solid Waste Landfills.................................................................................... 16
Section 5.9: USTs ............................................................................................................. 16
SECTION 6.0 - LEAD BASED PAINT SCREEN ...................................................................... 16
SECTION 7.0 - PRELIMINARY RADON INSPECTION ......................................................... 16
SECTION 8.0 - LEAD IN WATER TESTING............................................................................ 16
SECTION 9.0 - WETLANDS INVESTIGATION ...................................................................... 16
SECTION 10.0 - MULTI-MEDIA COMPLIANCE INSPECTION............................................ 16
SECTION 11.0 - FINDINGS, OPINIONS, CONCLUSIONS, RECOMMENDATIONS .......... 16
Section 11.1: Findings ...................................................................................................... 16
Section 11.1.1: On-Site RECs............................................................................... 17
Section 11.1.2: Off-Site RECs .............................................................................. 17
Section 11.1.3: Historical RECs ........................................................................... 17
Section 11.1.4: Non CERCLA Related Concerns ................................................ 17
Section 11.1.5: Environmental Non Compliance ................................................. 18
Section 11.2: Opinions & Conclusions............................................................................. 18
Section 11.3: Recommendations....................................................................................... 18

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Phase I ESA of the Former Active Homes Manufacturing Building Located at
7876 Van Dyke, Marlette, Michigan
PME Project No. 22-692; June 23, 2005

TABLES
Table 1:
Table 2:

Aerial and Sanborn Summary for the Subject Site
Aerial and Sanborn Summary for the Adjacent Properties

FIGURES
Figure 1:
Figure 2:

Site Location Map
Generalized Diagram of the Subject Site and Surrounding Area

APPENDICES
Appendix A:
Appendix B:
Appendix C:
Appendix D:
Appendix E:
Appendix F:
Appendix G:
Appendix H:
Appendix I:
Appendix J:

Documentation of Sources Researched
Aerial Photography and Sanborn Maps
Assessing, Building, and Fire Department Records
Previous Site Investigations
Color Photos from Site Reconnaissance
Professional Resumes
Utility Information
Soil Survey Information
Supplemental Information
State & Federal Regulatory Database and File Review Documentation and
Correspondence
Appendix K: Signed Proposal for Scope of Work and List of Acronyms and
Terminology Used in This Report

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Phase I ESA of the Former Active Homes Manufacturing Building Located at
7876 Van Dyke, Marlette, Michigan
PME Project No. 22-692; June 23, 2005

SECTION 1.0 – SITE OVERVIEW
The subject site property is approximately 34.12 acres of land, containing the main manufacturing building, located on the western portion of the building. In addition, an office building is located west of the main building. The main building was originally constructed in approximately 1950, with several additions built throughout the years, and contains a total approximately 378,420-square feet of floor space. The current office building was constructed in
1996 and contains approximately 7,656-square feet of floor space, which is divided into offices and bathrooms. Unpaved parking areas are located to the north and west of the subject site buildings. Overgrown vegetation is located east and south of the subject site building. There is a metal canopy located east of the main building. In addition, there is a water tower located east of the building. The remainder of the property is vacant/undeveloped land.
Reasonably ascertainable records for the subject site extended back to approximately 1941. Data failure occurred prior to that date. Standard and other historical sources were able to document that the first developed use of the subject site occurred in at least 1950, with the construction of the main manufacturing building, with several additions throughout the years. The subject site has operated as a modular home manufacturer since development in 1950. In approximately
2003, the operations were abandoned and the subject site building has been unoccupied since.
The current office building was constructed in 1996, which replaced the original office. PME was unable to determine the initial construction date of the historical office building. Prior to development, in 1950, the subject site was utilized as an agricultural field.
Although the mailing address is Marlette, which is located within Sanilac County, the property is just outside the county line in the Township of Burnside in Lapeer County.
SECTION 2.0 – HISTORICAL REVIEW
Research of historical records for the subject site was completed to evaluate the current and past uses of the subject site. The research was completed to assess whether operations were conducted that involved the use, storage and/or disposal of hazardous waste, hazardous substances, and/or petroleum products.
An understanding of the subject site area was obtained from reasonably ascertainable standard and other historical sources extending back to 1940. Data failure occurred prior to that date and between 1941 and 1949, 1951 and 1956. Interviewees provided independent knowledge of subject site and surrounding area usage which in turn provided information confirming historical subject site and general adjoining and surrounding land usage. See Appendix A for specific documentation of standard and other historical sources consulted and availability of these sources. The history of the subject site and adjoining and surrounding areas, which was able to be derived from standard historical sources and other sources to satisfy the ASTM standard requirements for uses of a property (except those excluded by data failure), have been described within the text of this report.

PM Environmental, Inc.
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Phase I ESA of the Former Active Homes Manufacturing Building Located at
7876 Van Dyke, Marlette, Michigan
PME Project No. 22-692; June 23, 2005

Section 2.1: Chain of Title
A chain of title was not conducted for the subject property. PME utilized aerial photography, city directories, assessing information, and interviews with individuals knowledgeable of the subject site area as sources to determine the historical usage of the subject site property (see
Appendix A). Information from these sources is referenced throughout this report.
Section 2.1.1: Environmental Liens
PME contacted Ms. Jackie Barnett, Michigan Department of Environmental Quality (MDEQ),
Remediation and Redevelopment Division (RRD), for information about environmental liens on the subject site. There was no information regarding environmental liens encumbering the subject site, or any pending, threatened, or past environmental litigation, environmental administrative procedures, or notices from government entities regarding possible violations of environmental law or possible environmental liability.
Section 2.2: Aerial Photographs and Sanborn Map Coverage
Historical aerial photography is often useful in identifying past usages of a property or surrounding area, building locations, and discernible notable features, which may indicate potential environmental concerns with regard to the subject site or surrounding area.
Reasonably ascertainable aerial photography was obtained from Michigan State University
Aerial Archive, East Lansing, Michigan for 1941 (scale: unknown), 1957 (scale: unknown), 1964
(scale: unknown), 1972 (scale: unknown), and 1982 (scale: unknown)(Appendix B). PME reviewed the 1996 (scale 1”: 600”), Lapeer County Aerial. Reference to the subject site or adjoining site usages in a particular aerial year is based on information obtained through site observations as well as standard and other historic sources. It should be noted that the scale and resolution of the aerial photographs provided for only general descriptions of the subject site and adjoining properties and limited description and discernment of site-specific features.
Sanborn Fire Insurance Maps are historical map records of fire prevention hazards for specific urban areas. These maps often provide data that sometimes can be used to determine the presence of underground and aboveground storage tanks (USTs/ASTs), type of building materials, location of flammable material storage, and types of businesses that occupied a particular site. Sanborn Fire Insurance Maps typically are dated from the late 1800's to the
1950's, and include updates for selected areas as recently as 1990. Sanborn Fire Insurance Maps were not available for the subject site area.
Table 1: Aerial and Sanborn Summary for the Subject Site
Year and
Source
1941 Aerial
(MSU)

Summary of Information
Based on consistency of vegetation and well defined field perimeters, the subject site appears to be utilized as an agricultural field.

PM Environmental, Inc.
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Phase I ESA of the Former Active Homes Manufacturing Building Located at
7876 Van Dyke, Marlette, Michigan
PME Project No. 22-692; June 23, 2005

1957 Aerial
(MSU)
1964 Aerial
(MSU)
1972 Aerial
(MSU)
1982 Aerial
(MSU)

1996 Aerial
(Lapeer
County)

In this aerial year, the southern portion of the subject site is partially visible; the southern portion of the property appears to be vacant.
The subject site appears to be occupied by one large building, located in the center of the property and a small square building, located on the southern portion of the property. The northern portion of the property is occupied by a parking lot.
In this aerial year, the subject site is covered by the aerial year date and is not visible.
This aerial year appears similar to the 1964 aerial, with the exception of an addition to the building. Due to the dark resolution of the aerial, more definitive details could not be determined.
In this aerial year, there appears to be several additions to the main building. There is a small square building, which is consistent with the current office building, located west of the main building. In addition, there is a small building located southwest of the main building, which is consistent with the display home. There appears to be an unpaved parking lot located west and north of the building. There is exterior storage located east of the building. One water tower is located southeast of the building.

Table 2: Aerial and Sanborn Summary for the Adjoining Properties
Year and
Source

1941 Aerial
(MSU)

1957 Aerial
(MSU)
1964 Aerial
(MSU)
1972 Aerial
(MSU)
1982 Aerial
(MSU)
1996 Aerial
(Lapeer
County)

North Adjoining
Property
Based on consistency of vegetation and well defined field perimeters, this property appears to be utilized as an agricultural field.

Similar to previous aerial year.
Similar to previous aerial year.
Similar to previous aerial year.

East Adjoining
Property
Based on consistency of vegetation and well defined field perimeters, this property appears to be utilized as an agricultural field.
Similar to previous aerial year.
Similar to previous aerial year.
Similar to previous aerial year.
Similar to previous aerial year.

South Adjoining
Property
Based on consistency of vegetation and well defined field perimeters, this property appears to be utilized as an agricultural field.
Similar to previous aerial year.
Similar to previous aerial year.
Similar to previous aerial year.
Similar to previous aerial year.

West Adjoining
Property
Based on consistency of vegetation and well defined field perimeters, this property appears to be utilized as an agricultural field.
Similar to previous aerial year.
Similar to previous aerial year.
Similar to previous aerial year.
Similar to previous aerial year.

Similar to previous aerial year.

Similar to previous aerial year.

Similar to previous aerial year.

Similar to previous aerial year.

Not visible.

Section 2.3: City Directories
Reasonably ascertainable R.L. Polk’s City Directories and Bresser’s Cross-Index Directories of
Marlette, Michigan were researched. Bresser’s Cross-Index Directories indicated the following limited and selective listing for the subject site and adjoining properties from 1993 to 2002. R.L.
Polk Directories were not available for the subject site area prior to 1993. Directories were
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Phase I ESA of the Former Active Homes Manufacturing Building Located at
7876 Van Dyke, Marlette, Michigan
PME Project No. 22-692; June 23, 2005

researched in at least three-year increments. It should not be construed that the earliest date represented is the initial date of occupancy. Other descriptions regarding adjoining property historical usage and development should also be referenced as provided in the text of this report.
Listings that have been “bolded” may represent a REC to the subject site if no other data is available to determine otherwise.
City Directories provided coverage for the subject site area and provide the following limited listing of historical subject site address occupants: The North, East, South, and West adjoining properties did not have listings because they are utilized as agricultural fields.
Subject Site – 7876 Van Dyke
2002 – 1993 No Listings
Subject Site – Additional Address: 7938 Van Dyke
2002 - 1993 Active Homes Corporation
1999 – 1995 Active Building Systems
Section 2.4: Interviews with Knowledgeable Site Contacts
The objective of completing interviews with knowledgeable site contacts is to obtain information about the uses and physical characteristics of the property.
In general, interviewees supported the information reviewed from other historical sources (i.e. aerial photos, city records, etc.).
Section 2.4.1: Interview with Owner
PME was informed the current subject site owner has abandoned the property and is unable to be contacted; therefore, PME was unable to interview the owner.
Section 2.4.2: Interview with “key site manager”
The subject site building is currently unoccupied; therefore, PME was unable to interview a
“key-site manager”.
Section 2.4.3: Interview with Occupants
The ASTM Standard specifies that if the property has five or less occupants, a reasonable attempt to interview a representative from each occupant shall be made. If there are more than five occupants, a reasonable attempt to interview the major occupant(s) shall be made, as well as any occupants whose operations are likely to indicate RECs. For multi-residential properties, residential occupants do not need to be interviewed.
The subject site building is currently unoccupied; therefore, PME was unable to interview
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additional occupants.
Section 2.4.4: Interview with Local Government Officials
PME interviewed representatives from Burnside Township Offices and the Lapeer County
Health Department.
Section 2.4.4a: Local Fire Department
PME attempted to interview the City of Marlette Fire Department, however the fire department is volunteer-only and therefore, there was no information pertaining to the subject site.
Section 2.4.4b: Local Health Department
PME submitted a Freedom of Information Act (FOIA) request to the Lapeer County Health
Department, Environmental Health Division. In addition, PME attempted to contact a representative of Lapeer County Health Department. PME did not receive a response within the time constraints of this report.
Section 2.4.5: Interview with Others
PME interviewed Mr. Tom Lupo, Burnside Township Assessor and Mr. Bill Spencer, Burnside
Township Building Department Manager, on May 19, 2005. Mr. Lupo and Mr. Spencer accompanied PME to the subject site building. Mr. Lupo informed PME the operations at the subject site ceased in approximately 2003, when the owner abandoned the company. In addition,
Mr. Lupo informed PME the subject site had a septic backup and a portion of the building was closed off, and temporary restrooms were installed. Mr. Lupo had limited information pertaining to the subject site.
Section 2.5: Building Department/Assessing Records
PME reviewed Burnside Township Building Department records for the subject site. The records contained one permit (permit number: 605-1996), for the removal and construction of the office building, located west of the main building. The permit was dated November 22,
1996.
Reasonably ascertainable assessment information provided by the Burnside Township Assessor’s
Office was obtained and reviewed. Copies of all available assessment records for the subject site and the current legal description are included in Appendix C. Pertinent information obtained from these records is referenced throughout this report.
Section 2.5.1: Zoning Department Records
Based upon review of the Burnside Township zoning map, the subject site is currently zoned
“Light Industrial.” It is unknown how long this zoning designation has been in place; however, based on the historical usage, it is likely that this site has had a similar zoning since
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approximately 1950.
Section 2.6: Previous Site Investigations
No previous site investigations were identified by PME for the subject site. Previous reports may exist for the subject site, however, none were provided to PME by the client or owner of the property, and none were available with the MDEQ-RRD or WHMD.
Section 2.6.1: List of Previous Reports
Not applicable.
Section 2.6.2: Summary of Previous Investigations
Not applicable.
Section 2.6.3: PME’s Opinion of Adequacy of Previous Investigations
Not applicable.
SECTION 3.0 - SITE INSPECTION
Section 3.1: Name of Inspector(s), Date and Time of Inspection
Mr. Rachael, Project Consultant for PME conducted the site inspection on May 19, 2005, at
10:00 a.m. Qualification statements for the environmental professionals involved in this ESA are included as Appendix F.
Section 3.1.1: Weather
At the time of reconnaissance, weather conditions were approximately 75o F and overcast.
Section 3.1.2: Physical Setting
The subject site consists of a 34.12-acre parcel of land located on the east side of Van Dyke
Road. The subject site building is located on the western portion of the subject site. The eastern portion of the property contains vacant/undeveloped land. There is a small office building and a model display home located west of the main building. Unpaved driveways and parking areas are located to the west and north of the subject site buildings. Overgrown vegetation is located east and south of the buildings.
The subject site is further described as located in Township ten North (T.10N), Range twelve
East (R.12E), Section 25, Marlette, Lapeer County, Michigan.

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Section 3.1.3: Current Property Use
The subject site is currently unoccupied.
Section 3.1.4: Intended Property Use
The intended property use is unknown.
Section 3.1.5: Utilities
The subject site building is connected to natural gas, which is supplied by SEMCo. PME was unable to determine the natural gas availability for the subject site area, and the possibility exists that an alternative-heating source was utilized. The original date of development at the site was approximately 1950; therefore, the subject site may have utilized an UST for heating oil storage.
Section 3.1.5a: Municipal Water/Water Wells
PME interviewed a representative of Burnside Township. The representative of this department indicated that the subject site is not currently connected to municipal water service. PME was unable to locate a water well at the subject site. Burnside Township does not have records pertaining to water well installation.
Section 3.1.5b: Sanitary Sewer/Septic System
PME interviewed a representative of Burnside Township. The representative of this department indicated that the subject site is not currently connected to municipal sewer service. PME was unable to locate the septic field at the subject site. Burnside Township does not have records pertaining to the septic tank installation. In addition, Mr. Lupo, Burnside Township Assessor informed PME the subject site had a septic backup and a portion of the building was closed off, and temporary restrooms were installed. The potential exists for the interior floor drains to lead to the septic system. The usage of the building as a manufacturing facility; the use and storage of petroleum based substances; the unknown waste management practices represent a concern to the septic system.
Section 3.1.5c: Storm Sewer/Storm Water Detention Ponds
PME did not observe storm water catch basins at the subject site.
Section 3.2: Description of Site Building
The subject site property is approximately 34.12 acres of land, containing the main manufacturing building, located on the western portion of the building. In addition, the office building is located west of the main building. The main building was originally constructed in approximately 1950, with several additions throughout the years, and contains a total of approximately 378,420-square feet of floor space, which is divided into offices, a shop area,
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storage areas (photograph #5), a tool room and bathrooms. The current office building was constructed in 1996 and contains approximately 7,656-square feet of floor space, which is divided into offices and bathrooms.
PME was unable to determine the locations of the historical operations.
PME did not have access to the office building. However, limited observations were made.
Interior finish materials in the office building include 2-foot by 4-foot suspended acoustical ceiling tile, carpeting, drywall walls. The main manufacturing building is unfinished with concrete block walls, drywall walls, 12” by 12” glue-on ceiling tiles (within the offices of the manufacturing area), metal-deck roof, concrete slab floors and linoleum floors. PME observed two truck wells located within the manufacturing, located along the eastern portion of the building. PME observed excessive mold throughout the manufacturing area of the main building, due to water damage. PME recommends addition investigation of the mold throughout the building.
PME was informed that the subject site building is heated with natural gas. PME was unable to locate the furnace and/or boiler room.
Section 3.2.1: Description of Current Business Operations
The subject site is currently unoccupied; therefore, there are no current operations.
Section 3.2.2: Current Interior Hazardous Material Usage/Storage
The subject site is currently unoccupied; therefore, there is no current hazardous material usage.
PME observed several 55-gallon drums and ASTs (of unknown contents) within the main building. Refer to Section 3.5.2 for additional information.
Section 3.2.3: Current Interior Waste Streams
The subject site is currently unoccupied; therefore, there are no current interior waste streams.
Section 3.2.4: Historical Interior Waste Streams
The subject site has been utilized as a modular home manufacturing facility, since approximately
1950. Although the subject site has been owned by several companies in the past, the operations have consistently been the same. Interior waste streams included: the disposal of vinyl siding, wood pallets, and limited waste oils. PME observed ASTs and 55-gallon drums within the main manufacturing. The unknown historical waste management practices represent a REC to the subject site.

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Section 3.2.5: Interior Pits, Drains, Sumps and Drywells
PME identified one floor drain within the subject site building, located in the northern portion of the manufacturing. PME did not observe any significant staining around the floor drain. PME did not have access to the bathrooms, due to historical plumbing problems. The integrity of the floor drains in the buildings historically utilized for manufactured home assembly is unknown.
The potential failure of the drainage system (i.e. cracks, leaks) to have occurred over time, and the current and historical usage of hazardous substances and represents a REC for the subject site.
PME has not identified any interior underground pits, sumps or dry wells.
Section 3.3: Description of the Remainder of the Property (Excluding Site Buildings)
Unpaved parking areas are located to the north and west of the subject site buildings.
Overgrown vegetation is located east and south of the subject site building. There is a metal canopy located east of the main building, for exterior storage. In addition, there is a water tower located east of the building.
Section 3.3.1: Exterior Site Operations
Current and historical exterior site operations consist of temporary vehicle parking, which does not represent a REC.
Review of aerial photographs indicates exterior storage of trailers and modular homes, which does not represent a REC.
Section 3.3.2: Exterior Pits, Ponds, and Lagoons
No pits, ponds, or lagoons were identified on the subject site property during the site reconnaissance. Section 3.3.3: Exterior Waste Storage
The subject site is currently unoccupied; therefore, there was no exterior waste storage.
Section 3.3.4: Solid Waste Storage and Disposal
The subject site is currently unoccupied; therefore, there was no solid waste storage or disposal.
Section 3.4: Agricultural Waste
The subject site property may have historically been utilized for agricultural purposes. In PME’s professional experience, historical records regarding crop growth are archived or are not necessarily recorded unless a farmer is certified under a state or federal program and therefore are not considered reasonably accessible or pertinent within consideration of time and cost
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constraints and practical application of obtaining such information. Most agri-chemicals sprayed on crops are diluted with water. The mere historical agricultural cropland usage of the subject site is viewed as a de minimis condition by PME as defined in the ASTM Standard E-1527-00.
Areas of agricultural land that present the potential for environmental concerns are chemical and pesticide storage and mixing area where concentrated spills can occur, vehicle maintenance areas, land disposal areas, fuel supply areas, and dry wells. No such areas (i.e., “farm hubs”) have been identified with the subject site property through review of reasonable ascertainable standard and other historical sources.
Section 3.5: Underground Storage Tanks and Aboveground Storage Tanks
Section 3.5.1: USTs
Review of reasonably ascertainable standard and other historical sources, and site observations, have not identified the current and historical presence of USTs on the subject site. Specifically, no records of USTs are on file with the MDEQ-RRD, Lansing, Michigan, and PME did not observe any evidence of USTs (i.e. fill ports, vent pipes, etc.) during the site reconnaissance.
Section 3.5.2: ASTs/55-Gallon Drums
The EPA’s Oil Pollution Prevention Rule became effective January 10, 1974, and was revised on
July 17, 2002. Facilities subject to the rule must prepare and implement a plan to prevent any discharge of oil into or upon navigable waters or adjoining shorelines. The plan is called a Spill
Prevention, Control, and Countermeasure (SPCC) Plan. A facility with an aggregate aboveground storage capacity of 1,320 gallons or more of any kind of oil, including but not limited to petroleum, fuel oil, sludge, oil refuse, oil mixed with wastes other than dredged spoil, fats, oils or greases from animals, vegetable oils, synthetic oils, and mineral oils, is subject to the
SPCC Rule.
PME observed one 250-gallon and two 500-gallon ASTs within secondary containment.
Additionally, PME observed several 55-gallon drums located within secondary containment.
PME was unable to identify the contents of the ASTs and 55-gallon drums, with the exception of two 55-gallon drums labeled “waste oil” and “engine-diesel fuel”. The staging area of the ASTs and 55-gallon drums is located within the northern portion of the manufacturing building. The
ASTs and 55-gallon drums were abandoned and need to be properly disposed of. PME observed limited staining on the concrete floor surrounding the AST and 55-gallon drum storage. The waste management practices of the historical occupants are unknown, which represents a
REC to the subject site.
Section 3.6: Potential PCB Containing Materials
Older transformers and other electrical equipment could contain PCBs at a level that subjects them to regulation by the United States Environmental Protection Agency (U.S. EPA). PCBs in electrical equipment are controlled by U.S. EPA regulations 40 CFR, Part 761. Under the regulations, there are three categories into which electrical equipment can be classified:

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Less than 50 parts per million (PPM) of PCBs - “Non-PCB” transformer
50 ppm–500 ppm - “PCB-Contaminated” electrical equipment
Greater than 500 ppm - “PCB” transformer

During site reconnaissance, PME observed a pad-mounted transformer located to the west of the subject site building. The transformer, which is likely owned by Detroit Edison (DTE), did not contain a label indicating PCB content; however, the transformer appeared to be good condition with no evidence of leaks.
Section 3.7: Electromagnetic Fields
Identification of electromagnetic fields is not included within the scope of work for this Phase I
ESA. However, PME did not observe any high tension wires or substations in the vicinity of the subject site.
Section 3.8: Oil and Gas Wells
PME reviewed the MDEQ-Geologic Survey Division (GSD) web site (www.deq.state.mi.us/mir) to determine if an oil and/or gas well existed previously on the subject site or surrounding area.
No records of an oil and/or gas well existing on or adjacent to the subject site area were identified. Section 3.9: Topography
The United States Geological Survey Division (U.S.G.S.) 7.5-Minute Topographic Map of the
Marlette, Michigan Quadrangle, 1963 (photo revised in 1980) for the subject site was reviewed in accordance with the ASTM standards (Figure 1). The map was reviewed to determine if conditions exist whereby hazardous substances or petroleum products migrate to or from the subject site to surface water, groundwater or soil.
Based on the topographic map, the subject site is located at an elevation of 845 feet above mean sea level. The immediate subject site area appears to slope to the southeast toward the Columbus
Drain, which is located approximately one-half of a mile away at an elevation of 810 feet.
Section 3.9.1: Drainage Patterns
The subject site and surrounding properties appear to be sloped to the southeast. Storm water likely penetrates the subsurface in the unpaved portions of the subject site.
Section 3.9.2: General Soil Profile
According to information available from the United States Department of Agriculture, Soil
Survey of Lapeer County, Michigan (published January 1972) the subject site area is generally characterized by the following soil types (Appendix H):

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Capac fine sandy loam, 0 to 2 percent slopes, which is characterized by sparse areas of deciduous tree forest litter from 0 to 2 inches bgs, otherwise, grayish brown to yellow sandy loam from 0 to
12 inches bgs, grayish brown to yellowish brown clay loam from 12 to 34 inches bgs, and gray loam from 34 + inches bgs.
Section 3.9.3: Geology
The “Hydrogeologic Atlas of Michigan”, produced by Western Michigan University and the
United States Environmental Protection Agency, 1981; “Quaternary Geology of Southern
Michigan”, Department of Geological Sciences, University of Michigan, Ann Arbor, Michigan
(1982); and “Bedrock Geology of Southern Michigan”, Michigan Department of Natural
Resources (MDNR), Geological Survey Division (1987) were reviewed.
According to the aforementioned sources, in this area of Lapeer County, quaternary deposits are underlain by bedrock composed of Marshall Sandstone of the Mississippian System. Bedrock is covered by end moraines of coarse-textured till, which is described as “grayish to reddish brown, non-sorted glacial debris; matrix is dominantly sandy clay loam, sandy loam, or loamy sand texture, locally resembles outwash except for sporadic occurrence of non-sorted clayey or silty lenses and lack or stratification; variable amounts of cobbles and boulders. Occurs in narrow linear belts of hummocky relief marking former stillstands of ice-sheet margin. Includes small areas of ground moraine as well as outwash. Thickness tends to be somewhat greater than adjacent ground moraine areas.”
Section 3.9.4: Depth to Groundwater & Local Groundwater Flow
A review of topographic features/gradient may be suggestive of the hydrogeologic gradient in the immediate subject site area, since in a general way, the water table typically conforms to surface topography. Based solely on topographical features, the anticipated groundwater flow direction would be to the southeast.
Section 3.10: Adjoining Properties
A visual inspection of the adjoining properties was made from the subject site and public thoroughfares. Color photographs are included within Appendix E. Refer to Sections 2.2 and
2.3 for details on historical usage.
North Adjoining Property
The north adjoining property is currently occupied by an agricultural field (photograph #16).
Review of aerial photography documents that this site has been utilized as an agricultural field since at least 1941 until present.

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East Adjoining Property
The east adjoining property is currently occupied by an agricultural field (photograph #17).
Review of aerial photography documents that this site has been utilized as an agricultural field since at least 1941 until present.
South Adjoining Property
The south adjoining property is currently occupied by an agricultural field. Review of aerial photography documents that this site has been utilized as an agricultural field since at least 1941 until present.
West Adjoining Property
The west adjoining property is currently occupied by an agricultural field (photograph #18).
Review of aerial photography documents that this site has been utilized as an agricultural field since at least 1941 until present.
SECTION 4.0 - ASBESTOS CONTAINING MATERIALS (ACM) INSPECTION
Asbestos containing products are often referred to as “asbestos containing materials” (ACM) and can include floor tile, plaster, drywall, surfacing, pipe wrap, roofing materials, siding and many other common building materials. ASTM Standard Designation E-1527-2000 and NESHAP regulations define ACM as containing more than one percent asbestos, which is also considered regulated ACM. Friable ACM is ACM that can be crumbled, pulverized, or reduced to powder by hand pressure. Non-friable refers to materials that contain asbestos bound by cement, plastic, adhesive, etc., (i.e. gaskets, floor coverings, roofing materials, etc.) which if handled through routine maintenance, will not become friable.
PME only performed a limited visual inspection for suspect ACM during the site reconnaissance as part of the Phase I ESA process. Therefore, PME’s inspection or survey did not strictly adhere to AHERA, NESHAP, or OSHA regulations, since this is not the purpose a Phase I ESA.
This limited survey likely is not adequate to identify all suspect ACM, if the building is constructed prior to 1980, or is scheduled for renovation or demolition. Additional sampling may be necessary. PME can provide a separate proposal for additional sampling if requested
Access in building structural columns or equipment liners (i.e., building columns, supports, behind walls, boiler or tank interiors, above ceilings, etc.), destructive sampling, random sampling, etc. were not included as part of this limited inspection.
Section 4.1: Identification of Certified Asbestos Inspector
Ms. Rachael Koch, Project Consultant of PME, accredited asbestos inspector (accreditation number A34085), performed a limited visual inspection only. Sampling of suspect ACM was not authorized as part of the scope of work.

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Section 4.2: Suspect Friable and Non-Friable ACM
PME observed suspect friable ACM including suspended 12” by 12” ceiling tiles and damaged drywall (locker rooms and offices within the main manufacturing building) and spray applied surfacing on walls (eastern portion of the main manufacturing building).
PME observed suspect non-friable ACM including linoleum flooring and drywall walls.
PME was unable to locate a boiler room and did not have access to the office building; therefore cannot comment on the presence of ACM within the boiler room.
PME recommends a full asbestos inspection prior to renovations or demolition.
Section 4.3: Analytical Results of Suspect Friable and Non-Friable ACM
PME was not authorized to collect and submit samples of suspect ACM for analysis.
SECTION 5.0 - REGULATORY FILE REVIEW
Appendix J includes the Environmental Data Resources, Inc. (EDR), Milford, Connecticut,
Radius Map Report. This report details facilities found in state and federal environmental databases which are located within a pre-specified distance {i.e., Approximate Minimum Search
Distance (AMSD)} from the subject site. The pre-specified distances are established per the
ASTM Standard (E-1527-2000). ASTM has established search distances for federal and state sites of potential environmental concern and the distances at which particular types of liabilities
(e.g., NPL, CERCLIS, RCRA, etc.) are considered to have potential environmental impact to the subject site. Appendix J contains a brief description of each database. A map locating all identified sites and their distance from the subject site is included in the EDR Radius Map Report within Appendix J.
The radius map included in the report, indicates those sites found within a specified distance of the subject site, and the radius report segments the sites found based on distance from the subject site. Not all sites found in the EDR Radius Map Report are located within the AMSD as specified by ASTM. In addition, sites identified within unmapped section of the EDR Radius
Map Report may be identified as within AMSD by PME through review of additional site location information. Additional sites may also be identified through consultation with State of
Michigan Web site (http://www.michigan.gov/deq) for registered UST and Part 201 Natural
Resources and Environmental Protection Act (NREPA), P.A. 451, 1994, as amended sites. The following is a listing of sites found within the AMSD.
Government Record

Search Distance

Number
Found

Section 5.1: NPL
EPA National Priority List (NPL)

1.0 Mile
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Section 5.2: CERCLIS/NFRAP
EPA Comprehensive Environmental Response,
Compensation and Liability Information
System (CERCLIS) List

0.50 Mile

0

CERCLIS No Further Remedial Action
Planned (NFRAP) sites

Subject Site &
Adjoining

0

State Hazardous Waste Sites (SHWS)
Identified for Investigation or Remediation
(State Equivalent to CERCLIS)

1.0 Mile

0

Baseline Environmental Assessments (BEAs)

0.5 Mile

0

Federal Resource Conservation and
Recovery Act (RCRA) Corrective
Action Report (CORRACTS) Facility list

1.0 Mile

0

RCRA non-CORRACTS Treatment,
Storage and Disposal (TSD) Facility list

0.50 mile

0

Section 5.3: State Master Lists

Section 5.4: TSDFs

Section 5.5: RCRA Generator of Hazardous Waste
RCRA Small Quantity Generator

Subject Site &
Adjoining

0

RCRA Large Quantity Generator

Subject Site &
Adjoining

0

Subject Site

0

0.5 Mile

0

Section 5.6: ERNS
Federal Emergency Response Notification
System (ERNS) List
Section 5.7: LUSTs
Michigan Registered Leaking Underground
Storage Tank (LUST) List

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Section 5.8: Solid Waste Landfills
Solid Waste Disposal/Landfills
(landfill, transfer station) List

0.50 Mile

0

Subject Site &
Adjoining

0

Section 5.9: USTs
Michigan Registered Underground
Storage Tank (UST) List
SECTION 6.0 - LEAD BASED PAINT SCREEN
A lead based paint inspection was not requested or required for this site.
SECTION 7.0 - PRELIMINARY RADON INSPECTION
A radon inspection was not requested or required for this site.
SECTION 8.0 - LEAD IN WATER TESTING
A lead in water inspection was not part of the scope of work for this Phase I ESA.
SECTION 9.0 - WETLANDS INVESTIGATION
A wetlands investigation was not part of the scope of work for this Phase I ESA. However, PME did not observe any wet areas potentially associated with wetlands on the subject site during the site reconnaissance.
SECTION 10.0 - MULTI-MEDIA COMPLIANCE INSPECTION
A multi-media compliance inspection was not required or requested for this Phase I ESA.
SECTION 11.0 - FINDINGS, OPINIONS, CONCLUSIONS, RECOMMENDATIONS
PME has completed the Phase I ESA, in conformance with the scope and limitations of ASTM
Practice E-1527-2000, for the Former Active Homes Manufacturing Building, located at 7876
Van Dyke, Marlette, Lapeer County, Michigan. Any exceptions or deletions from this practice are described in Limitations Section of this report.
Section 11.1: Findings
The following known or suspect environmental conditions associated with the subject site property have been identified. These conditions may include RECs, both on-site and off-site, as well as Historical RECs, non-ASTM findings such as Asbestos-Containing Materials inspection and/or wetland identification, and environmental non-compliance issues.

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Section 11.1.1: On-Site RECs
No evidence or indication of on-site RECs has been revealed with the exception of the following:


The subject site building has operated as a mobile home manufacturing facility. PME observed a staging area of the 55-gallon drums and ASTs, containing waste oil and unlabeled substances. This staging area was located within the northeastern portion of the manufacturing building. PME observed staining around the 55-gallon drums and
AST storage and within expansion joints. The waste management practices of the historical occupants are unknown.



The integrity of the floor drains in the buildings is unknown. The potential failure of the drainage system (i.e. cracks, leaks) to have occurred over time, and the current and historical usage of hazardous substances has been identified as a REC.



PME was unable to determine the natural gas availability for the subject site area, the possibility exists that an alternative-heating source was utilized. PME has not identified a previous fuel source for heating through reasonably ascertainable standard and other historic sources consulted. The original date of development at the site was approximately 1950; therefore, the subject site may have utilized an AST or UST for heating oil storage, which represents a REC. The possibility exists for an orphan fuel oil
UST to be present at the subject site.



Based on the usage of the building as a manufacturing facility, the use and storage of petroleum based substances and the unknown waste management practices represent a concern in regards to the septic system. The potential exists for the interior floor drains to lead to the septic system. PME was unable to identify the location of the septic field.
Section 11.1.2: Off-Site RECs

No evidence or indication of off-site RECs has been revealed for the subject site.
Section 11.1.3: Historical RECs
A historical REC, as defined in the ASTM Standard, is a REC that was previously identified and has been adequately addressed, and no longer represents a REC. PME has not identified any historical RECs in association with the subject site.
Section 11.1.4: Non CERCLA Related Concerns
PME observed suspect friable ACM including suspended 12” by 12” ceiling tiles and damaged drywall (locker rooms and offices within the main manufacturing building) and spray applied surfacing on walls (eastern portion of the main manufacturing building). PME observed suspect non-friable ACM including linoleum flooring and drywall walls. PME was unable to locate a boiler room and did not have access to the office building and therefore, cannot comment on the
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presence of ACM within the boiler room or the office building. PME recommends a full asbestos inspection prior to any renovations or demolition.
PME observed excessive mold throughout the manufacturing area of the main building, due to water damage. PME recommends addition investigation of the mold throughout the building.
No sensitive ecological areas were observed on the subject site property, including potential wetlands. PME observed a pad-mounted transformer located to the west of the subject site building. The transformer, which is likely owned by Detroit Edison (DTE), did not contain a label indicating
PCB content; however, the transformer appeared to be good condition with no evidence of leaks.
Section 11.1.5: Environmental Non Compliance
No environmental non-compliance issues were identified.
Section 11.1.6: Potential Areas of Concern
No PAOC’s were identified.
Section 11.2: Opinions & Conclusions
In the professional opinion of PME, an appropriate level of inquiry has been made into the previous ownership and uses of the property consistent with good commercial and customary practice in an effort to minimize liability.
Section 11.3: Recommendations
The additional investigation, which we believe to be necessary to investigate the on-site REC, would consist of the advancement of eleven soil borings at an estimated cost of $12,375.00.

PM Environmental, Inc.
Page 18

Appendix C

Site Photographs

Subject View of the western portion of the subject site, facing south
Site 7876 Van Dyke, Marlette, Michigan
Client Outlook Properties, LLC

PME
Project No.
22-692

1

Subject View of the northern potion of the property, facing south
Site 7876 Van Dyke, Marlette, Michigan
Client Outlook Properties, LLC

PME
Project No.
22-692

2

Photographs taken on May 19, 2005 by Rachael Koch

Site Photographs

Subject View of the eastern portion of the building, facing south
Site 7876 Van Dyke, Marlette, Michigan
Client Outlook Properties, LLC

PME
Project No.
22-692

3

Subject View of the southern portion of the building, facing east
Site 7876 Van Dyke, Marlette, Michigan
Client Outlook Properties, LLC

PME
Project No.
22-692

4

Photographs taken on May 19, 2005 by Rachael Koch

Site Photographs

Subject View of the western portion of property, facing north
Site 7876 Van Dyke, Marlette, Michigan
Client Outlook Properties, LLC

PME
Project No.
22-692

5

Subject View of the northern portion of the building, facing south
Site 7876 Van Dyke, Marlette, Michigan
Client Outlook Properties, LLC

PME
Project No.
22-692

6

Photographs taken on May 19, 2005 by Rachael Koch

Site Photographs

Subject View of the central portion of the building
Site 7876 Van Dyke, Marlette, Michigan
Client Outlook Properties, LLC

PME
Project No.
22-692

7

Subject View of the southern portion of the building
Site 7876 Van Dyke, Marlette, Michigan
Client Outlook Properties, LLC

PME
Project No.
22-692

8

Photographs taken on May 19, 2005 by Rachael Koch

Site Photographs

Subject View of a portion of wall, covered in mold
Site 7876 Van Dyke, Marlette, Michigan
Client Outlook Properties, LLC

PME
Project No.
22-692

9

Subject View of the spray on insulation
Site 7876 Van Dyke, Marlette, Michigan
Client Outlook Properties, LLC

PME
Project No.
22-692

10

Photographs taken on May 19, 2005 by Rachael Koch

Site Photographs

Subject View of the ASTs, located in the northern portion of the building
Site 7876 Van Dyke, Marlette, Michigan
Client Outlook Properties, LLC

PME
Project No.
22-692

11

Subject View of the 55-gallon drums, located in the northern portion of the building
Site 7876 Van Dyke, Marlette, Michigan
Client Outlook Properties, LLC

PME
Project No.
22-692

12

Photographs taken on May 19, 2005 by Rachael Koch

Site Photographs

Subject View of the pad mounted transformer, located west of the building
Site 7876 Van Dyke, Marlette, Michigan
Client Outlook Properties, LLC

PME
Project No.
22-692

13

Subject View of the canopy covered storage area, located east of the building
Site 7876 Van Dyke, Marlette, Michigan
Client Outlook Properties, LLC

PME
Project No.
22-692

14

Photographs taken on May 19, 2005 by Rachael Koch

Site Photographs

Subject View of the office, located west of the main building
Site 7876 Van Dyke, Marlette, Michigan
Client Outlook Properties, LLC

PME
Project No.
22-692

15

Subject View of the north adjoining property, agricultural land
Site 7876 Van Dyke, Marlette, Michigan
Client Outlook Properties, LLC

PME
Project No.
22-692

16

Photographs taken on May 19, 2005 by Rachael Koch

Site Photographs

Subject View of the east adjoining property
Site 7876 Van Dyke, Marlette, Michigan
Client Outlook Properties, LLC

PME
Project No.
22-692

17

Subject View of the west adjoining property
Site 7876 Van Dyke, Marlette, Michigan
Client Outlook Properties, LLC

PME
Project No.
22-692

18

Photographs taken on May 19, 2005 by Rachael Koch

Appendix D

31628 Glendale St.
Livonia, Michigan 48150
TEL: 734.422.8000
FAX: 734.422.5342
Website: www.rtilab.com

May 05, 2006

Rachael Koch
PM Environmental, Inc.
22655 S. Chrysler Drive
Hazel Park, MI 48030-1705
TEL: (248) 336-9988
FAX (248) 336-9989
RE: 7876 Van Dyke - 22-692A
Dear Rachael Koch:

Order No.: 0604884

RTI Laboratories, Inc. received 10 sample(s) on 4/28/2006 for the analyses presented in the following report.
A Case Narrative has been included denoting specific problems, if any were encountered.
Associated quality control data was within laboratory defined or method specified acceptance limits except as noted.
If you have any questions regarding these tests results, please feel free to call.

Sincerely,

Charles O`Bryan
Director, Quality Management

31628 Glendale St.
Livonia, Michigan 48150
TEL: 734.422.8000
FAX: 734.422.5342
Website: www.rtilab.com

CLIENT:
Project:

Case Narrative
WO#:

0604884

Date:

5/5/2006

PM Environmental, Inc.
7876 Van Dyke - 22-692A

This report in its entirety consists of the documents listed below. All documents contain the RTI Work
Order Number assigned to this report.
1. Paginated Report including: Case Narrative, Analytical Results and Applicable Quality Control
Summary Reports.
2. A Cover Letter that immediately precedes the Paginated Report.
3. Paginated copies of the Chain of Custody Documents supplied with this sample set.
Concentrations reported with a J flag in the Qual field are values below the reporting limit (RL) but greater than the established method detection limit (MDL). There is greater uncertainty associated with these results and data should be considered as estimated.
Concentrations reported with an E flag in the Qual field are values that exceed the upper quantification range. There is greater uncertainty associated with these results and data should be considered as estimated. Any comments or problems with the analytical events associated with this report are noted below.

Page 1 of 66

31628 Glendale St.

Analytical Report

Livonia, Michigan 48150
TEL: 734.422.8000
FAX: 734.422.5342
Website: www.rtilab.com

(consolidated)

WO#:

0604884

Date Reported:

5/5/2006

Collection Date: 4/27/2006 11:35:00 AM

CLIENT:

PM Environmental, Inc.

Project:

7876 Van Dyke - 22-692A

Lab ID:

0604884-001

Matrix: SOIL

Client Sample ID SB-1 1-2'
Analyses

Result

RL Qual Units

DF

Polychlorinated Biphenyls

Date Analyzed
Analyst: MB

SW8082

Aroclor 1016

ND

37

µg/Kg-dry

1

5/2/2006 8:11:29 PM

Aroclor 1221

ND

37

µg/Kg-dry

1

5/2/2006 8:11:29 PM

Aroclor 1232

ND

37

µg/Kg-dry

1

5/2/2006 8:11:29 PM

Aroclor 1242

ND

37

µg/Kg-dry

1

5/2/2006 8:11:29 PM

Aroclor 1248

ND

37

µg/Kg-dry

1

5/2/2006 8:11:29 PM

Aroclor 1254

ND

37

µg/Kg-dry

1

5/2/2006 8:11:29 PM

Aroclor 1260

ND

37

µg/Kg-dry

1

5/2/2006 8:11:29 PM

Surr: Decachlorobiphenyl

75.3

70-130

%REC

1

5/2/2006 8:11:29 PM

Surr: Tetrachloro-m-xylene

67.3

70-130

%REC

1

5/2/2006 8:11:29 PM

530

420

µg/Kg-dry

20

5/1/2006 1:40:01 PM

15,000

2,100

µg/Kg-dry

20

5/1/2006 1:40:01 PM

7,400

2,100

µg/Kg-dry

20

5/1/2006 1:40:01 PM

S

Metals, ICP/MS

Analyst: AB2

SW6020A

Cadmium
Chromium
Lead

Polynuclear Aromatic Hydrocarbons
Semi-Volatile Organic Compounds

Analyst: JG3

SW8270C

2-Methylnaphthalene

ND

370

µg/Kg-dry

1

5/2/2006 4:49:00 PM

Acenaphthene

ND

370

µg/Kg-dry

1

5/2/2006 4:49:00 PM

Acenaphthylene

ND

370

µg/Kg-dry

1

5/2/2006 4:49:00 PM

Anthracene

ND

370

µg/Kg-dry

1

5/2/2006 4:49:00 PM

Benz(a)anthracene

ND

370

µg/Kg-dry

1

5/2/2006 4:49:00 PM

Benzo(a)pyrene

ND

370

µg/Kg-dry

1

5/2/2006 4:49:00 PM

Benzo(b)fluoranthene

ND

370

µg/Kg-dry

1

5/2/2006 4:49:00 PM

Benzo(g,h,i)perylene

ND

370

µg/Kg-dry

1

5/2/2006 4:49:00 PM

Benzo(k)fluoranthene

ND

370

µg/Kg-dry

1

5/2/2006 4:49:00 PM

Chrysene

ND

370

µg/Kg-dry

1

5/2/2006 4:49:00 PM

Dibenz(a,h)anthracene

ND

370

µg/Kg-dry

1

5/2/2006 4:49:00 PM

Fluoranthene

ND

370

µg/Kg-dry

1

5/2/2006 4:49:00 PM

Fluorene

ND

370

µg/Kg-dry

1

5/2/2006 4:49:00 PM

Indeno(1,2,3-cd)pyrene

ND

370

µg/Kg-dry

1

5/2/2006 4:49:00 PM

Naphthalene

ND

370

µg/Kg-dry

1

5/2/2006 4:49:00 PM

Phenanthrene

ND

370

µg/Kg-dry

1

5/2/2006 4:49:00 PM

Pyrene

ND

370

µg/Kg-dry

1

5/2/2006 4:49:00 PM

Surr: 2,4,6-Tribromophenol

74.1

25-93.9

%REC

1

5/2/2006 4:49:00 PM

Surr: 2-Fluorobiphenyl

90.8

26-105

%REC

1

5/2/2006 4:49:00 PM

Qualifiers:

*

Value exceeds Maximum Contaminant Level

B

Analyte detected in the associated Method Blank

E

Value above quantitation range

H

Holding times for preparation or analysis exceeded

M

Manual Integration used to determine area response

RL

Reporting Detection Limit

ND
S

Not Detected at the Reporting Limit
Spike Recovery outside accepted recovery limits

Page 2 of 66

31628 Glendale St.

Analytical Report

Livonia, Michigan 48150
TEL: 734.422.8000
FAX: 734.422.5342
Website: www.rtilab.com

(consolidated)

WO#:

0604884

Date Reported:

5/5/2006

Collection Date: 4/27/2006 11:35:00 AM

CLIENT:

PM Environmental, Inc.

Project:

7876 Van Dyke - 22-692A

Lab ID:

0604884-001

Matrix: SOIL

Client Sample ID SB-1 1-2'
Analyses

Result

RL Qual Units

Polynuclear Aromatic Hydrocarbons
Semi-Volatile Organic Compounds

DF

Date Analyzed
Analyst: JG3

SW8270C

Surr: 2-Fluorophenol

96.7

25-120

%REC

1

5/2/2006 4:49:00 PM

Surr: Nitrobenzene-d5

90.9

30.1-104

%REC

1

5/2/2006 4:49:00 PM

Surr: Phenol-d5

94.7

25-118

%REC

1

5/2/2006 4:49:00 PM

Surr: Terphenyl-d14

92.9

27.1-115

%REC

1

5/2/2006 4:49:00 PM

1,1,1,2-Tetrachloroethane

ND

56

µg/Kg-dry

50.1

5/1/2006 7:45:00 PM

1,1,1-Trichloroethane

ND

56

µg/Kg-dry

50.1

5/1/2006 7:45:00 PM

1,1,2,2-Tetrachloroethane

ND

56

µg/Kg-dry

50.1

5/1/2006 7:45:00 PM

1,1,2-Trichloro-1,2,2-trifluoroethane

ND

56

µg/Kg-dry

50.1

5/1/2006 7:45:00 PM

1,1,2-Trichloroethane

ND

56

µg/Kg-dry

50.1

5/1/2006 7:45:00 PM

1,1-Dichloroethane

ND

56

µg/Kg-dry

50.1

5/1/2006 7:45:00 PM

1,1-Dichloroethene

ND

56

µg/Kg-dry

50.1

5/1/2006 7:45:00 PM

1,1-Dichloropropene

ND

56

µg/Kg-dry

50.1

5/1/2006 7:45:00 PM

1,2,3-Trichlorobenzene

ND

56

µg/Kg-dry

50.1

5/1/2006 7:45:00 PM

1,2,3-Trichloropropane

ND

56

µg/Kg-dry

50.1

5/1/2006 7:45:00 PM

1,2,3-Trimethylbenzene

ND

56

µg/Kg-dry

50.1

5/1/2006 7:45:00 PM

1,2,4-Trichlorobenzene

ND

280

µg/Kg-dry

50.1

5/1/2006 7:45:00 PM

1,2,4-Trimethylbenzene

ND

56

µg/Kg-dry

50.1

5/1/2006 7:45:00 PM

1,2-Dibromo-3-chloropropane

ND

56

µg/Kg-dry

50.1

5/1/2006 7:45:00 PM

1,2-Dichlorobenzene

ND

56

µg/Kg-dry

50.1

5/1/2006 7:45:00 PM

1,2-Dichloroethane

ND

56

µg/Kg-dry

50.1

5/1/2006 7:45:00 PM

1,2-Dichloropropane

ND

56

µg/Kg-dry

50.1

5/1/2006 7:45:00 PM

1,3,5-Trimethylbenzene

ND

56

µg/Kg-dry

50.1

5/1/2006 7:45:00 PM

1,3-Dichlorobenzene

ND

56

µg/Kg-dry

50.1

5/1/2006 7:45:00 PM

1,3-Dichloropropane

ND

56

µg/Kg-dry

50.1

5/1/2006 7:45:00 PM

1,4-Dichlorobenzene

ND

56

µg/Kg-dry

50.1

5/1/2006 7:45:00 PM

2,2-Dichloropropane

ND

56

µg/Kg-dry

50.1

5/1/2006 7:45:00 PM

2-Chloroethyl vinyl ether

ND

560

µg/Kg-dry

50.1

5/1/2006 7:45:00 PM

2-Chlorotoluene

ND

56

µg/Kg-dry

50.1

5/1/2006 7:45:00 PM

2-Hexanone

ND

2,800

µg/Kg-dry

50.1

5/1/2006 7:45:00 PM

2-Methylnaphthalene

ND

280

µg/Kg-dry

50.1

5/1/2006 7:45:00 PM

2-Nitropropane

ND

230

µg/Kg-dry

50.1

5/1/2006 7:45:00 PM

4-Chlorotoluene

ND

56

µg/Kg-dry

50.1

5/1/2006 7:45:00 PM

Acetone

ND

2,800

µg/Kg-dry

50.1

5/1/2006 7:45:00 PM

Volatile Organic Compounds

Qualifiers:

Analyst: JW

SW8260B

*

Value exceeds Maximum Contaminant Level

B

Analyte detected in the associated Method Blank

E

Value above quantitation range

H

Holding times for preparation or analysis exceeded

M

Manual Integration used to determine area response

RL

Reporting Detection Limit

ND
S

Not Detected at the Reporting Limit
Spike Recovery outside accepted recovery limits

Page 3 of 66

31628 Glendale St.

Analytical Report

Livonia, Michigan 48150
TEL: 734.422.8000
FAX: 734.422.5342
Website: www.rtilab.com

(consolidated)

WO#:

0604884

Date Reported:

5/5/2006

Collection Date: 4/27/2006 11:35:00 AM

CLIENT:

PM Environmental, Inc.

Project:

7876 Van Dyke - 22-692A

Lab ID:

0604884-001

Matrix: SOIL

Client Sample ID SB-1 1-2'
Analyses

Result

RL Qual Units

Volatile Organic Compounds

DF

Date Analyzed
Analyst: JW

SW8260B

Acrylonitrile

ND

280

µg/Kg-dry

50.1

5/1/2006 7:45:00 PM

Benzene

ND

56

µg/Kg-dry

50.1

5/1/2006 7:45:00 PM

Bromobenzene

ND

56

µg/Kg-dry

50.1

5/1/2006 7:45:00 PM

Bromochloromethane

ND

56

µg/Kg-dry

50.1

5/1/2006 7:45:00 PM

Bromodichloromethane

ND

56

µg/Kg-dry

50.1

5/1/2006 7:45:00 PM

Bromoform

ND

56

µg/Kg-dry

50.1

5/1/2006 7:45:00 PM

Bromomethane

ND

280

µg/Kg-dry

50.1

5/1/2006 7:45:00 PM

Carbon disulfide

ND

280

µg/Kg-dry

50.1

5/1/2006 7:45:00 PM

Carbon tetrachloride

ND

56

µg/Kg-dry

50.1

5/1/2006 7:45:00 PM

Chlorobenzene

ND

56

µg/Kg-dry

50.1

5/1/2006 7:45:00 PM

Chloroethane

ND

280

µg/Kg-dry

50.1

5/1/2006 7:45:00 PM

Chloroform

ND

56

µg/Kg-dry

50.1

5/1/2006 7:45:00 PM

Chloromethane

ND

56

µg/Kg-dry

50.1

5/1/2006 7:45:00 PM

cis-1,2-Dichloroethene

ND

56

µg/Kg-dry

50.1

5/1/2006 7:45:00 PM

cis-1,3-Dichloropropene

ND

56

µg/Kg-dry

50.1

5/1/2006 7:45:00 PM

Dibromochloromethane

ND

56

µg/Kg-dry

50.1

5/1/2006 7:45:00 PM

Dibromomethane

ND

56

µg/Kg-dry

50.1

5/1/2006 7:45:00 PM

Dichlorodifluoromethane

ND

56

µg/Kg-dry

50.1

5/1/2006 7:45:00 PM

Dichloromethane

ND

280

µg/Kg-dry

50.1

5/1/2006 7:45:00 PM

Diethyl ether

ND

280

µg/Kg-dry

50.1

5/1/2006 7:45:00 PM

Ethyl methacrylate

ND

56

µg/Kg-dry

50.1

5/1/2006 7:45:00 PM

Ethylbenzene

ND

56

µg/Kg-dry

50.1

5/1/2006 7:45:00 PM

Ethylene dibromide

ND

56

µg/Kg-dry

50.1

5/1/2006 7:45:00 PM

Hexachlorobutadiene

ND

280

µg/Kg-dry

50.1

5/1/2006 7:45:00 PM

Hexachloroethane

ND

56

µg/Kg-dry

50.1

5/1/2006 7:45:00 PM

Isopropyl ether

ND

280

µg/Kg-dry

50.1

5/1/2006 7:45:00 PM

Isopropylbenzene

ND

56

µg/Kg-dry

50.1

5/1/2006 7:45:00 PM

m,p-Xylene

ND

110

µg/Kg-dry

50.1

5/1/2006 7:45:00 PM

Methyl ethyl ketone

ND

280

µg/Kg-dry

50.1

5/1/2006 7:45:00 PM

Methyl Iodide

ND

280

µg/Kg-dry

50.1

5/1/2006 7:45:00 PM

Methyl isobutyl ketone

ND

560

µg/Kg-dry

50.1

5/1/2006 7:45:00 PM

Methyl tert-butyl ether

ND

280

µg/Kg-dry

50.1

5/1/2006 7:45:00 PM

Naphthalene

ND

280

µg/Kg-dry

50.1

5/1/2006 7:45:00 PM

n-Butylbenzene

ND

56

µg/Kg-dry

50.1

5/1/2006 7:45:00 PM

n-Propylbenzene

ND

56

µg/Kg-dry

50.1

5/1/2006 7:45:00 PM

Qualifiers:

*

Value exceeds Maximum Contaminant Level

B

Analyte detected in the associated Method Blank

E

Value above quantitation range

H

Holding times for preparation or analysis exceeded

M

Manual Integration used to determine area response

RL

Reporting Detection Limit

ND
S

Not Detected at the Reporting Limit
Spike Recovery outside accepted recovery limits

Page 4 of 66

31628 Glendale St.

Analytical Report

Livonia, Michigan 48150
TEL: 734.422.8000
FAX: 734.422.5342
Website: www.rtilab.com

(consolidated)

WO#:

0604884

Date Reported:

5/5/2006

Collection Date: 4/27/2006 11:35:00 AM

CLIENT:

PM Environmental, Inc.

Project:

7876 Van Dyke - 22-692A

Lab ID:

0604884-001

Matrix: SOIL

Client Sample ID SB-1 1-2'
Analyses

Result

RL Qual Units

Volatile Organic Compounds

DF

Date Analyzed
Analyst: JW

SW8260B

o-Xylene

ND

56

µg/Kg-dry

50.1

5/1/2006 7:45:00 PM

p-Isopropyltoluene

ND

56

µg/Kg-dry

50.1

5/1/2006 7:45:00 PM

sec-Butylbenzene

ND

56

µg/Kg-dry

50.1

5/1/2006 7:45:00 PM

Styrene

ND

56

µg/Kg-dry

50.1

5/1/2006 7:45:00 PM

t-Butyl alcohol

ND

2,300

µg/Kg-dry

50.1

5/1/2006 7:45:00 PM

tert-Amyl Methyl Ether

ND

230

µg/Kg-dry

50.1

5/1/2006 7:45:00 PM

tert-Butyl Ethyl Ether

ND

280

µg/Kg-dry

50.1

5/1/2006 7:45:00 PM

tert-Butylbenzene

ND

56

µg/Kg-dry

50.1

5/1/2006 7:45:00 PM

Tetrachloroethene

ND

56

µg/Kg-dry

50.1

5/1/2006 7:45:00 PM

69

56

µg/Kg-dry

50.1

5/1/2006 7:45:00 PM

trans-1,2-Dichloroethene

ND

56

µg/Kg-dry

50.1

5/1/2006 7:45:00 PM

trans-1,3-Dichloropropene

ND

56

µg/Kg-dry

50.1

5/1/2006 7:45:00 PM

trans-1,4-Dichloro-2-butene

ND

56

µg/Kg-dry

50.1

5/1/2006 7:45:00 PM

Trichloroethene

ND

56

µg/Kg-dry

50.1

5/1/2006 7:45:00 PM

Trichlorofluoromethane

ND

56

µg/Kg-dry

50.1

5/1/2006 7:45:00 PM

Vinyl chloride

ND

45

µg/Kg-dry

50.1

5/1/2006 7:45:00 PM

Xylenes, Total

ND

170

µg/Kg-dry

50.1

5/1/2006 7:45:00 PM

Surr: 4-Bromofluorobenzene

112

70-130

%REC

50.1

5/1/2006 7:45:00 PM

Surr: Dibromofluoromethane

108

70-130

%REC

50.1

5/1/2006 7:45:00 PM

Surr: Toluene-d8

118

70-130

%REC

50.1

5/1/2006 7:45:00 PM

11

1.0

1

5/1/2006

Toluene

PERCENT MOISTURE
Percent Moisture

Qualifiers:

Analyst: MT3

D2216 wt% *

Value exceeds Maximum Contaminant Level

B

Analyte detected in the associated Method Blank

E

Value above quantitation range

H

Holding times for preparation or analysis exceeded

M

Manual Integration used to determine area response

RL

Reporting Detection Limit

ND
S

Not Detected at the Reporting Limit
Spike Recovery outside accepted recovery limits

Page 5 of 66

31628 Glendale St.

Analytical Report

Livonia, Michigan 48150
TEL: 734.422.8000
FAX: 734.422.5342
Website: www.rtilab.com

(consolidated)

WO#:

0604884

Date Reported:

5/5/2006

Collection Date: 4/27/2006 11:00:00 AM

CLIENT:

PM Environmental, Inc.

Project:

7876 Van Dyke - 22-692A

Lab ID:

0604884-002

Matrix: SOIL

Client Sample ID SB-2 2-3'
Analyses

Result

RL Qual Units

DF

Polychlorinated Biphenyls

Date Analyzed
Analyst: MB

SW8082

Aroclor 1016

ND

38

µg/Kg-dry

1

5/2/2006 8:51:03 PM

Aroclor 1221

ND

38

µg/Kg-dry

1

5/2/2006 8:51:03 PM

Aroclor 1232

ND

38

µg/Kg-dry

1

5/2/2006 8:51:03 PM

Aroclor 1242

ND

38

µg/Kg-dry

1

5/2/2006 8:51:03 PM

Aroclor 1248

ND

38

µg/Kg-dry

1

5/2/2006 8:51:03 PM

Aroclor 1254

ND

38

µg/Kg-dry

1

5/2/2006 8:51:03 PM

Aroclor 1260

ND

38

µg/Kg-dry

1

5/2/2006 8:51:03 PM

Surr: Decachlorobiphenyl

84.2

70-130

%REC

1

5/2/2006 8:51:03 PM

Surr: Tetrachloro-m-xylene

71.9

70-130

%REC

1

5/2/2006 8:51:03 PM

530

460

µg/Kg-dry

20

5/1/2006 1:46:53 PM

Chromium

14,000

2,300

µg/Kg-dry

20

5/1/2006 1:46:53 PM

Lead

21,000

2,300

µg/Kg-dry

20

5/1/2006 1:46:53 PM

Metals, ICP/MS

Analyst: AB2

SW6020A

Cadmium

Polynuclear Aromatic Hydrocarbons
Semi-Volatile Organic Compounds

Analyst: JG3

SW8270C

2-Methylnaphthalene

ND

380

µg/Kg-dry

1

5/2/2006 5:26:00 PM

Acenaphthene

ND

380

µg/Kg-dry

1

5/2/2006 5:26:00 PM

Acenaphthylene

ND

380

µg/Kg-dry

1

5/2/2006 5:26:00 PM

Anthracene

ND

380

µg/Kg-dry

1

5/2/2006 5:26:00 PM

Benz(a)anthracene

ND

380

µg/Kg-dry

1

5/2/2006 5:26:00 PM

Benzo(a)pyrene

ND

380

µg/Kg-dry

1

5/2/2006 5:26:00 PM

Benzo(b)fluoranthene

ND

380

µg/Kg-dry

1

5/2/2006 5:26:00 PM

Benzo(g,h,i)perylene

ND

380

µg/Kg-dry

1

5/2/2006 5:26:00 PM

Benzo(k)fluoranthene

ND

380

µg/Kg-dry

1

5/2/2006 5:26:00 PM

Chrysene

ND

380

µg/Kg-dry

1

5/2/2006 5:26:00 PM

Dibenz(a,h)anthracene

ND

380

µg/Kg-dry

1

5/2/2006 5:26:00 PM

Fluoranthene

ND

380

µg/Kg-dry

1

5/2/2006 5:26:00 PM

Fluorene

ND

380

µg/Kg-dry

1

5/2/2006 5:26:00 PM

Indeno(1,2,3-cd)pyrene

ND

380

µg/Kg-dry

1

5/2/2006 5:26:00 PM

Naphthalene

ND

380

µg/Kg-dry

1

5/2/2006 5:26:00 PM

Phenanthrene

ND

380

µg/Kg-dry

1

5/2/2006 5:26:00 PM

Pyrene

ND

380

µg/Kg-dry

1

5/2/2006 5:26:00 PM

Surr: 2,4,6-Tribromophenol

89.8

25-93.9

%REC

1

5/2/2006 5:26:00 PM

Surr: 2-Fluorobiphenyl

91.8

26-105

%REC

1

5/2/2006 5:26:00 PM

Qualifiers:

*

Value exceeds Maximum Contaminant Level

B

Analyte detected in the associated Method Blank

E

Value above quantitation range

H

Holding times for preparation or analysis exceeded

M

Manual Integration used to determine area response

RL

Reporting Detection Limit

ND
S

Not Detected at the Reporting Limit
Spike Recovery outside accepted recovery limits

Page 6 of 66

31628 Glendale St.

Analytical Report

Livonia, Michigan 48150
TEL: 734.422.8000
FAX: 734.422.5342
Website: www.rtilab.com

(consolidated)

WO#:

0604884

Date Reported:

5/5/2006

Collection Date: 4/27/2006 11:00:00 AM

CLIENT:

PM Environmental, Inc.

Project:

7876 Van Dyke - 22-692A

Lab ID:

0604884-002

Matrix: SOIL

Client Sample ID SB-2 2-3'
Analyses

Result

RL Qual Units

Polynuclear Aromatic Hydrocarbons
Semi-Volatile Organic Compounds

DF

Date Analyzed
Analyst: JG3

SW8270C

Surr: 2-Fluorophenol

100

25-120

%REC

1

5/2/2006 5:26:00 PM

Surr: Nitrobenzene-d5

92.0

30.1-104

%REC

1

5/2/2006 5:26:00 PM

Surr: Phenol-d5

98.8

25-118

%REC

1

5/2/2006 5:26:00 PM

Surr: Terphenyl-d14

96.7

27.1-115

%REC

1

5/2/2006 5:26:00 PM

1,1,1,2-Tetrachloroethane

ND

61

µg/Kg-dry

53.3

5/1/2006 9:26:00 PM

1,1,1-Trichloroethane

ND

61

µg/Kg-dry

53.3

5/1/2006 9:26:00 PM

1,1,2,2-Tetrachloroethane

ND

61

µg/Kg-dry

53.3

5/1/2006 9:26:00 PM

1,1,2-Trichloro-1,2,2-trifluoroethane

ND

61

µg/Kg-dry

53.3

5/1/2006 9:26:00 PM

1,1,2-Trichloroethane

ND

61

µg/Kg-dry

53.3

5/1/2006 9:26:00 PM

1,1-Dichloroethane

ND

61

µg/Kg-dry

53.3

5/1/2006 9:26:00 PM

1,1-Dichloroethene

ND

61

µg/Kg-dry

53.3

5/1/2006 9:26:00 PM

1,1-Dichloropropene

ND

61

µg/Kg-dry

53.3

5/1/2006 9:26:00 PM

1,2,3-Trichlorobenzene

ND

61

µg/Kg-dry

53.3

5/1/2006 9:26:00 PM

1,2,3-Trichloropropane

ND

61

µg/Kg-dry

53.3

5/1/2006 9:26:00 PM

1,2,3-Trimethylbenzene

ND

61

µg/Kg-dry

53.3

5/1/2006 9:26:00 PM

1,2,4-Trichlorobenzene

ND

310

µg/Kg-dry

53.3

5/1/2006 9:26:00 PM

1,2,4-Trimethylbenzene

ND

61

µg/Kg-dry

53.3

5/1/2006 9:26:00 PM

1,2-Dibromo-3-chloropropane

ND

61

µg/Kg-dry

53.3

5/1/2006 9:26:00 PM

1,2-Dichlorobenzene

ND

61

µg/Kg-dry

53.3

5/1/2006 9:26:00 PM

1,2-Dichloroethane

ND

61

µg/Kg-dry

53.3

5/1/2006 9:26:00 PM

1,2-Dichloropropane

ND

61

µg/Kg-dry

53.3

5/1/2006 9:26:00 PM

1,3,5-Trimethylbenzene

ND

61

µg/Kg-dry

53.3

5/1/2006 9:26:00 PM

1,3-Dichlorobenzene

ND

61

µg/Kg-dry

53.3

5/1/2006 9:26:00 PM

1,3-Dichloropropane

ND

61

µg/Kg-dry

53.3

5/1/2006 9:26:00 PM

1,4-Dichlorobenzene

ND

61

µg/Kg-dry

53.3

5/1/2006 9:26:00 PM

2,2-Dichloropropane

ND

61

µg/Kg-dry

53.3

5/1/2006 9:26:00 PM

2-Chloroethyl vinyl ether

ND

610

µg/Kg-dry

53.3

5/1/2006 9:26:00 PM

2-Chlorotoluene

ND

61

µg/Kg-dry

53.3

5/1/2006 9:26:00 PM

2-Hexanone

ND

3,100

µg/Kg-dry

53.3

5/1/2006 9:26:00 PM

2-Methylnaphthalene

ND

310

µg/Kg-dry

53.3

5/1/2006 9:26:00 PM

2-Nitropropane

ND

250

µg/Kg-dry

53.3

5/1/2006 9:26:00 PM

4-Chlorotoluene

ND

61

µg/Kg-dry

53.3

5/1/2006 9:26:00 PM

Acetone

ND

3,100

µg/Kg-dry

53.3

5/1/2006 9:26:00 PM

Volatile Organic Compounds

Qualifiers:

Analyst: JW

SW8260B

*

Value exceeds Maximum Contaminant Level

B

Analyte detected in the associated Method Blank

E

Value above quantitation range

H

Holding times for preparation or analysis exceeded

M

Manual Integration used to determine area response

RL

Reporting Detection Limit

ND
S

Not Detected at the Reporting Limit
Spike Recovery outside accepted recovery limits

Page 7 of 66

31628 Glendale St.

Analytical Report

Livonia, Michigan 48150
TEL: 734.422.8000
FAX: 734.422.5342
Website: www.rtilab.com

(consolidated)

WO#:

0604884

Date Reported:

5/5/2006

Collection Date: 4/27/2006 11:00:00 AM

CLIENT:

PM Environmental, Inc.

Project:

7876 Van Dyke - 22-692A

Lab ID:

0604884-002

Matrix: SOIL

Client Sample ID SB-2 2-3'
Analyses

Result

RL Qual Units

Volatile Organic Compounds

DF

Date Analyzed
Analyst: JW

SW8260B

Acrylonitrile

ND

310

µg/Kg-dry

53.3

5/1/2006 9:26:00 PM

Benzene

ND

61

µg/Kg-dry

53.3

5/1/2006 9:26:00 PM

Bromobenzene

ND

61

µg/Kg-dry

53.3

5/1/2006 9:26:00 PM

Bromochloromethane

ND

61

µg/Kg-dry

53.3

5/1/2006 9:26:00 PM

Bromodichloromethane

ND

61

µg/Kg-dry

53.3

5/1/2006 9:26:00 PM

Bromoform

ND

61

µg/Kg-dry

53.3

5/1/2006 9:26:00 PM

Bromomethane

ND

310

µg/Kg-dry

53.3

5/1/2006 9:26:00 PM

Carbon disulfide

ND

310

µg/Kg-dry

53.3

5/1/2006 9:26:00 PM

Carbon tetrachloride

ND

61

µg/Kg-dry

53.3

5/1/2006 9:26:00 PM

Chlorobenzene

ND

61

µg/Kg-dry

53.3

5/1/2006 9:26:00 PM

Chloroethane

ND

310

µg/Kg-dry

53.3

5/1/2006 9:26:00 PM

Chloroform

ND

61

µg/Kg-dry

53.3

5/1/2006 9:26:00 PM

Chloromethane

ND

61

µg/Kg-dry

53.3

5/1/2006 9:26:00 PM

cis-1,2-Dichloroethene

ND

61

µg/Kg-dry

53.3

5/1/2006 9:26:00 PM

cis-1,3-Dichloropropene

ND

61

µg/Kg-dry

53.3

5/1/2006 9:26:00 PM

Dibromochloromethane

ND

61

µg/Kg-dry

53.3

5/1/2006 9:26:00 PM

Dibromomethane

ND

61

µg/Kg-dry

53.3

5/1/2006 9:26:00 PM

Dichlorodifluoromethane

ND

61

µg/Kg-dry

53.3

5/1/2006 9:26:00 PM

Dichloromethane

ND

310

µg/Kg-dry

53.3

5/1/2006 9:26:00 PM

Diethyl ether

ND

310

µg/Kg-dry

53.3

5/1/2006 9:26:00 PM

Ethyl methacrylate

ND

61

µg/Kg-dry

53.3

5/1/2006 9:26:00 PM

Ethylbenzene

ND

61

µg/Kg-dry

53.3

5/1/2006 9:26:00 PM

Ethylene dibromide

ND

61

µg/Kg-dry

53.3

5/1/2006 9:26:00 PM

Hexachlorobutadiene

ND

310

µg/Kg-dry

53.3

5/1/2006 9:26:00 PM

Hexachloroethane

ND

61

µg/Kg-dry

53.3

5/1/2006 9:26:00 PM

Isopropyl ether

ND

310

µg/Kg-dry

53.3

5/1/2006 9:26:00 PM

Isopropylbenzene

ND

61

µg/Kg-dry

53.3

5/1/2006 9:26:00 PM

m,p-Xylene

ND

120

µg/Kg-dry

53.3

5/1/2006 9:26:00 PM

Methyl ethyl ketone

ND

310

µg/Kg-dry

53.3

5/1/2006 9:26:00 PM

Methyl Iodide

ND

310

µg/Kg-dry

53.3

5/1/2006 9:26:00 PM

Methyl isobutyl ketone

ND

610

µg/Kg-dry

53.3

5/1/2006 9:26:00 PM

Methyl tert-butyl ether

ND

310

µg/Kg-dry

53.3

5/1/2006 9:26:00 PM

Naphthalene

ND

310

µg/Kg-dry

53.3

5/1/2006 9:26:00 PM

n-Butylbenzene

ND

61

µg/Kg-dry

53.3

5/1/2006 9:26:00 PM

n-Propylbenzene

ND

61

µg/Kg-dry

53.3

5/1/2006 9:26:00 PM

Qualifiers:

*

Value exceeds Maximum Contaminant Level

B

Analyte detected in the associated Method Blank

E

Value above quantitation range

H

Holding times for preparation or analysis exceeded

M

Manual Integration used to determine area response

RL

Reporting Detection Limit

ND
S

Not Detected at the Reporting Limit
Spike Recovery outside accepted recovery limits

Page 8 of 66

31628 Glendale St.

Analytical Report

Livonia, Michigan 48150
TEL: 734.422.8000
FAX: 734.422.5342
Website: www.rtilab.com

(consolidated)

WO#:

0604884

Date Reported:

5/5/2006

Collection Date: 4/27/2006 11:00:00 AM

CLIENT:

PM Environmental, Inc.

Project:

7876 Van Dyke - 22-692A

Lab ID:

0604884-002

Matrix: SOIL

Client Sample ID SB-2 2-3'
Analyses

Result

RL Qual Units

Volatile Organic Compounds

DF

Date Analyzed
Analyst: JW

SW8260B

o-Xylene

ND

61

µg/Kg-dry

53.3

5/1/2006 9:26:00 PM

p-Isopropyltoluene

ND

61

µg/Kg-dry

53.3

5/1/2006 9:26:00 PM

sec-Butylbenzene

ND

61

µg/Kg-dry

53.3

5/1/2006 9:26:00 PM

Styrene

ND

61

µg/Kg-dry

53.3

5/1/2006 9:26:00 PM

t-Butyl alcohol

ND

2,500

µg/Kg-dry

53.3

5/1/2006 9:26:00 PM

tert-Amyl Methyl Ether

ND

250

µg/Kg-dry

53.3

5/1/2006 9:26:00 PM

tert-Butyl Ethyl Ether

ND

310

µg/Kg-dry

53.3

5/1/2006 9:26:00 PM

tert-Butylbenzene

ND

61

µg/Kg-dry

53.3

5/1/2006 9:26:00 PM

Tetrachloroethene

ND

61

µg/Kg-dry

53.3

5/1/2006 9:26:00 PM

Toluene

ND

61

µg/Kg-dry

53.3

5/1/2006 9:26:00 PM

trans-1,2-Dichloroethene

ND

61

µg/Kg-dry

53.3

5/1/2006 9:26:00 PM

trans-1,3-Dichloropropene

ND

61

µg/Kg-dry

53.3

5/1/2006 9:26:00 PM

trans-1,4-Dichloro-2-butene

ND

61

µg/Kg-dry

53.3

5/1/2006 9:26:00 PM

Trichloroethene

ND

61

µg/Kg-dry

53.3

5/1/2006 9:26:00 PM

Trichlorofluoromethane

ND

61

µg/Kg-dry

53.3

5/1/2006 9:26:00 PM

Vinyl chloride

ND

49

µg/Kg-dry

53.3

5/1/2006 9:26:00 PM

Xylenes, Total

ND

180

µg/Kg-dry

53.3

5/1/2006 9:26:00 PM

Surr: 4-Bromofluorobenzene

114

70-130

%REC

53.3

5/1/2006 9:26:00 PM

Surr: Dibromofluoromethane

107

70-130

%REC

53.3

5/1/2006 9:26:00 PM

Surr: Toluene-d8

117

70-130

%REC

53.3

5/1/2006 9:26:00 PM

13

1.0

1

5/1/2006

PERCENT MOISTURE
Percent Moisture

Qualifiers:

Analyst: MT3

D2216 wt% *

Value exceeds Maximum Contaminant Level

B

Analyte detected in the associated Method Blank

E

Value above quantitation range

H

Holding times for preparation or analysis exceeded

M

Manual Integration used to determine area response

RL

Reporting Detection Limit

ND
S

Not Detected at the Reporting Limit
Spike Recovery outside accepted recovery limits

Page 9 of 66

31628 Glendale St.

Analytical Report

Livonia, Michigan 48150
TEL: 734.422.8000
FAX: 734.422.5342
Website: www.rtilab.com

(consolidated)

WO#:

0604884

Date Reported:

5/5/2006

Collection Date: 4/27/2006 11:20:00 AM

CLIENT:

PM Environmental, Inc.

Project:

7876 Van Dyke - 22-692A

Lab ID:

0604884-003

Matrix: SOIL

Client Sample ID SB-3 2-3'
Analyses

Result

RL Qual Units

DF

Polychlorinated Biphenyls

Date Analyzed
Analyst: MB

SW8082

Aroclor 1016

ND

39

µg/Kg-dry

1

5/2/2006 9:30:37 PM

Aroclor 1221

ND

39

µg/Kg-dry

1

5/2/2006 9:30:37 PM

Aroclor 1232

ND

39

µg/Kg-dry

1

5/2/2006 9:30:37 PM

Aroclor 1242

ND

39

µg/Kg-dry

1

5/2/2006 9:30:37 PM

Aroclor 1248

ND

39

µg/Kg-dry

1

5/2/2006 9:30:37 PM

Aroclor 1254

ND

39

µg/Kg-dry

1

5/2/2006 9:30:37 PM

Aroclor 1260

ND

39

µg/Kg-dry

1

5/2/2006 9:30:37 PM

Surr: Decachlorobiphenyl

86.6

70-130

%REC

1

5/2/2006 9:30:37 PM

Surr: Tetrachloro-m-xylene

72.7

70-130

%REC

1

5/2/2006 9:30:37 PM

670

450

µg/Kg-dry

20

5/1/2006 1:49:10 PM

Chromium

14,000

2,300

µg/Kg-dry

20

5/1/2006 1:49:10 PM

Lead

15,000

2,300

µg/Kg-dry

20

5/1/2006 1:49:10 PM

Metals, ICP/MS

Analyst: AB2

SW6020A

Cadmium

Polynuclear Aromatic Hydrocarbons
Semi-Volatile Organic Compounds

Analyst: JG3

SW8270C

2-Methylnaphthalene

ND

390

µg/Kg-dry

1

5/2/2006 6:02:00 PM

Acenaphthene

ND

390

µg/Kg-dry

1

5/2/2006 6:02:00 PM

Acenaphthylene

ND

390

µg/Kg-dry

1

5/2/2006 6:02:00 PM

Anthracene

ND

390

µg/Kg-dry

1

5/2/2006 6:02:00 PM

Benz(a)anthracene

ND

390

µg/Kg-dry

1

5/2/2006 6:02:00 PM

Benzo(a)pyrene

ND

390

µg/Kg-dry

1

5/2/2006 6:02:00 PM

Benzo(b)fluoranthene

ND

390

µg/Kg-dry

1

5/2/2006 6:02:00 PM

Benzo(g,h,i)perylene

ND

390

µg/Kg-dry

1

5/2/2006 6:02:00 PM

Benzo(k)fluoranthene

ND

390

µg/Kg-dry

1

5/2/2006 6:02:00 PM

Chrysene

ND

390

µg/Kg-dry

1

5/2/2006 6:02:00 PM

Dibenz(a,h)anthracene

ND

390

µg/Kg-dry

1

5/2/2006 6:02:00 PM

Fluoranthene

ND

390

µg/Kg-dry

1

5/2/2006 6:02:00 PM

Fluorene

ND

390

µg/Kg-dry

1

5/2/2006 6:02:00 PM

Indeno(1,2,3-cd)pyrene

ND

390

µg/Kg-dry

1

5/2/2006 6:02:00 PM

Naphthalene

ND

390

µg/Kg-dry

1

5/2/2006 6:02:00 PM

Phenanthrene

ND

390

µg/Kg-dry

1

5/2/2006 6:02:00 PM

Pyrene

ND

390

µg/Kg-dry

1

5/2/2006 6:02:00 PM

Surr: 2,4,6-Tribromophenol

78.7

25-93.9

%REC

1

5/2/2006 6:02:00 PM

Surr: 2-Fluorobiphenyl

85.9

26-105

%REC

1

5/2/2006 6:02:00 PM

Qualifiers:

*

Value exceeds Maximum Contaminant Level

B

Analyte detected in the associated Method Blank

E

Value above quantitation range

H

Holding times for preparation or analysis exceeded

M

Manual Integration used to determine area response

RL

Reporting Detection Limit

ND
S

Not Detected at the Reporting Limit
Spike Recovery outside accepted recovery limits

Page 10 of 66

31628 Glendale St.

Analytical Report

Livonia, Michigan 48150
TEL: 734.422.8000
FAX: 734.422.5342
Website: www.rtilab.com

(consolidated)

WO#:

0604884

Date Reported:

5/5/2006

Collection Date: 4/27/2006 11:20:00 AM

CLIENT:

PM Environmental, Inc.

Project:

7876 Van Dyke - 22-692A

Lab ID:

0604884-003

Matrix: SOIL

Client Sample ID SB-3 2-3'
Analyses

Result

RL Qual Units

Polynuclear Aromatic Hydrocarbons
Semi-Volatile Organic Compounds

DF

Date Analyzed
Analyst: JG3

SW8270C

Surr: 2-Fluorophenol

96.4

25-120

%REC

1

5/2/2006 6:02:00 PM

Surr: Nitrobenzene-d5

84.0

30.1-104

%REC

1

5/2/2006 6:02:00 PM

Surr: Phenol-d5

96.0

25-118

%REC

1

5/2/2006 6:02:00 PM

Surr: Terphenyl-d14

97.0

27.1-115

%REC

1

5/2/2006 6:02:00 PM

1,1,1,2-Tetrachloroethane

ND

59

µg/Kg-dry

50.9

5/1/2006 10:00:00 PM

1,1,1-Trichloroethane

ND

59

µg/Kg-dry

50.9

5/1/2006 10:00:00 PM

1,1,2,2-Tetrachloroethane

ND

59

µg/Kg-dry

50.9

5/1/2006 10:00:00 PM

1,1,2-Trichloro-1,2,2-trifluoroethane

ND

59

µg/Kg-dry

50.9

5/1/2006 10:00:00 PM

1,1,2-Trichloroethane

ND

59

µg/Kg-dry

50.9

5/1/2006 10:00:00 PM

1,1-Dichloroethane

ND

59

µg/Kg-dry

50.9

5/1/2006 10:00:00 PM

1,1-Dichloroethene

ND

59

µg/Kg-dry

50.9

5/1/2006 10:00:00 PM

1,1-Dichloropropene

ND

59

µg/Kg-dry

50.9

5/1/2006 10:00:00 PM

1,2,3-Trichlorobenzene

ND

59

µg/Kg-dry

50.9

5/1/2006 10:00:00 PM

1,2,3-Trichloropropane

ND

59

µg/Kg-dry

50.9

5/1/2006 10:00:00 PM

1,2,3-Trimethylbenzene

ND

59

µg/Kg-dry

50.9

5/1/2006 10:00:00 PM

1,2,4-Trichlorobenzene

ND

300

µg/Kg-dry

50.9

5/1/2006 10:00:00 PM

1,2,4-Trimethylbenzene

ND

59

µg/Kg-dry

50.9

5/1/2006 10:00:00 PM

1,2-Dibromo-3-chloropropane

ND

59

µg/Kg-dry

50.9

5/1/2006 10:00:00 PM

1,2-Dichlorobenzene

ND

59

µg/Kg-dry

50.9

5/1/2006 10:00:00 PM

1,2-Dichloroethane

ND

59

µg/Kg-dry

50.9

5/1/2006 10:00:00 PM

1,2-Dichloropropane

ND

59

µg/Kg-dry

50.9

5/1/2006 10:00:00 PM

1,3,5-Trimethylbenzene

ND

59

µg/Kg-dry

50.9

5/1/2006 10:00:00 PM

1,3-Dichlorobenzene

ND

59

µg/Kg-dry

50.9

5/1/2006 10:00:00 PM

1,3-Dichloropropane

ND

59

µg/Kg-dry

50.9

5/1/2006 10:00:00 PM

1,4-Dichlorobenzene

ND

59

µg/Kg-dry

50.9

5/1/2006 10:00:00 PM

2,2-Dichloropropane

ND

59

µg/Kg-dry

50.9

5/1/2006 10:00:00 PM

2-Chloroethyl vinyl ether

ND

590

µg/Kg-dry

50.9

5/1/2006 10:00:00 PM

2-Chlorotoluene

ND

59

µg/Kg-dry

50.9

5/1/2006 10:00:00 PM

2-Hexanone

ND

3,000

µg/Kg-dry

50.9

5/1/2006 10:00:00 PM

2-Methylnaphthalene

ND

300

µg/Kg-dry

50.9

5/1/2006 10:00:00 PM

2-Nitropropane

ND

240

µg/Kg-dry

50.9

5/1/2006 10:00:00 PM

4-Chlorotoluene

ND

59

µg/Kg-dry

50.9

5/1/2006 10:00:00 PM

Acetone

ND

3,000

µg/Kg-dry

50.9

5/1/2006 10:00:00 PM

Volatile Organic Compounds

Qualifiers:

Analyst: JW

SW8260B

*

Value exceeds Maximum Contaminant Level

B

Analyte detected in the associated Method Blank

E

Value above quantitation range

H

Holding times for preparation or analysis exceeded

M

Manual Integration used to determine area response

RL

Reporting Detection Limit

ND
S

Not Detected at the Reporting Limit
Spike Recovery outside accepted recovery limits

Page 11 of 66

31628 Glendale St.

Analytical Report

Livonia, Michigan 48150
TEL: 734.422.8000
FAX: 734.422.5342
Website: www.rtilab.com

(consolidated)

WO#:

0604884

Date Reported:

5/5/2006

Collection Date: 4/27/2006 11:20:00 AM

CLIENT:

PM Environmental, Inc.

Project:

7876 Van Dyke - 22-692A

Lab ID:

0604884-003

Matrix: SOIL

Client Sample ID SB-3 2-3'
Analyses

Result

RL Qual Units

Volatile Organic Compounds

DF

Date Analyzed
Analyst: JW

SW8260B

Acrylonitrile

ND

300

µg/Kg-dry

50.9

5/1/2006 10:00:00 PM

Benzene

ND

59

µg/Kg-dry

50.9

5/1/2006 10:00:00 PM

Bromobenzene

ND

59

µg/Kg-dry

50.9

5/1/2006 10:00:00 PM

Bromochloromethane

ND

59

µg/Kg-dry

50.9

5/1/2006 10:00:00 PM

Bromodichloromethane

ND

59

µg/Kg-dry

50.9

5/1/2006 10:00:00 PM

Bromoform

ND

59

µg/Kg-dry

50.9

5/1/2006 10:00:00 PM

Bromomethane

ND

300

µg/Kg-dry

50.9

5/1/2006 10:00:00 PM

Carbon disulfide

ND

300

µg/Kg-dry

50.9

5/1/2006 10:00:00 PM

Carbon tetrachloride

ND

59

µg/Kg-dry

50.9

5/1/2006 10:00:00 PM

Chlorobenzene

ND

59

µg/Kg-dry

50.9

5/1/2006 10:00:00 PM

Chloroethane

ND

300

µg/Kg-dry

50.9

5/1/2006 10:00:00 PM

Chloroform

ND

59

µg/Kg-dry

50.9

5/1/2006 10:00:00 PM

Chloromethane

ND

59

µg/Kg-dry

50.9

5/1/2006 10:00:00 PM

cis-1,2-Dichloroethene

ND

59

µg/Kg-dry

50.9

5/1/2006 10:00:00 PM

cis-1,3-Dichloropropene

ND

59

µg/Kg-dry

50.9

5/1/2006 10:00:00 PM

Dibromochloromethane

ND

59

µg/Kg-dry

50.9

5/1/2006 10:00:00 PM

Dibromomethane

ND

59

µg/Kg-dry

50.9

5/1/2006 10:00:00 PM

Dichlorodifluoromethane

ND

59

µg/Kg-dry

50.9

5/1/2006 10:00:00 PM

Dichloromethane

ND

300

µg/Kg-dry

50.9

5/1/2006 10:00:00 PM

Diethyl ether

ND

300

µg/Kg-dry

50.9

5/1/2006 10:00:00 PM

Ethyl methacrylate

ND

59

µg/Kg-dry

50.9

5/1/2006 10:00:00 PM

Ethylbenzene

ND

59

µg/Kg-dry

50.9

5/1/2006 10:00:00 PM

Ethylene dibromide

ND

59

µg/Kg-dry

50.9

5/1/2006 10:00:00 PM

Hexachlorobutadiene

ND

300

µg/Kg-dry

50.9

5/1/2006 10:00:00 PM

Hexachloroethane

ND

59

µg/Kg-dry

50.9

5/1/2006 10:00:00 PM

Isopropyl ether

ND

300

µg/Kg-dry

50.9

5/1/2006 10:00:00 PM

Isopropylbenzene

ND

59

µg/Kg-dry

50.9

5/1/2006 10:00:00 PM

m,p-Xylene

ND

120

µg/Kg-dry

50.9

5/1/2006 10:00:00 PM

Methyl ethyl ketone

ND

300

µg/Kg-dry

50.9

5/1/2006 10:00:00 PM

Methyl Iodide

ND

300

µg/Kg-dry

50.9

5/1/2006 10:00:00 PM

Methyl isobutyl ketone

ND

590

µg/Kg-dry

50.9

5/1/2006 10:00:00 PM

Methyl tert-butyl ether

ND

300

µg/Kg-dry

50.9

5/1/2006 10:00:00 PM

Naphthalene

ND

300

µg/Kg-dry

50.9

5/1/2006 10:00:00 PM

n-Butylbenzene

ND

59

µg/Kg-dry

50.9

5/1/2006 10:00:00 PM

n-Propylbenzene

ND

59

µg/Kg-dry

50.9

5/1/2006 10:00:00 PM

Qualifiers:

*

Value exceeds Maximum Contaminant Level

B

Analyte detected in the associated Method Blank

E

Value above quantitation range

H

Holding times for preparation or analysis exceeded

M

Manual Integration used to determine area response

RL

Reporting Detection Limit

ND
S

Not Detected at the Reporting Limit
Spike Recovery outside accepted recovery limits

Page 12 of 66

31628 Glendale St.

Analytical Report

Livonia, Michigan 48150
TEL: 734.422.8000
FAX: 734.422.5342
Website: www.rtilab.com

(consolidated)

WO#:

0604884

Date Reported:

5/5/2006

Collection Date: 4/27/2006 11:20:00 AM

CLIENT:

PM Environmental, Inc.

Project:

7876 Van Dyke - 22-692A

Lab ID:

0604884-003

Matrix: SOIL

Client Sample ID SB-3 2-3'
Analyses

Result

RL Qual Units

Volatile Organic Compounds

DF

Date Analyzed
Analyst: JW

SW8260B

o-Xylene

ND

59

µg/Kg-dry

50.9

5/1/2006 10:00:00 PM

p-Isopropyltoluene

ND

59

µg/Kg-dry

50.9

5/1/2006 10:00:00 PM

sec-Butylbenzene

ND

59

µg/Kg-dry

50.9

5/1/2006 10:00:00 PM

Styrene

ND

59

µg/Kg-dry

50.9

5/1/2006 10:00:00 PM

t-Butyl alcohol

ND

2,400

µg/Kg-dry

50.9

5/1/2006 10:00:00 PM

tert-Amyl Methyl Ether

ND

240

µg/Kg-dry

50.9

5/1/2006 10:00:00 PM

tert-Butyl Ethyl Ether

ND

300

µg/Kg-dry

50.9

5/1/2006 10:00:00 PM

tert-Butylbenzene

ND

59

µg/Kg-dry

50.9

5/1/2006 10:00:00 PM

Tetrachloroethene

ND

59

µg/Kg-dry

50.9

5/1/2006 10:00:00 PM

Toluene

ND

59

µg/Kg-dry

50.9

5/1/2006 10:00:00 PM

trans-1,2-Dichloroethene

ND

59

µg/Kg-dry

50.9

5/1/2006 10:00:00 PM

trans-1,3-Dichloropropene

ND

59

µg/Kg-dry

50.9

5/1/2006 10:00:00 PM

trans-1,4-Dichloro-2-butene

ND

59

µg/Kg-dry

50.9

5/1/2006 10:00:00 PM

Trichloroethene

ND

59

µg/Kg-dry

50.9

5/1/2006 10:00:00 PM

Trichlorofluoromethane

ND

59

µg/Kg-dry

50.9

5/1/2006 10:00:00 PM

Vinyl chloride

ND

48

µg/Kg-dry

50.9

5/1/2006 10:00:00 PM

Xylenes, Total

ND

180

µg/Kg-dry

50.9

5/1/2006 10:00:00 PM

Surr: 4-Bromofluorobenzene

115

70-130

%REC

50.9

5/1/2006 10:00:00 PM

Surr: Dibromofluoromethane

111

70-130

%REC

50.9

5/1/2006 10:00:00 PM

Surr: Toluene-d8

116

70-130

%REC

50.9

5/1/2006 10:00:00 PM

14

1.0

1

5/1/2006

PERCENT MOISTURE
Percent Moisture

Qualifiers:

Analyst: MT3

D2216 wt% *

Value exceeds Maximum Contaminant Level

B

Analyte detected in the associated Method Blank

E

Value above quantitation range

H

Holding times for preparation or analysis exceeded

M

Manual Integration used to determine area response

RL

Reporting Detection Limit

ND
S

Not Detected at the Reporting Limit
Spike Recovery outside accepted recovery limits

Page 13 of 66

31628 Glendale St.

Analytical Report

Livonia, Michigan 48150
TEL: 734.422.8000
FAX: 734.422.5342
Website: www.rtilab.com

(consolidated)

WO#:

0604884

Date Reported:

5/5/2006

Collection Date: 4/27/2006 10:45:00 AM

CLIENT:

PM Environmental, Inc.

Project:

7876 Van Dyke - 22-692A

Lab ID:

0604884-004

Matrix: SOIL

Client Sample ID SB-4 2-3'
Analyses

Result

RL Qual Units

DF

Polychlorinated Biphenyls

Date Analyzed
Analyst: MB

SW8082

Aroclor 1016

ND

39

µg/Kg-dry

1

5/2/2006 10:10:17 PM

Aroclor 1221

ND

39

µg/Kg-dry

1

5/2/2006 10:10:17 PM

Aroclor 1232

ND

39

µg/Kg-dry

1

5/2/2006 10:10:17 PM

Aroclor 1242

ND

39

µg/Kg-dry

1

5/2/2006 10:10:17 PM

Aroclor 1248

ND

39

µg/Kg-dry

1

5/2/2006 10:10:17 PM

Aroclor 1254

ND

39

µg/Kg-dry

1

5/2/2006 10:10:17 PM

Aroclor 1260

ND

39

µg/Kg-dry

1

5/2/2006 10:10:17 PM

Surr: Decachlorobiphenyl

88.6

70-130

%REC

1

5/2/2006 10:10:17 PM

Surr: Tetrachloro-m-xylene

75.5

70-130

%REC

1

5/2/2006 10:10:17 PM

570

450

µg/Kg-dry

20

5/1/2006 1:51:28 PM

Chromium

14,000

2,300

µg/Kg-dry

20

5/1/2006 1:51:28 PM

Lead

13,000

2,300

µg/Kg-dry

20

5/1/2006 1:51:28 PM

Metals, ICP/MS

Analyst: AB2

SW6020A

Cadmium

Polynuclear Aromatic Hydrocarbons
Semi-Volatile Organic Compounds

Analyst: JG3

SW8270C

2-Methylnaphthalene

ND

390

µg/Kg-dry

1

5/2/2006 6:39:00 PM

Acenaphthene

ND

390

µg/Kg-dry

1

5/2/2006 6:39:00 PM

Acenaphthylene

ND

390

µg/Kg-dry

1

5/2/2006 6:39:00 PM

Anthracene

ND

390

µg/Kg-dry

1

5/2/2006 6:39:00 PM

Benz(a)anthracene

ND

390

µg/Kg-dry

1

5/2/2006 6:39:00 PM

Benzo(a)pyrene

ND

390

µg/Kg-dry

1

5/2/2006 6:39:00 PM

Benzo(b)fluoranthene

ND

390

µg/Kg-dry

1

5/2/2006 6:39:00 PM

Benzo(g,h,i)perylene

ND

390

µg/Kg-dry

1

5/2/2006 6:39:00 PM

Benzo(k)fluoranthene

ND

390

µg/Kg-dry

1

5/2/2006 6:39:00 PM

Chrysene

ND

390

µg/Kg-dry

1

5/2/2006 6:39:00 PM

Dibenz(a,h)anthracene

ND

390

µg/Kg-dry

1

5/2/2006 6:39:00 PM

Fluoranthene

ND

390

µg/Kg-dry

1

5/2/2006 6:39:00 PM

Fluorene

ND

390

µg/Kg-dry

1

5/2/2006 6:39:00 PM

Indeno(1,2,3-cd)pyrene

ND

390

µg/Kg-dry

1

5/2/2006 6:39:00 PM

Naphthalene

ND

390

µg/Kg-dry

1

5/2/2006 6:39:00 PM

Phenanthrene

ND

390

µg/Kg-dry

1

5/2/2006 6:39:00 PM

Pyrene

ND

390

µg/Kg-dry

1

5/2/2006 6:39:00 PM

Surr: 2,4,6-Tribromophenol

73.0

25-93.9

%REC

1

5/2/2006 6:39:00 PM

Surr: 2-Fluorobiphenyl

88.3

26-105

%REC

1

5/2/2006 6:39:00 PM

Qualifiers:

*

Value exceeds Maximum Contaminant Level

B

Analyte detected in the associated Method Blank

E

Value above quantitation range

H

Holding times for preparation or analysis exceeded

M

Manual Integration used to determine area response

RL

Reporting Detection Limit

ND
S

Not Detected at the Reporting Limit
Spike Recovery outside accepted recovery limits

Page 14 of 66

31628 Glendale St.

Analytical Report

Livonia, Michigan 48150
TEL: 734.422.8000
FAX: 734.422.5342
Website: www.rtilab.com

(consolidated)

WO#:

0604884

Date Reported:

5/5/2006

Collection Date: 4/27/2006 10:45:00 AM

CLIENT:

PM Environmental, Inc.

Project:

7876 Van Dyke - 22-692A

Lab ID:

0604884-004

Matrix: SOIL

Client Sample ID SB-4 2-3'
Analyses

Result

RL Qual Units

Polynuclear Aromatic Hydrocarbons
Semi-Volatile Organic Compounds

DF

Date Analyzed
Analyst: JG3

SW8270C

Surr: 2-Fluorophenol

96.2

25-120

%REC

1

5/2/2006 6:39:00 PM

Surr: Nitrobenzene-d5

88.2

30.1-104

%REC

1

5/2/2006 6:39:00 PM

Surr: Phenol-d5

94.2

25-118

%REC

1

5/2/2006 6:39:00 PM

Surr: Terphenyl-d14

95.0

27.1-115

%REC

1

5/2/2006 6:39:00 PM

1,1,1,2-Tetrachloroethane

ND

62

µg/Kg-dry

52.9

5/1/2006 10:34:00 PM

1,1,1-Trichloroethane

ND

62

µg/Kg-dry

52.9

5/1/2006 10:34:00 PM

1,1,2,2-Tetrachloroethane

ND

62

µg/Kg-dry

52.9

5/1/2006 10:34:00 PM

1,1,2-Trichloro-1,2,2-trifluoroethane

ND

62

µg/Kg-dry

52.9

5/1/2006 10:34:00 PM

1,1,2-Trichloroethane

ND

62

µg/Kg-dry

52.9

5/1/2006 10:34:00 PM

1,1-Dichloroethane

ND

62

µg/Kg-dry

52.9

5/1/2006 10:34:00 PM

1,1-Dichloroethene

ND

62

µg/Kg-dry

52.9

5/1/2006 10:34:00 PM

1,1-Dichloropropene

ND

62

µg/Kg-dry

52.9

5/1/2006 10:34:00 PM

1,2,3-Trichlorobenzene

ND

62

µg/Kg-dry

52.9

5/1/2006 10:34:00 PM

1,2,3-Trichloropropane

ND

62

µg/Kg-dry

52.9

5/1/2006 10:34:00 PM

1,2,3-Trimethylbenzene

ND

62

µg/Kg-dry

52.9

5/1/2006 10:34:00 PM

1,2,4-Trichlorobenzene

ND

310

µg/Kg-dry

52.9

5/1/2006 10:34:00 PM

1,2,4-Trimethylbenzene

ND

62

µg/Kg-dry

52.9

5/1/2006 10:34:00 PM

1,2-Dibromo-3-chloropropane

ND

62

µg/Kg-dry

52.9

5/1/2006 10:34:00 PM

1,2-Dichlorobenzene

ND

62

µg/Kg-dry

52.9

5/1/2006 10:34:00 PM

1,2-Dichloroethane

ND

62

µg/Kg-dry

52.9

5/1/2006 10:34:00 PM

1,2-Dichloropropane

ND

62

µg/Kg-dry

52.9

5/1/2006 10:34:00 PM

1,3,5-Trimethylbenzene

ND

62

µg/Kg-dry

52.9

5/1/2006 10:34:00 PM

1,3-Dichlorobenzene

ND

62

µg/Kg-dry

52.9

5/1/2006 10:34:00 PM

1,3-Dichloropropane

ND

62

µg/Kg-dry

52.9

5/1/2006 10:34:00 PM

1,4-Dichlorobenzene

ND

62

µg/Kg-dry

52.9

5/1/2006 10:34:00 PM

2,2-Dichloropropane

ND

62

µg/Kg-dry

52.9

5/1/2006 10:34:00 PM

2-Chloroethyl vinyl ether

ND

620

µg/Kg-dry

52.9

5/1/2006 10:34:00 PM

2-Chlorotoluene

ND

62

µg/Kg-dry

52.9

5/1/2006 10:34:00 PM

2-Hexanone

ND

3,100

µg/Kg-dry

52.9

5/1/2006 10:34:00 PM

2-Methylnaphthalene

ND

310

µg/Kg-dry

52.9

5/1/2006 10:34:00 PM

2-Nitropropane

ND

250

µg/Kg-dry

52.9

5/1/2006 10:34:00 PM

4-Chlorotoluene

ND

62

µg/Kg-dry

52.9

5/1/2006 10:34:00 PM

Acetone

ND

3,100

µg/Kg-dry

52.9

5/1/2006 10:34:00 PM

Volatile Organic Compounds

Qualifiers:

Analyst: JW

SW8260B

*

Value exceeds Maximum Contaminant Level

B

Analyte detected in the associated Method Blank

E

Value above quantitation range

H

Holding times for preparation or analysis exceeded

M

Manual Integration used to determine area response

RL

Reporting Detection Limit

ND
S

Not Detected at the Reporting Limit
Spike Recovery outside accepted recovery limits

Page 15 of 66

31628 Glendale St.

Analytical Report

Livonia, Michigan 48150
TEL: 734.422.8000
FAX: 734.422.5342
Website: www.rtilab.com

(consolidated)

WO#:

0604884

Date Reported:

5/5/2006

Collection Date: 4/27/2006 10:45:00 AM

CLIENT:

PM Environmental, Inc.

Project:

7876 Van Dyke - 22-692A

Lab ID:

0604884-004

Matrix: SOIL

Client Sample ID SB-4 2-3'
Analyses

Result

RL Qual Units

Volatile Organic Compounds

DF

Date Analyzed
Analyst: JW

SW8260B

Acrylonitrile

ND

310

µg/Kg-dry

52.9

5/1/2006 10:34:00 PM

Benzene

ND

62

µg/Kg-dry

52.9

5/1/2006 10:34:00 PM

Bromobenzene

ND

62

µg/Kg-dry

52.9

5/1/2006 10:34:00 PM

Bromochloromethane

ND

62

µg/Kg-dry

52.9

5/1/2006 10:34:00 PM

Bromodichloromethane

ND

62

µg/Kg-dry

52.9

5/1/2006 10:34:00 PM

Bromoform

ND

62

µg/Kg-dry

52.9

5/1/2006 10:34:00 PM

Bromomethane

ND

310

µg/Kg-dry

52.9

5/1/2006 10:34:00 PM

Carbon disulfide

ND

310

µg/Kg-dry

52.9

5/1/2006 10:34:00 PM

Carbon tetrachloride

ND

62

µg/Kg-dry

52.9

5/1/2006 10:34:00 PM

Chlorobenzene

ND

62

µg/Kg-dry

52.9

5/1/2006 10:34:00 PM

Chloroethane

ND

310

µg/Kg-dry

52.9

5/1/2006 10:34:00 PM

Chloroform

ND

62

µg/Kg-dry

52.9

5/1/2006 10:34:00 PM

Chloromethane

ND

62

µg/Kg-dry

52.9

5/1/2006 10:34:00 PM

cis-1,2-Dichloroethene

ND

62

µg/Kg-dry

52.9

5/1/2006 10:34:00 PM

cis-1,3-Dichloropropene

ND

62

µg/Kg-dry

52.9

5/1/2006 10:34:00 PM

Dibromochloromethane

ND

62

µg/Kg-dry

52.9

5/1/2006 10:34:00 PM

Dibromomethane

ND

62

µg/Kg-dry

52.9

5/1/2006 10:34:00 PM

Dichlorodifluoromethane

ND

62

µg/Kg-dry

52.9

5/1/2006 10:34:00 PM

Dichloromethane

ND

310

µg/Kg-dry

52.9

5/1/2006 10:34:00 PM

Diethyl ether

ND

310

µg/Kg-dry

52.9

5/1/2006 10:34:00 PM

Ethyl methacrylate

ND

62

µg/Kg-dry

52.9

5/1/2006 10:34:00 PM

Ethylbenzene

ND

62

µg/Kg-dry

52.9

5/1/2006 10:34:00 PM

Ethylene dibromide

ND

62

µg/Kg-dry

52.9

5/1/2006 10:34:00 PM

Hexachlorobutadiene

ND

310

µg/Kg-dry

52.9

5/1/2006 10:34:00 PM

Hexachloroethane

ND

62

µg/Kg-dry

52.9

5/1/2006 10:34:00 PM

Isopropyl ether

ND

310

µg/Kg-dry

52.9

5/1/2006 10:34:00 PM

Isopropylbenzene

ND

62

µg/Kg-dry

52.9

5/1/2006 10:34:00 PM

m,p-Xylene

ND

120

µg/Kg-dry

52.9

5/1/2006 10:34:00 PM

Methyl ethyl ketone

ND

310

µg/Kg-dry

52.9

5/1/2006 10:34:00 PM

Methyl Iodide

ND

310

µg/Kg-dry

52.9

5/1/2006 10:34:00 PM

Methyl isobutyl ketone

ND

620

µg/Kg-dry

52.9

5/1/2006 10:34:00 PM

Methyl tert-butyl ether

ND

310

µg/Kg-dry

52.9

5/1/2006 10:34:00 PM

Naphthalene

ND

310

µg/Kg-dry

52.9

5/1/2006 10:34:00 PM

n-Butylbenzene

ND

62

µg/Kg-dry

52.9

5/1/2006 10:34:00 PM

n-Propylbenzene

ND

62

µg/Kg-dry

52.9

5/1/2006 10:34:00 PM

Qualifiers:

*

Value exceeds Maximum Contaminant Level

B

Analyte detected in the associated Method Blank

E

Value above quantitation range

H

Holding times for preparation or analysis exceeded

M

Manual Integration used to determine area response

RL

Reporting Detection Limit

ND
S

Not Detected at the Reporting Limit
Spike Recovery outside accepted recovery limits

Page 16 of 66

31628 Glendale St.

Analytical Report

Livonia, Michigan 48150
TEL: 734.422.8000
FAX: 734.422.5342
Website: www.rtilab.com

(consolidated)

WO#:

0604884

Date Reported:

5/5/2006

Collection Date: 4/27/2006 10:45:00 AM

CLIENT:

PM Environmental, Inc.

Project:

7876 Van Dyke - 22-692A

Lab ID:

0604884-004

Matrix: SOIL

Client Sample ID SB-4 2-3'
Analyses

Result

RL Qual Units

Volatile Organic Compounds

DF

Date Analyzed
Analyst: JW

SW8260B

o-Xylene

ND

62

µg/Kg-dry

52.9

5/1/2006 10:34:00 PM

p-Isopropyltoluene

ND

62

µg/Kg-dry

52.9

5/1/2006 10:34:00 PM

sec-Butylbenzene

ND

62

µg/Kg-dry

52.9

5/1/2006 10:34:00 PM

Styrene

ND

62

µg/Kg-dry

52.9

5/1/2006 10:34:00 PM

t-Butyl alcohol

ND

2,500

µg/Kg-dry

52.9

5/1/2006 10:34:00 PM

tert-Amyl Methyl Ether

ND

250

µg/Kg-dry

52.9

5/1/2006 10:34:00 PM

tert-Butyl Ethyl Ether

ND

310

µg/Kg-dry

52.9

5/1/2006 10:34:00 PM

tert-Butylbenzene

ND

62

µg/Kg-dry

52.9

5/1/2006 10:34:00 PM

Tetrachloroethene

ND

62

µg/Kg-dry

52.9

5/1/2006 10:34:00 PM

Toluene

ND

62

µg/Kg-dry

52.9

5/1/2006 10:34:00 PM

trans-1,2-Dichloroethene

ND

62

µg/Kg-dry

52.9

5/1/2006 10:34:00 PM

trans-1,3-Dichloropropene

ND

62

µg/Kg-dry

52.9

5/1/2006 10:34:00 PM

trans-1,4-Dichloro-2-butene

ND

62

µg/Kg-dry

52.9

5/1/2006 10:34:00 PM

Trichloroethene

ND

62

µg/Kg-dry

52.9

5/1/2006 10:34:00 PM

Trichlorofluoromethane

ND

62

µg/Kg-dry

52.9

5/1/2006 10:34:00 PM

Vinyl chloride

ND

50

µg/Kg-dry

52.9

5/1/2006 10:34:00 PM

Xylenes, Total

ND

190

µg/Kg-dry

52.9

5/1/2006 10:34:00 PM

Surr: 4-Bromofluorobenzene

111

70-130

%REC

52.9

5/1/2006 10:34:00 PM

Surr: Dibromofluoromethane

112

70-130

%REC

52.9

5/1/2006 10:34:00 PM

Surr: Toluene-d8

106

70-130

%REC

52.9

5/1/2006 10:34:00 PM

15

1.0

1

5/1/2006

PERCENT MOISTURE
Percent Moisture

Qualifiers:

Analyst: MT3

D2216 wt% *

Value exceeds Maximum Contaminant Level

B

Analyte detected in the associated Method Blank

E

Value above quantitation range

H

Holding times for preparation or analysis exceeded

M

Manual Integration used to determine area response

RL

Reporting Detection Limit

ND
S

Not Detected at the Reporting Limit
Spike Recovery outside accepted recovery limits

Page 17 of 66

31628 Glendale St.

Analytical Report

Livonia, Michigan 48150
TEL: 734.422.8000
FAX: 734.422.5342
Website: www.rtilab.com

(consolidated)

WO#:

0604884

Date Reported:

5/5/2006

Collection Date: 4/27/2006 12:00:00 PM

CLIENT:

PM Environmental, Inc.

Project:

7876 Van Dyke - 22-692A

Lab ID:

0604884-005

Matrix: SOIL

Client Sample ID SB-5 1-2'
Analyses

Result

RL Qual Units

DF

Polychlorinated Biphenyls

Date Analyzed
Analyst: MB

SW8082

Aroclor 1016

ND

38

µg/Kg-dry

1

5/2/2006 10:49:54 PM

Aroclor 1221

ND

38

µg/Kg-dry

1

5/2/2006 10:49:54 PM

Aroclor 1232

ND

38

µg/Kg-dry

1

5/2/2006 10:49:54 PM

Aroclor 1242

ND

38

µg/Kg-dry

1

5/2/2006 10:49:54 PM

Aroclor 1248

ND

38

µg/Kg-dry

1

5/2/2006 10:49:54 PM

Aroclor 1254

ND

38

µg/Kg-dry

1

5/2/2006 10:49:54 PM

Aroclor 1260

ND

38

µg/Kg-dry

1

5/2/2006 10:49:54 PM

Surr: Decachlorobiphenyl

87.7

70-130

%REC

1

5/2/2006 10:49:54 PM

Surr: Tetrachloro-m-xylene

72.0

70-130

%REC

1

5/2/2006 10:49:54 PM

490

450

µg/Kg-dry

20

5/1/2006 1:53:45 PM

16,000

2,200

µg/Kg-dry

20

5/1/2006 1:53:45 PM

9,300

2,200

µg/Kg-dry

20

5/1/2006 1:53:45 PM

Metals, ICP/MS

Analyst: AB2

SW6020A

Cadmium
Chromium
Lead

Polynuclear Aromatic Hydrocarbons
Semi-Volatile Organic Compounds

Analyst: JG3

SW8270C

2-Methylnaphthalene

ND

380

µg/Kg-dry

1

5/2/2006 7:16:00 PM

Acenaphthene

ND

380

µg/Kg-dry

1

5/2/2006 7:16:00 PM

Acenaphthylene

ND

380

µg/Kg-dry

1

5/2/2006 7:16:00 PM

Anthracene

ND

380

µg/Kg-dry

1

5/2/2006 7:16:00 PM

Benz(a)anthracene

ND

380

µg/Kg-dry

1

5/2/2006 7:16:00 PM

Benzo(a)pyrene

ND

380

µg/Kg-dry

1

5/2/2006 7:16:00 PM

Benzo(b)fluoranthene

ND

380

µg/Kg-dry

1

5/2/2006 7:16:00 PM

Benzo(g,h,i)perylene

ND

380

µg/Kg-dry

1

5/2/2006 7:16:00 PM

Benzo(k)fluoranthene

ND

380

µg/Kg-dry

1

5/2/2006 7:16:00 PM

Chrysene

ND

380

µg/Kg-dry

1

5/2/2006 7:16:00 PM

Dibenz(a,h)anthracene

ND

380

µg/Kg-dry

1

5/2/2006 7:16:00 PM

Fluoranthene

ND

380

µg/Kg-dry

1

5/2/2006 7:16:00 PM

Fluorene

ND

380

µg/Kg-dry

1

5/2/2006 7:16:00 PM

Indeno(1,2,3-cd)pyrene

ND

380

µg/Kg-dry

1

5/2/2006 7:16:00 PM

Naphthalene

ND

380

µg/Kg-dry

1

5/2/2006 7:16:00 PM

Phenanthrene

ND

380

µg/Kg-dry

1

5/2/2006 7:16:00 PM

Pyrene

ND

380

µg/Kg-dry

1

5/2/2006 7:16:00 PM

Surr: 2,4,6-Tribromophenol

74.8

25-93.9

%REC

1

5/2/2006 7:16:00 PM

Surr: 2-Fluorobiphenyl

98.1

26-105

%REC

1

5/2/2006 7:16:00 PM

Qualifiers:

*

Value exceeds Maximum Contaminant Level

B

Analyte detected in the associated Method Blank

E

Value above quantitation range

H

Holding times for preparation or analysis exceeded

M

Manual Integration used to determine area response

RL

Reporting Detection Limit

ND
S

Not Detected at the Reporting Limit
Spike Recovery outside accepted recovery limits

Page 18 of 66

31628 Glendale St.

Analytical Report

Livonia, Michigan 48150
TEL: 734.422.8000
FAX: 734.422.5342
Website: www.rtilab.com

(consolidated)

WO#:

0604884

Date Reported:

5/5/2006

Collection Date: 4/27/2006 12:00:00 PM

CLIENT:

PM Environmental, Inc.

Project:

7876 Van Dyke - 22-692A

Lab ID:

0604884-005

Matrix: SOIL

Client Sample ID SB-5 1-2'
Analyses

Result

RL Qual Units

Polynuclear Aromatic Hydrocarbons
Semi-Volatile Organic Compounds

DF

Date Analyzed
Analyst: JG3

SW8270C

Surr: 2-Fluorophenol

106

25-120

%REC

1

5/2/2006 7:16:00 PM

Surr: Nitrobenzene-d5

101

30.1-104

%REC

1

5/2/2006 7:16:00 PM

Surr: Phenol-d5

106

25-118

%REC

1

5/2/2006 7:16:00 PM

Surr: Terphenyl-d14

106

27.1-115

%REC

1

5/2/2006 7:16:00 PM

1,1,1,2-Tetrachloroethane

ND

63

µg/Kg-dry

55

5/1/2006 11:07:00 PM

1,1,1-Trichloroethane

ND

63

µg/Kg-dry

55

5/1/2006 11:07:00 PM

1,1,2,2-Tetrachloroethane

ND

63

µg/Kg-dry

55

5/1/2006 11:07:00 PM

1,1,2-Trichloro-1,2,2-trifluoroethane

ND

63

µg/Kg-dry

55

5/1/2006 11:07:00 PM

1,1,2-Trichloroethane

ND

63

µg/Kg-dry

55

5/1/2006 11:07:00 PM

1,1-Dichloroethane

ND

63

µg/Kg-dry

55

5/1/2006 11:07:00 PM

1,1-Dichloroethene

ND

63

µg/Kg-dry

55

5/1/2006 11:07:00 PM

1,1-Dichloropropene

ND

63

µg/Kg-dry

55

5/1/2006 11:07:00 PM

1,2,3-Trichlorobenzene

ND

63

µg/Kg-dry

55

5/1/2006 11:07:00 PM

1,2,3-Trichloropropane

ND

63

µg/Kg-dry

55

5/1/2006 11:07:00 PM

1,2,3-Trimethylbenzene

ND

63

µg/Kg-dry

55

5/1/2006 11:07:00 PM

1,2,4-Trichlorobenzene

ND

310

µg/Kg-dry

55

5/1/2006 11:07:00 PM

1,2,4-Trimethylbenzene

ND

63

µg/Kg-dry

55

5/1/2006 11:07:00 PM

1,2-Dibromo-3-chloropropane

ND

63

µg/Kg-dry

55

5/1/2006 11:07:00 PM

1,2-Dichlorobenzene

ND

63

µg/Kg-dry

55

5/1/2006 11:07:00 PM

1,2-Dichloroethane

ND

63

µg/Kg-dry

55

5/1/2006 11:07:00 PM

1,2-Dichloropropane

ND

63

µg/Kg-dry

55

5/1/2006 11:07:00 PM

1,3,5-Trimethylbenzene

ND

63

µg/Kg-dry

55

5/1/2006 11:07:00 PM

1,3-Dichlorobenzene

ND

63

µg/Kg-dry

55

5/1/2006 11:07:00 PM

1,3-Dichloropropane

ND

63

µg/Kg-dry

55

5/1/2006 11:07:00 PM

1,4-Dichlorobenzene

ND

63

µg/Kg-dry

55

5/1/2006 11:07:00 PM

2,2-Dichloropropane

ND

63

µg/Kg-dry

55

5/1/2006 11:07:00 PM

2-Chloroethyl vinyl ether

ND

630

µg/Kg-dry

55

5/1/2006 11:07:00 PM

2-Chlorotoluene

ND

63

µg/Kg-dry

55

5/1/2006 11:07:00 PM

2-Hexanone

ND

3,100

µg/Kg-dry

55

5/1/2006 11:07:00 PM

2-Methylnaphthalene

ND

310

µg/Kg-dry

55

5/1/2006 11:07:00 PM

2-Nitropropane

ND

250

µg/Kg-dry

55

5/1/2006 11:07:00 PM

4-Chlorotoluene

ND

63

µg/Kg-dry

55

5/1/2006 11:07:00 PM

Acetone

ND

3,100

µg/Kg-dry

55

5/1/2006 11:07:00 PM

Volatile Organic Compounds

Qualifiers:

Analyst: JW

SW8260B

*

Value exceeds Maximum Contaminant Level

B

Analyte detected in the associated Method Blank

E

Value above quantitation range

H

Holding times for preparation or analysis exceeded

M

Manual Integration used to determine area response

RL

Reporting Detection Limit

ND
S

Not Detected at the Reporting Limit
Spike Recovery outside accepted recovery limits

Page 19 of 66

31628 Glendale St.

Analytical Report

Livonia, Michigan 48150
TEL: 734.422.8000
FAX: 734.422.5342
Website: www.rtilab.com

(consolidated)

WO#:

0604884

Date Reported:

5/5/2006

Collection Date: 4/27/2006 12:00:00 PM

CLIENT:

PM Environmental, Inc.

Project:

7876 Van Dyke - 22-692A

Lab ID:

0604884-005

Matrix: SOIL

Client Sample ID SB-5 1-2'
Analyses

Result

RL Qual Units

Volatile Organic Compounds

DF

Date Analyzed
Analyst: JW

SW8260B

Acrylonitrile

ND

310

µg/Kg-dry

55

5/1/2006 11:07:00 PM

Benzene

ND

63

µg/Kg-dry

55

5/1/2006 11:07:00 PM

Bromobenzene

ND

63

µg/Kg-dry

55

5/1/2006 11:07:00 PM

Bromochloromethane

ND

63

µg/Kg-dry

55

5/1/2006 11:07:00 PM

Bromodichloromethane

ND

63

µg/Kg-dry

55

5/1/2006 11:07:00 PM

Bromoform

ND

63

µg/Kg-dry

55

5/1/2006 11:07:00 PM

Bromomethane

ND

310

µg/Kg-dry

55

5/1/2006 11:07:00 PM

Carbon disulfide

ND

310

µg/Kg-dry

55

5/1/2006 11:07:00 PM

Carbon tetrachloride

ND

63

µg/Kg-dry

55

5/1/2006 11:07:00 PM

Chlorobenzene

ND

63

µg/Kg-dry

55

5/1/2006 11:07:00 PM

Chloroethane

ND

310

µg/Kg-dry

55

5/1/2006 11:07:00 PM

Chloroform

ND

63

µg/Kg-dry

55

5/1/2006 11:07:00 PM

Chloromethane

ND

63

µg/Kg-dry

55

5/1/2006 11:07:00 PM

cis-1,2-Dichloroethene

ND

63

µg/Kg-dry

55

5/1/2006 11:07:00 PM

cis-1,3-Dichloropropene

ND

63

µg/Kg-dry

55

5/1/2006 11:07:00 PM

Dibromochloromethane

ND

63

µg/Kg-dry

55

5/1/2006 11:07:00 PM

Dibromomethane

ND

63

µg/Kg-dry

55

5/1/2006 11:07:00 PM

Dichlorodifluoromethane

ND

63

µg/Kg-dry

55

5/1/2006 11:07:00 PM

Dichloromethane

ND

310

µg/Kg-dry

55

5/1/2006 11:07:00 PM

Diethyl ether

ND

310

µg/Kg-dry

55

5/1/2006 11:07:00 PM

Ethyl methacrylate

ND

63

µg/Kg-dry

55

5/1/2006 11:07:00 PM

Ethylbenzene

ND

63

µg/Kg-dry

55

5/1/2006 11:07:00 PM

Ethylene dibromide

ND

63

µg/Kg-dry

55

5/1/2006 11:07:00 PM

Hexachlorobutadiene

ND

310

µg/Kg-dry

55

5/1/2006 11:07:00 PM

Hexachloroethane

ND

63

µg/Kg-dry

55

5/1/2006 11:07:00 PM

Isopropyl ether

ND

310

µg/Kg-dry

55

5/1/2006 11:07:00 PM

Isopropylbenzene

ND

63

µg/Kg-dry

55

5/1/2006 11:07:00 PM

m,p-Xylene

ND

130

µg/Kg-dry

55

5/1/2006 11:07:00 PM

Methyl ethyl ketone

ND

310

µg/Kg-dry

55

5/1/2006 11:07:00 PM

Methyl Iodide

ND

310

µg/Kg-dry

55

5/1/2006 11:07:00 PM

Methyl isobutyl ketone

ND

630

µg/Kg-dry

55

5/1/2006 11:07:00 PM

Methyl tert-butyl ether

ND

310

µg/Kg-dry

55

5/1/2006 11:07:00 PM

Naphthalene

ND

310

µg/Kg-dry

55

5/1/2006 11:07:00 PM

n-Butylbenzene

ND

63

µg/Kg-dry

55

5/1/2006 11:07:00 PM

n-Propylbenzene

ND

63

µg/Kg-dry

55

5/1/2006 11:07:00 PM

Qualifiers:

*

Value exceeds Maximum Contaminant Level

B

Analyte detected in the associated Method Blank

E

Value above quantitation range

H

Holding times for preparation or analysis exceeded

M

Manual Integration used to determine area response

RL

Reporting Detection Limit

ND
S

Not Detected at the Reporting Limit
Spike Recovery outside accepted recovery limits

Page 20 of 66

31628 Glendale St.

Analytical Report

Livonia, Michigan 48150
TEL: 734.422.8000
FAX: 734.422.5342
Website: www.rtilab.com

(consolidated)

WO#:

0604884

Date Reported:

5/5/2006

Collection Date: 4/27/2006 12:00:00 PM

CLIENT:

PM Environmental, Inc.

Project:

7876 Van Dyke - 22-692A

Lab ID:

0604884-005

Matrix: SOIL

Client Sample ID SB-5 1-2'
Analyses

Result

RL Qual Units

Volatile Organic Compounds

DF

Date Analyzed
Analyst: JW

SW8260B

o-Xylene

ND

63

µg/Kg-dry

55

5/1/2006 11:07:00 PM

p-Isopropyltoluene

ND

63

µg/Kg-dry

55

5/1/2006 11:07:00 PM

sec-Butylbenzene

ND

63

µg/Kg-dry

55

5/1/2006 11:07:00 PM

Styrene

ND

63

µg/Kg-dry

55

5/1/2006 11:07:00 PM

t-Butyl alcohol

ND

2,500

µg/Kg-dry

55

5/1/2006 11:07:00 PM

tert-Amyl Methyl Ether

ND

250

µg/Kg-dry

55

5/1/2006 11:07:00 PM

tert-Butyl Ethyl Ether

ND

310

µg/Kg-dry

55

5/1/2006 11:07:00 PM

tert-Butylbenzene

ND

63

µg/Kg-dry

55

5/1/2006 11:07:00 PM

Tetrachloroethene

ND

63

µg/Kg-dry

55

5/1/2006 11:07:00 PM

Toluene

ND

63

µg/Kg-dry

55

5/1/2006 11:07:00 PM

trans-1,2-Dichloroethene

ND

63

µg/Kg-dry

55

5/1/2006 11:07:00 PM

trans-1,3-Dichloropropene

ND

63

µg/Kg-dry

55

5/1/2006 11:07:00 PM

trans-1,4-Dichloro-2-butene

ND

63

µg/Kg-dry

55

5/1/2006 11:07:00 PM

Trichloroethene

ND

63

µg/Kg-dry

55

5/1/2006 11:07:00 PM

Trichlorofluoromethane

ND

63

µg/Kg-dry

55

5/1/2006 11:07:00 PM

Vinyl chloride

ND

50

µg/Kg-dry

55

5/1/2006 11:07:00 PM

Xylenes, Total

ND

190

µg/Kg-dry

55

5/1/2006 11:07:00 PM

Surr: 4-Bromofluorobenzene

114

70-130

%REC

55

5/1/2006 11:07:00 PM

Surr: Dibromofluoromethane

109

70-130

%REC

55

5/1/2006 11:07:00 PM

Surr: Toluene-d8

111

70-130

%REC

55

5/1/2006 11:07:00 PM

12

1.0

1

5/1/2006

PERCENT MOISTURE
Percent Moisture

Qualifiers:

Analyst: MT3

D2216 wt% *

Value exceeds Maximum Contaminant Level

B

Analyte detected in the associated Method Blank

E

Value above quantitation range

H

Holding times for preparation or analysis exceeded

M

Manual Integration used to determine area response

RL

Reporting Detection Limit

ND
S

Not Detected at the Reporting Limit
Spike Recovery outside accepted recovery limits

Page 21 of 66

31628 Glendale St.

Analytical Report

Livonia, Michigan 48150
TEL: 734.422.8000
FAX: 734.422.5342
Website: www.rtilab.com

(consolidated)

WO#:

0604884

Date Reported:

5/5/2006

Collection Date: 4/27/2006 12:30:00 PM

CLIENT:

PM Environmental, Inc.

Project:

7876 Van Dyke - 22-692A

Lab ID:

0604884-006

Matrix: SOIL

Client Sample ID SB-6 1-2'
Analyses

Result

RL Qual Units

DF

Polychlorinated Biphenyls

Date Analyzed
Analyst: MB

SW8082

Aroclor 1016

ND

40

µg/Kg-dry

1

5/2/2006 11:29:32 PM

Aroclor 1221

ND

40

µg/Kg-dry

1

5/2/2006 11:29:32 PM

Aroclor 1232

ND

40

µg/Kg-dry

1

5/2/2006 11:29:32 PM

Aroclor 1242

ND

40

µg/Kg-dry

1

5/2/2006 11:29:32 PM

Aroclor 1248

ND

40

µg/Kg-dry

1

5/2/2006 11:29:32 PM

Aroclor 1254

ND

40

µg/Kg-dry

1

5/2/2006 11:29:32 PM

Aroclor 1260

ND

40

µg/Kg-dry

1

5/2/2006 11:29:32 PM

Surr: Decachlorobiphenyl

86.4

70-130

%REC

1

5/2/2006 11:29:32 PM

Surr: Tetrachloro-m-xylene

75.1

70-130

%REC

1

5/2/2006 11:29:32 PM

ND

450

µg/Kg-dry

20

5/1/2006 2:01:06 PM

Chromium

12,000

2,300

µg/Kg-dry

20

5/1/2006 2:01:06 PM

Lead

13,000

2,300

µg/Kg-dry

20

5/1/2006 2:01:06 PM

Metals, ICP/MS

Analyst: AB2

SW6020A

Cadmium

Polynuclear Aromatic Hydrocarbons
Semi-Volatile Organic Compounds

Analyst: JG3

SW8270C

2-Methylnaphthalene

ND

400

µg/Kg-dry

1

5/2/2006 7:53:00 PM

Acenaphthene

ND

400

µg/Kg-dry

1

5/2/2006 7:53:00 PM

Acenaphthylene

ND

400

µg/Kg-dry

1

5/2/2006 7:53:00 PM

Anthracene

ND

400

µg/Kg-dry

1

5/2/2006 7:53:00 PM

Benz(a)anthracene

ND

400

µg/Kg-dry

1

5/2/2006 7:53:00 PM

Benzo(a)pyrene

ND

400

µg/Kg-dry

1

5/2/2006 7:53:00 PM

Benzo(b)fluoranthene

ND

400

µg/Kg-dry

1

5/2/2006 7:53:00 PM

Benzo(g,h,i)perylene

ND

400

µg/Kg-dry

1

5/2/2006 7:53:00 PM

Benzo(k)fluoranthene

ND

400

µg/Kg-dry

1

5/2/2006 7:53:00 PM

Chrysene

ND

400

µg/Kg-dry

1

5/2/2006 7:53:00 PM

Dibenz(a,h)anthracene

ND

400

µg/Kg-dry

1

5/2/2006 7:53:00 PM

Fluoranthene

ND

400

µg/Kg-dry

1

5/2/2006 7:53:00 PM

Fluorene

ND

400

µg/Kg-dry

1

5/2/2006 7:53:00 PM

Indeno(1,2,3-cd)pyrene

ND

400

µg/Kg-dry

1

5/2/2006 7:53:00 PM

Naphthalene

ND

400

µg/Kg-dry

1

5/2/2006 7:53:00 PM

Phenanthrene

ND

400

µg/Kg-dry

1

5/2/2006 7:53:00 PM

Pyrene

ND

400

µg/Kg-dry

1

5/2/2006 7:53:00 PM

Surr: 2,4,6-Tribromophenol

77.4

25-93.9

%REC

1

5/2/2006 7:53:00 PM

Surr: 2-Fluorobiphenyl

94.0

26-105

%REC

1

5/2/2006 7:53:00 PM

Qualifiers:

*

Value exceeds Maximum Contaminant Level

B

Analyte detected in the associated Method Blank

E

Value above quantitation range

H

Holding times for preparation or analysis exceeded

M

Manual Integration used to determine area response

RL

Reporting Detection Limit

ND
S

Not Detected at the Reporting Limit
Spike Recovery outside accepted recovery limits

Page 22 of 66

31628 Glendale St.

Analytical Report

Livonia, Michigan 48150
TEL: 734.422.8000
FAX: 734.422.5342
Website: www.rtilab.com

(consolidated)

WO#:

0604884

Date Reported:

5/5/2006

Collection Date: 4/27/2006 12:30:00 PM

CLIENT:

PM Environmental, Inc.

Project:

7876 Van Dyke - 22-692A

Lab ID:

0604884-006

Matrix: SOIL

Client Sample ID SB-6 1-2'
Analyses

Result

RL Qual Units

Polynuclear Aromatic Hydrocarbons
Semi-Volatile Organic Compounds

DF

Date Analyzed
Analyst: JG3

SW8270C

Surr: 2-Fluorophenol

106

25-120

%REC

1

5/2/2006 7:53:00 PM

Surr: Nitrobenzene-d5

96.8

30.1-104

%REC

1

5/2/2006 7:53:00 PM

Surr: Phenol-d5

103

25-118

%REC

1

5/2/2006 7:53:00 PM

Surr: Terphenyl-d14

102

27.1-115

%REC

1

5/2/2006 7:53:00 PM

1,1,1,2-Tetrachloroethane

ND

66

µg/Kg-dry

54.8

5/2/2006 1:22:00 AM

1,1,1-Trichloroethane

ND

66

µg/Kg-dry

54.8

5/2/2006 1:22:00 AM

1,1,2,2-Tetrachloroethane

ND

66

µg/Kg-dry

54.8

5/2/2006 1:22:00 AM

1,1,2-Trichloro-1,2,2-trifluoroethane

ND

66

µg/Kg-dry

54.8

5/2/2006 1:22:00 AM

1,1,2-Trichloroethane

ND

66

µg/Kg-dry

54.8

5/2/2006 1:22:00 AM

1,1-Dichloroethane

ND

66

µg/Kg-dry

54.8

5/2/2006 1:22:00 AM

1,1-Dichloroethene

ND

66

µg/Kg-dry

54.8

5/2/2006 1:22:00 AM

1,1-Dichloropropene

ND

66

µg/Kg-dry

54.8

5/2/2006 1:22:00 AM

1,2,3-Trichlorobenzene

ND

66

µg/Kg-dry

54.8

5/2/2006 1:22:00 AM

1,2,3-Trichloropropane

ND

66

µg/Kg-dry

54.8

5/2/2006 1:22:00 AM

1,2,3-Trimethylbenzene

ND

66

µg/Kg-dry

54.8

5/2/2006 1:22:00 AM

1,2,4-Trichlorobenzene

ND

330

µg/Kg-dry

54.8

5/2/2006 1:22:00 AM

1,2,4-Trimethylbenzene

ND

66

µg/Kg-dry

54.8

5/2/2006 1:22:00 AM

1,2-Dibromo-3-chloropropane

ND

66

µg/Kg-dry

54.8

5/2/2006 1:22:00 AM

1,2-Dichlorobenzene

ND

66

µg/Kg-dry

54.8

5/2/2006 1:22:00 AM

1,2-Dichloroethane

ND

66

µg/Kg-dry

54.8

5/2/2006 1:22:00 AM

1,2-Dichloropropane

ND

66

µg/Kg-dry

54.8

5/2/2006 1:22:00 AM

1,3,5-Trimethylbenzene

ND

66

µg/Kg-dry

54.8

5/2/2006 1:22:00 AM

1,3-Dichlorobenzene

ND

66

µg/Kg-dry

54.8

5/2/2006 1:22:00 AM

1,3-Dichloropropane

ND

66

µg/Kg-dry

54.8

5/2/2006 1:22:00 AM

1,4-Dichlorobenzene

ND

66

µg/Kg-dry

54.8

5/2/2006 1:22:00 AM

2,2-Dichloropropane

ND

66

µg/Kg-dry

54.8

5/2/2006 1:22:00 AM

2-Chloroethyl vinyl ether

ND

660

µg/Kg-dry

54.8

5/2/2006 1:22:00 AM

2-Chlorotoluene

ND

66

µg/Kg-dry

54.8

5/2/2006 1:22:00 AM

2-Hexanone

ND

3,300

µg/Kg-dry

54.8

5/2/2006 1:22:00 AM

2-Methylnaphthalene

ND

330

µg/Kg-dry

54.8

5/2/2006 1:22:00 AM

2-Nitropropane

ND

260

µg/Kg-dry

54.8

5/2/2006 1:22:00 AM

4-Chlorotoluene

ND

66

µg/Kg-dry

54.8

5/2/2006 1:22:00 AM

Acetone

ND

3,300

µg/Kg-dry

54.8

5/2/2006 1:22:00 AM

Volatile Organic Compounds

Qualifiers:

Analyst: JW

SW8260B

*

Value exceeds Maximum Contaminant Level

B

Analyte detected in the associated Method Blank

E

Value above quantitation range

H

Holding times for preparation or analysis exceeded

M

Manual Integration used to determine area response

RL

Reporting Detection Limit

ND
S

Not Detected at the Reporting Limit
Spike Recovery outside accepted recovery limits

Page 23 of 66

31628 Glendale St.

Analytical Report

Livonia, Michigan 48150
TEL: 734.422.8000
FAX: 734.422.5342
Website: www.rtilab.com

(consolidated)

WO#:

0604884

Date Reported:

5/5/2006

Collection Date: 4/27/2006 12:30:00 PM

CLIENT:

PM Environmental, Inc.

Project:

7876 Van Dyke - 22-692A

Lab ID:

0604884-006

Matrix: SOIL

Client Sample ID SB-6 1-2'
Analyses

Result

RL Qual Units

Volatile Organic Compounds

DF

Date Analyzed
Analyst: JW

SW8260B

Acrylonitrile

ND

330

µg/Kg-dry

54.8

5/2/2006 1:22:00 AM

Benzene

ND

66

µg/Kg-dry

54.8

5/2/2006 1:22:00 AM

Bromobenzene

ND

66

µg/Kg-dry

54.8

5/2/2006 1:22:00 AM

Bromochloromethane

ND

66

µg/Kg-dry

54.8

5/2/2006 1:22:00 AM

Bromodichloromethane

ND

66

µg/Kg-dry

54.8

5/2/2006 1:22:00 AM

Bromoform

ND

66

µg/Kg-dry

54.8

5/2/2006 1:22:00 AM

Bromomethane

ND

330

µg/Kg-dry

54.8

5/2/2006 1:22:00 AM

Carbon disulfide

ND

330

µg/Kg-dry

54.8

5/2/2006 1:22:00 AM

Carbon tetrachloride

ND

66

µg/Kg-dry

54.8

5/2/2006 1:22:00 AM

Chlorobenzene

ND

66

µg/Kg-dry

54.8

5/2/2006 1:22:00 AM

Chloroethane

ND

330

µg/Kg-dry

54.8

5/2/2006 1:22:00 AM

Chloroform

ND

66

µg/Kg-dry

54.8

5/2/2006 1:22:00 AM

Chloromethane

ND

66

µg/Kg-dry

54.8

5/2/2006 1:22:00 AM

cis-1,2-Dichloroethene

ND

66

µg/Kg-dry

54.8

5/2/2006 1:22:00 AM

cis-1,3-Dichloropropene

ND

66

µg/Kg-dry

54.8

5/2/2006 1:22:00 AM

Dibromochloromethane

ND

66

µg/Kg-dry

54.8

5/2/2006 1:22:00 AM

Dibromomethane

ND

66

µg/Kg-dry

54.8

5/2/2006 1:22:00 AM

Dichlorodifluoromethane

ND

66

µg/Kg-dry

54.8

5/2/2006 1:22:00 AM

Dichloromethane

ND

330

µg/Kg-dry

54.8

5/2/2006 1:22:00 AM

Diethyl ether

ND

330

µg/Kg-dry

54.8

5/2/2006 1:22:00 AM

Ethyl methacrylate

ND

66

µg/Kg-dry

54.8

5/2/2006 1:22:00 AM

Ethylbenzene

ND

66

µg/Kg-dry

54.8

5/2/2006 1:22:00 AM

Ethylene dibromide

ND

66

µg/Kg-dry

54.8

5/2/2006 1:22:00 AM

Hexachlorobutadiene

ND

330

µg/Kg-dry

54.8

5/2/2006 1:22:00 AM

Hexachloroethane

ND

66

µg/Kg-dry

54.8

5/2/2006 1:22:00 AM

Isopropyl ether

ND

330

µg/Kg-dry

54.8

5/2/2006 1:22:00 AM

Isopropylbenzene

ND

66

µg/Kg-dry

54.8

5/2/2006 1:22:00 AM

m,p-Xylene

ND

130

µg/Kg-dry

54.8

5/2/2006 1:22:00 AM

Methyl ethyl ketone

ND

330

µg/Kg-dry

54.8

5/2/2006 1:22:00 AM

Methyl Iodide

ND

330

µg/Kg-dry

54.8

5/2/2006 1:22:00 AM

Methyl isobutyl ketone

ND

660

µg/Kg-dry

54.8

5/2/2006 1:22:00 AM

Methyl tert-butyl ether

ND

330

µg/Kg-dry

54.8

5/2/2006 1:22:00 AM

Naphthalene

ND

330

µg/Kg-dry

54.8

5/2/2006 1:22:00 AM

n-Butylbenzene

ND

66

µg/Kg-dry

54.8

5/2/2006 1:22:00 AM

n-Propylbenzene

ND

66

µg/Kg-dry

54.8

5/2/2006 1:22:00 AM

Qualifiers:

*

Value exceeds Maximum Contaminant Level

B

Analyte detected in the associated Method Blank

E

Value above quantitation range

H

Holding times for preparation or analysis exceeded

M

Manual Integration used to determine area response

RL

Reporting Detection Limit

ND
S

Not Detected at the Reporting Limit
Spike Recovery outside accepted recovery limits

Page 24 of 66

31628 Glendale St.

Analytical Report

Livonia, Michigan 48150
TEL: 734.422.8000
FAX: 734.422.5342
Website: www.rtilab.com

(consolidated)

WO#:

0604884

Date Reported:

5/5/2006

Collection Date: 4/27/2006 12:30:00 PM

CLIENT:

PM Environmental, Inc.

Project:

7876 Van Dyke - 22-692A

Lab ID:

0604884-006

Matrix: SOIL

Client Sample ID SB-6 1-2'
Analyses

Result

RL Qual Units

Volatile Organic Compounds

DF

Date Analyzed
Analyst: JW

SW8260B

o-Xylene

ND

66

µg/Kg-dry

54.8

5/2/2006 1:22:00 AM

p-Isopropyltoluene

ND

66

µg/Kg-dry

54.8

5/2/2006 1:22:00 AM

sec-Butylbenzene

ND

66

µg/Kg-dry

54.8

5/2/2006 1:22:00 AM

Styrene

ND

66

µg/Kg-dry

54.8

5/2/2006 1:22:00 AM

t-Butyl alcohol

ND

2,600

µg/Kg-dry

54.8

5/2/2006 1:22:00 AM

tert-Amyl Methyl Ether

ND

260

µg/Kg-dry

54.8

5/2/2006 1:22:00 AM

tert-Butyl Ethyl Ether

ND

330

µg/Kg-dry

54.8

5/2/2006 1:22:00 AM

tert-Butylbenzene

ND

66

µg/Kg-dry

54.8

5/2/2006 1:22:00 AM

Tetrachloroethene

ND

66

µg/Kg-dry

54.8

5/2/2006 1:22:00 AM

Toluene

ND

66

µg/Kg-dry

54.8

5/2/2006 1:22:00 AM

trans-1,2-Dichloroethene

ND

66

µg/Kg-dry

54.8

5/2/2006 1:22:00 AM

trans-1,3-Dichloropropene

ND

66

µg/Kg-dry

54.8

5/2/2006 1:22:00 AM

trans-1,4-Dichloro-2-butene

ND

66

µg/Kg-dry

54.8

5/2/2006 1:22:00 AM

Trichloroethene

ND

66

µg/Kg-dry

54.8

5/2/2006 1:22:00 AM

Trichlorofluoromethane

ND

66

µg/Kg-dry

54.8

5/2/2006 1:22:00 AM

Vinyl chloride

ND

53

µg/Kg-dry

54.8

5/2/2006 1:22:00 AM

Xylenes, Total

ND

200

µg/Kg-dry

54.8

5/2/2006 1:22:00 AM

Surr: 4-Bromofluorobenzene

113

70-130

%REC

54.8

5/2/2006 1:22:00 AM

Surr: Dibromofluoromethane

112

70-130

%REC

54.8

5/2/2006 1:22:00 AM

Surr: Toluene-d8

109

70-130

%REC

54.8

5/2/2006 1:22:00 AM

17

1.0

1

5/1/2006

PERCENT MOISTURE
Percent Moisture

Qualifiers:

Analyst: MT3

D2216 wt% *

Value exceeds Maximum Contaminant Level

B

Analyte detected in the associated Method Blank

E

Value above quantitation range

H

Holding times for preparation or analysis exceeded

M

Manual Integration used to determine area response

RL

Reporting Detection Limit

ND
S

Not Detected at the Reporting Limit
Spike Recovery outside accepted recovery limits

Page 25 of 66

31628 Glendale St.

Analytical Report

Livonia, Michigan 48150
TEL: 734.422.8000
FAX: 734.422.5342
Website: www.rtilab.com

(consolidated)

WO#:

0604884

Date Reported:

5/5/2006

Collection Date: 4/27/2006 12:45:00 PM

CLIENT:

PM Environmental, Inc.

Project:

7876 Van Dyke - 22-692A

Lab ID:

0604884-007

Matrix: SOIL

Client Sample ID SB-7 2-3'
Analyses

Result

RL Qual Units

DF

Polychlorinated Biphenyls

Date Analyzed
Analyst: MB

SW8082

Aroclor 1016

ND

41

µg/Kg-dry

1

5/3/2006 1:28:50 AM

Aroclor 1221

ND

41

µg/Kg-dry

1

5/3/2006 1:28:50 AM

Aroclor 1232

ND

41

µg/Kg-dry

1

5/3/2006 1:28:50 AM

Aroclor 1242

ND

41

µg/Kg-dry

1

5/3/2006 1:28:50 AM

Aroclor 1248

ND

41

µg/Kg-dry

1

5/3/2006 1:28:50 AM

Aroclor 1254

ND

41

µg/Kg-dry

1

5/3/2006 1:28:50 AM

Aroclor 1260

ND

41

µg/Kg-dry

1

5/3/2006 1:28:50 AM

Surr: Decachlorobiphenyl

91.7

70-130

%REC

1

5/3/2006 1:28:50 AM

Surr: Tetrachloro-m-xylene

72.6

70-130

%REC

1

5/3/2006 1:28:50 AM

600

470

µg/Kg-dry

20

5/1/2006 2:03:23 PM

Chromium

17,000

2,300

µg/Kg-dry

20

5/1/2006 2:03:23 PM

Lead

12,000

2,300

µg/Kg-dry

20

5/1/2006 2:03:23 PM

Metals, ICP/MS

Analyst: AB2

SW6020A

Cadmium

Polynuclear Aromatic Hydrocarbons
Semi-Volatile Organic Compounds

Analyst: JG3

SW8270C

2-Methylnaphthalene

ND

410

µg/Kg-dry

1

5/2/2006 8:29:00 PM

Acenaphthene

ND

410

µg/Kg-dry

1

5/2/2006 8:29:00 PM

Acenaphthylene

ND

410

µg/Kg-dry

1

5/2/2006 8:29:00 PM

Anthracene

ND

410

µg/Kg-dry

1

5/2/2006 8:29:00 PM

Benz(a)anthracene

ND

410

µg/Kg-dry

1

5/2/2006 8:29:00 PM

Benzo(a)pyrene

ND

410

µg/Kg-dry

1

5/2/2006 8:29:00 PM

Benzo(b)fluoranthene

ND

410

µg/Kg-dry

1

5/2/2006 8:29:00 PM

Benzo(g,h,i)perylene

ND

410

µg/Kg-dry

1

5/2/2006 8:29:00 PM

Benzo(k)fluoranthene

ND

410

µg/Kg-dry

1

5/2/2006 8:29:00 PM

Chrysene

ND

410

µg/Kg-dry

1

5/2/2006 8:29:00 PM

Dibenz(a,h)anthracene

ND

410

µg/Kg-dry

1

5/2/2006 8:29:00 PM

Fluoranthene

ND

410

µg/Kg-dry

1

5/2/2006 8:29:00 PM

Fluorene

ND

410

µg/Kg-dry

1

5/2/2006 8:29:00 PM

Indeno(1,2,3-cd)pyrene

ND

410

µg/Kg-dry

1

5/2/2006 8:29:00 PM

Naphthalene

ND

410

µg/Kg-dry

1

5/2/2006 8:29:00 PM

Phenanthrene

ND

410

µg/Kg-dry

1

5/2/2006 8:29:00 PM

Pyrene

ND

410

µg/Kg-dry

1

5/2/2006 8:29:00 PM

Surr: 2,4,6-Tribromophenol

63.8

25-93.9

%REC

1

5/2/2006 8:29:00 PM

Surr: 2-Fluorobiphenyl

79.7

26-105

%REC

1

5/2/2006 8:29:00 PM

Qualifiers:

*

Value exceeds Maximum Contaminant Level

B

Analyte detected in the associated Method Blank

E

Value above quantitation range

H

Holding times for preparation or analysis exceeded

M

Manual Integration used to determine area response

RL

Reporting Detection Limit

ND
S

Not Detected at the Reporting Limit
Spike Recovery outside accepted recovery limits

Page 26 of 66

31628 Glendale St.

Analytical Report

Livonia, Michigan 48150
TEL: 734.422.8000
FAX: 734.422.5342
Website: www.rtilab.com

(consolidated)

WO#:

0604884

Date Reported:

5/5/2006

Collection Date: 4/27/2006 12:45:00 PM

CLIENT:

PM Environmental, Inc.

Project:

7876 Van Dyke - 22-692A

Lab ID:

0604884-007

Matrix: SOIL

Client Sample ID SB-7 2-3'
Analyses

Result

RL Qual Units

Polynuclear Aromatic Hydrocarbons
Semi-Volatile Organic Compounds

DF

Date Analyzed
Analyst: JG3

SW8270C

Surr: 2-Fluorophenol

82.2

25-120

%REC

1

5/2/2006 8:29:00 PM

Surr: Nitrobenzene-d5

79.6

30.1-104

%REC

1

5/2/2006 8:29:00 PM

Surr: Phenol-d5

83.8

25-118

%REC

1

5/2/2006 8:29:00 PM

Surr: Terphenyl-d14

83.9

27.1-115

%REC

1

5/2/2006 8:29:00 PM

1,1,1,2-Tetrachloroethane

ND

64

µg/Kg-dry

51.4

5/2/2006 1:56:00 AM

1,1,1-Trichloroethane

ND

64

µg/Kg-dry

51.4

5/2/2006 1:56:00 AM

1,1,2,2-Tetrachloroethane

ND

64

µg/Kg-dry

51.4

5/2/2006 1:56:00 AM

1,1,2-Trichloro-1,2,2-trifluoroethane

ND

64

µg/Kg-dry

51.4

5/2/2006 1:56:00 AM

1,1,2-Trichloroethane

ND

64

µg/Kg-dry

51.4

5/2/2006 1:56:00 AM

1,1-Dichloroethane

ND

64

µg/Kg-dry

51.4

5/2/2006 1:56:00 AM

1,1-Dichloroethene

ND

64

µg/Kg-dry

51.4

5/2/2006 1:56:00 AM

1,1-Dichloropropene

ND

64

µg/Kg-dry

51.4

5/2/2006 1:56:00 AM

1,2,3-Trichlorobenzene

ND

64

µg/Kg-dry

51.4

5/2/2006 1:56:00 AM

1,2,3-Trichloropropane

ND

64

µg/Kg-dry

51.4

5/2/2006 1:56:00 AM

1,2,3-Trimethylbenzene

ND

64

µg/Kg-dry

51.4

5/2/2006 1:56:00 AM

1,2,4-Trichlorobenzene

ND

320

µg/Kg-dry

51.4

5/2/2006 1:56:00 AM

1,2,4-Trimethylbenzene

ND

64

µg/Kg-dry

51.4

5/2/2006 1:56:00 AM

1,2-Dibromo-3-chloropropane

ND

64

µg/Kg-dry

51.4

5/2/2006 1:56:00 AM

1,2-Dichlorobenzene

ND

64

µg/Kg-dry

51.4

5/2/2006 1:56:00 AM

1,2-Dichloroethane

ND

64

µg/Kg-dry

51.4

5/2/2006 1:56:00 AM

1,2-Dichloropropane

ND

64

µg/Kg-dry

51.4

5/2/2006 1:56:00 AM

1,3,5-Trimethylbenzene

ND

64

µg/Kg-dry

51.4

5/2/2006 1:56:00 AM

1,3-Dichlorobenzene

ND

64

µg/Kg-dry

51.4

5/2/2006 1:56:00 AM

1,3-Dichloropropane

ND

64

µg/Kg-dry

51.4

5/2/2006 1:56:00 AM

1,4-Dichlorobenzene

ND

64

µg/Kg-dry

51.4

5/2/2006 1:56:00 AM

2,2-Dichloropropane

ND

64

µg/Kg-dry

51.4

5/2/2006 1:56:00 AM

2-Chloroethyl vinyl ether

ND

640

µg/Kg-dry

51.4

5/2/2006 1:56:00 AM

2-Chlorotoluene

ND

64

µg/Kg-dry

51.4

5/2/2006 1:56:00 AM

2-Hexanone

ND

3,200

µg/Kg-dry

51.4

5/2/2006 1:56:00 AM

2-Methylnaphthalene

ND

320

µg/Kg-dry

51.4

5/2/2006 1:56:00 AM

2-Nitropropane

ND

260

µg/Kg-dry

51.4

5/2/2006 1:56:00 AM

4-Chlorotoluene

ND

64

µg/Kg-dry

51.4

5/2/2006 1:56:00 AM

Acetone

ND

3,200

µg/Kg-dry

51.4

5/2/2006 1:56:00 AM

Volatile Organic Compounds

Qualifiers:

Analyst: JW

SW8260B

*

Value exceeds Maximum Contaminant Level

B

Analyte detected in the associated Method Blank

E

Value above quantitation range

H

Holding times for preparation or analysis exceeded

M

Manual Integration used to determine area response

RL

Reporting Detection Limit

ND
S

Not Detected at the Reporting Limit
Spike Recovery outside accepted recovery limits

Page 27 of 66

31628 Glendale St.

Analytical Report

Livonia, Michigan 48150
TEL: 734.422.8000
FAX: 734.422.5342
Website: www.rtilab.com

(consolidated)

WO#:

0604884

Date Reported:

5/5/2006

Collection Date: 4/27/2006 12:45:00 PM

CLIENT:

PM Environmental, Inc.

Project:

7876 Van Dyke - 22-692A

Lab ID:

0604884-007

Matrix: SOIL

Client Sample ID SB-7 2-3'
Analyses

Result

RL Qual Units

Volatile Organic Compounds

DF

Date Analyzed
Analyst: JW

SW8260B

Acrylonitrile

ND

320

µg/Kg-dry

51.4

5/2/2006 1:56:00 AM

Benzene

ND

64

µg/Kg-dry

51.4

5/2/2006 1:56:00 AM

Bromobenzene

ND

64

µg/Kg-dry

51.4

5/2/2006 1:56:00 AM

Bromochloromethane

ND

64

µg/Kg-dry

51.4

5/2/2006 1:56:00 AM

Bromodichloromethane

ND

64

µg/Kg-dry

51.4

5/2/2006 1:56:00 AM

Bromoform

ND

64

µg/Kg-dry

51.4

5/2/2006 1:56:00 AM

Bromomethane

ND

320

µg/Kg-dry

51.4

5/2/2006 1:56:00 AM

Carbon disulfide

ND

320

µg/Kg-dry

51.4

5/2/2006 1:56:00 AM

Carbon tetrachloride

ND

64

µg/Kg-dry

51.4

5/2/2006 1:56:00 AM

Chlorobenzene

ND

64

µg/Kg-dry

51.4

5/2/2006 1:56:00 AM

Chloroethane

ND

320

µg/Kg-dry

51.4

5/2/2006 1:56:00 AM

Chloroform

ND

64

µg/Kg-dry

51.4

5/2/2006 1:56:00 AM

Chloromethane

ND

64

µg/Kg-dry

51.4

5/2/2006 1:56:00 AM

cis-1,2-Dichloroethene

ND

64

µg/Kg-dry

51.4

5/2/2006 1:56:00 AM

cis-1,3-Dichloropropene

ND

64

µg/Kg-dry

51.4

5/2/2006 1:56:00 AM

Dibromochloromethane

ND

64

µg/Kg-dry

51.4

5/2/2006 1:56:00 AM

Dibromomethane

ND

64

µg/Kg-dry

51.4

5/2/2006 1:56:00 AM

Dichlorodifluoromethane

ND

64

µg/Kg-dry

51.4

5/2/2006 1:56:00 AM

Dichloromethane

ND

320

µg/Kg-dry

51.4

5/2/2006 1:56:00 AM

Diethyl ether

ND

320

µg/Kg-dry

51.4

5/2/2006 1:56:00 AM

Ethyl methacrylate

ND

64

µg/Kg-dry

51.4

5/2/2006 1:56:00 AM

Ethylbenzene

ND

64

µg/Kg-dry

51.4

5/2/2006 1:56:00 AM

Ethylene dibromide

ND

64

µg/Kg-dry

51.4

5/2/2006 1:56:00 AM

Hexachlorobutadiene

ND

320

µg/Kg-dry

51.4

5/2/2006 1:56:00 AM

Hexachloroethane

ND

64

µg/Kg-dry

51.4

5/2/2006 1:56:00 AM

Isopropyl ether

ND

320

µg/Kg-dry

51.4

5/2/2006 1:56:00 AM

Isopropylbenzene

ND

64

µg/Kg-dry

51.4

5/2/2006 1:56:00 AM

m,p-Xylene

ND

130

µg/Kg-dry

51.4

5/2/2006 1:56:00 AM

Methyl ethyl ketone

ND

320

µg/Kg-dry

51.4

5/2/2006 1:56:00 AM

Methyl Iodide

ND

320

µg/Kg-dry

51.4

5/2/2006 1:56:00 AM

Methyl isobutyl ketone

ND

640

µg/Kg-dry

51.4

5/2/2006 1:56:00 AM

Methyl tert-butyl ether

ND

320

µg/Kg-dry

51.4

5/2/2006 1:56:00 AM

Naphthalene

ND

320

µg/Kg-dry

51.4

5/2/2006 1:56:00 AM

n-Butylbenzene

ND

64

µg/Kg-dry

51.4

5/2/2006 1:56:00 AM

n-Propylbenzene

ND

64

µg/Kg-dry

51.4

5/2/2006 1:56:00 AM

Qualifiers:

*

Value exceeds Maximum Contaminant Level

B

Analyte detected in the associated Method Blank

E

Value above quantitation range

H

Holding times for preparation or analysis exceeded

M

Manual Integration used to determine area response

RL

Reporting Detection Limit

ND
S

Not Detected at the Reporting Limit
Spike Recovery outside accepted recovery limits

Page 28 of 66

31628 Glendale St.

Analytical Report

Livonia, Michigan 48150
TEL: 734.422.8000
FAX: 734.422.5342
Website: www.rtilab.com

(consolidated)

WO#:

0604884

Date Reported:

5/5/2006

Collection Date: 4/27/2006 12:45:00 PM

CLIENT:

PM Environmental, Inc.

Project:

7876 Van Dyke - 22-692A

Lab ID:

0604884-007

Matrix: SOIL

Client Sample ID SB-7 2-3'
Analyses

Result

RL Qual Units

Volatile Organic Compounds

DF

Date Analyzed
Analyst: JW

SW8260B

o-Xylene

ND

64

µg/Kg-dry

51.4

5/2/2006 1:56:00 AM

p-Isopropyltoluene

ND

64

µg/Kg-dry

51.4

5/2/2006 1:56:00 AM

sec-Butylbenzene

ND

64

µg/Kg-dry

51.4

5/2/2006 1:56:00 AM

Styrene

ND

64

µg/Kg-dry

51.4

5/2/2006 1:56:00 AM

t-Butyl alcohol

ND

2,600

µg/Kg-dry

51.4

5/2/2006 1:56:00 AM

tert-Amyl Methyl Ether

ND

260

µg/Kg-dry

51.4

5/2/2006 1:56:00 AM

tert-Butyl Ethyl Ether

ND

320

µg/Kg-dry

51.4

5/2/2006 1:56:00 AM

tert-Butylbenzene

ND

64

µg/Kg-dry

51.4

5/2/2006 1:56:00 AM

Tetrachloroethene

ND

64

µg/Kg-dry

51.4

5/2/2006 1:56:00 AM

Toluene

ND

64

µg/Kg-dry

51.4

5/2/2006 1:56:00 AM

trans-1,2-Dichloroethene

ND

64

µg/Kg-dry

51.4

5/2/2006 1:56:00 AM

trans-1,3-Dichloropropene

ND

64

µg/Kg-dry

51.4

5/2/2006 1:56:00 AM

trans-1,4-Dichloro-2-butene

ND

64

µg/Kg-dry

51.4

5/2/2006 1:56:00 AM

Trichloroethene

ND

64

µg/Kg-dry

51.4

5/2/2006 1:56:00 AM

Trichlorofluoromethane

ND

64

µg/Kg-dry

51.4

5/2/2006 1:56:00 AM

Vinyl chloride

ND

51

µg/Kg-dry

51.4

5/2/2006 1:56:00 AM

Xylenes, Total

ND

190

µg/Kg-dry

51.4

5/2/2006 1:56:00 AM

Surr: 4-Bromofluorobenzene

115

70-130

%REC

51.4

5/2/2006 1:56:00 AM

Surr: Dibromofluoromethane

114

70-130

%REC

51.4

5/2/2006 1:56:00 AM

Surr: Toluene-d8

115

70-130

%REC

51.4

5/2/2006 1:56:00 AM

20

1.0

1

5/1/2006

PERCENT MOISTURE
Percent Moisture

Qualifiers:

Analyst: MT3

D2216 wt% *

Value exceeds Maximum Contaminant Level

B

Analyte detected in the associated Method Blank

E

Value above quantitation range

H

Holding times for preparation or analysis exceeded

M

Manual Integration used to determine area response

RL

Reporting Detection Limit

ND
S

Not Detected at the Reporting Limit
Spike Recovery outside accepted recovery limits

Page 29 of 66

31628 Glendale St.

Analytical Report

Livonia, Michigan 48150
TEL: 734.422.8000
FAX: 734.422.5342
Website: www.rtilab.com

(consolidated)

WO#:

0604884

Date Reported:

5/5/2006

Collection Date: 4/27/2006 1:00:00 PM

CLIENT:

PM Environmental, Inc.

Project:

7876 Van Dyke - 22-692A

Lab ID:

0604884-008

Matrix: SOIL

Client Sample ID SB-8 1-2'
Analyses

Result

RL Qual Units

DF

Polychlorinated Biphenyls

Date Analyzed
Analyst: MB

SW8082

Aroclor 1016

ND

39

µg/Kg-dry

1

5/3/2006 2:08:32 AM

Aroclor 1221

ND

39

µg/Kg-dry

1

5/3/2006 2:08:32 AM

Aroclor 1232

ND

39

µg/Kg-dry

1

5/3/2006 2:08:32 AM

Aroclor 1242

ND

39

µg/Kg-dry

1

5/3/2006 2:08:32 AM

Aroclor 1248

ND

39

µg/Kg-dry

1

5/3/2006 2:08:32 AM

Aroclor 1254

ND

39

µg/Kg-dry

1

5/3/2006 2:08:32 AM

Aroclor 1260

ND

39

µg/Kg-dry

1

5/3/2006 2:08:32 AM

Surr: Decachlorobiphenyl

83.5

70-130

%REC

1

5/3/2006 2:08:32 AM

Surr: Tetrachloro-m-xylene

72.4

70-130

%REC

1

5/3/2006 2:08:32 AM

670

440

µg/Kg-dry

20

5/1/2006 2:05:41 PM

Chromium

21,000

2,200

µg/Kg-dry

20

5/1/2006 2:05:41 PM

Lead

18,000

2,200

µg/Kg-dry

20

5/1/2006 2:05:41 PM

Metals, ICP/MS

Analyst: AB2

SW6020A

Cadmium

Polynuclear Aromatic Hydrocarbons
Semi-Volatile Organic Compounds

Analyst: JG3

SW8270C

2-Methylnaphthalene

ND

390

µg/Kg-dry

1

5/2/2006 9:06:00 PM

Acenaphthene

ND

390

µg/Kg-dry

1

5/2/2006 9:06:00 PM

Acenaphthylene

ND

390

µg/Kg-dry

1

5/2/2006 9:06:00 PM

Anthracene

ND

390

µg/Kg-dry

1

5/2/2006 9:06:00 PM

Benz(a)anthracene

ND

390

µg/Kg-dry

1

5/2/2006 9:06:00 PM

Benzo(a)pyrene

ND

390

µg/Kg-dry

1

5/2/2006 9:06:00 PM

Benzo(b)fluoranthene

ND

390

µg/Kg-dry

1

5/2/2006 9:06:00 PM

Benzo(g,h,i)perylene

ND

390

µg/Kg-dry

1

5/2/2006 9:06:00 PM

Benzo(k)fluoranthene

ND

390

µg/Kg-dry

1

5/2/2006 9:06:00 PM

Chrysene

ND

390

µg/Kg-dry

1

5/2/2006 9:06:00 PM

Dibenz(a,h)anthracene

ND

390

µg/Kg-dry

1

5/2/2006 9:06:00 PM

Fluoranthene

ND

390

µg/Kg-dry

1

5/2/2006 9:06:00 PM

Fluorene

ND

390

µg/Kg-dry

1

5/2/2006 9:06:00 PM

Indeno(1,2,3-cd)pyrene

ND

390

µg/Kg-dry

1

5/2/2006 9:06:00 PM

Naphthalene

ND

390

µg/Kg-dry

1

5/2/2006 9:06:00 PM

Phenanthrene

ND

390

µg/Kg-dry

1

5/2/2006 9:06:00 PM

Pyrene

ND

390

µg/Kg-dry

1

5/2/2006 9:06:00 PM

Surr: 2,4,6-Tribromophenol

77.6

25-93.9

%REC

1

5/2/2006 9:06:00 PM

Surr: 2-Fluorobiphenyl

89.8

26-105

%REC

1

5/2/2006 9:06:00 PM

Qualifiers:

*

Value exceeds Maximum Contaminant Level

B

Analyte detected in the associated Method Blank

E

Value above quantitation range

H

Holding times for preparation or analysis exceeded

M

Manual Integration used to determine area response

RL

Reporting Detection Limit

ND
S

Not Detected at the Reporting Limit
Spike Recovery outside accepted recovery limits

Page 30 of 66

31628 Glendale St.

Analytical Report

Livonia, Michigan 48150
TEL: 734.422.8000
FAX: 734.422.5342
Website: www.rtilab.com

(consolidated)

WO#:

0604884

Date Reported:

5/5/2006

Collection Date: 4/27/2006 1:00:00 PM

CLIENT:

PM Environmental, Inc.

Project:

7876 Van Dyke - 22-692A

Lab ID:

0604884-008

Matrix: SOIL

Client Sample ID SB-8 1-2'
Analyses

Result

RL Qual Units

Polynuclear Aromatic Hydrocarbons
Semi-Volatile Organic Compounds

DF

Date Analyzed
Analyst: JG3

SW8270C

Surr: 2-Fluorophenol

95.3

25-120

%REC

1

5/2/2006 9:06:00 PM

Surr: Nitrobenzene-d5

95.4

30.1-104

%REC

1

5/2/2006 9:06:00 PM

Surr: Phenol-d5

102

25-118

%REC

1

5/2/2006 9:06:00 PM

Surr: Terphenyl-d14

101

27.1-115

%REC

1

5/2/2006 9:06:00 PM

1,1,1,2-Tetrachloroethane

ND

62

µg/Kg-dry

53

5/2/2006 2:30:00 AM

1,1,1-Trichloroethane

ND

62

µg/Kg-dry

53

5/2/2006 2:30:00 AM

1,1,2,2-Tetrachloroethane

ND

62

µg/Kg-dry

53

5/2/2006 2:30:00 AM

1,1,2-Trichloro-1,2,2-trifluoroethane

ND

62

µg/Kg-dry

53

5/2/2006 2:30:00 AM

1,1,2-Trichloroethane

ND

62

µg/Kg-dry

53

5/2/2006 2:30:00 AM

1,1-Dichloroethane

ND

62

µg/Kg-dry

53

5/2/2006 2:30:00 AM

1,1-Dichloroethene

ND

62

µg/Kg-dry

53

5/2/2006 2:30:00 AM

1,1-Dichloropropene

ND

62

µg/Kg-dry

53

5/2/2006 2:30:00 AM

1,2,3-Trichlorobenzene

ND

62

µg/Kg-dry

53

5/2/2006 2:30:00 AM

1,2,3-Trichloropropane

ND

62

µg/Kg-dry

53

5/2/2006 2:30:00 AM

1,2,3-Trimethylbenzene

ND

62

µg/Kg-dry

53

5/2/2006 2:30:00 AM

1,2,4-Trichlorobenzene

ND

310

µg/Kg-dry

53

5/2/2006 2:30:00 AM

1,2,4-Trimethylbenzene

ND

62

µg/Kg-dry

53

5/2/2006 2:30:00 AM

1,2-Dibromo-3-chloropropane

ND

62

µg/Kg-dry

53

5/2/2006 2:30:00 AM

1,2-Dichlorobenzene

ND

62

µg/Kg-dry

53

5/2/2006 2:30:00 AM

1,2-Dichloroethane

ND

62

µg/Kg-dry

53

5/2/2006 2:30:00 AM

1,2-Dichloropropane

ND

62

µg/Kg-dry

53

5/2/2006 2:30:00 AM

1,3,5-Trimethylbenzene

ND

62

µg/Kg-dry

53

5/2/2006 2:30:00 AM

1,3-Dichlorobenzene

ND

62

µg/Kg-dry

53

5/2/2006 2:30:00 AM

1,3-Dichloropropane

ND

62

µg/Kg-dry

53

5/2/2006 2:30:00 AM

1,4-Dichlorobenzene

ND

62

µg/Kg-dry

53

5/2/2006 2:30:00 AM

2,2-Dichloropropane

ND

62

µg/Kg-dry

53

5/2/2006 2:30:00 AM

2-Chloroethyl vinyl ether

ND

620

µg/Kg-dry

53

5/2/2006 2:30:00 AM

2-Chlorotoluene

ND

62

µg/Kg-dry

53

5/2/2006 2:30:00 AM

2-Hexanone

ND

3,100

µg/Kg-dry

53

5/2/2006 2:30:00 AM

2-Methylnaphthalene

ND

310

µg/Kg-dry

53

5/2/2006 2:30:00 AM

2-Nitropropane

ND

250

µg/Kg-dry

53

5/2/2006 2:30:00 AM

4-Chlorotoluene

ND

62

µg/Kg-dry

53

5/2/2006 2:30:00 AM

Acetone

ND

3,100

µg/Kg-dry

53

5/2/2006 2:30:00 AM

Volatile Organic Compounds

Qualifiers:

Analyst: JW

SW8260B

*

Value exceeds Maximum Contaminant Level

B

Analyte detected in the associated Method Blank

E

Value above quantitation range

H

Holding times for preparation or analysis exceeded

M

Manual Integration used to determine area response

RL

Reporting Detection Limit

ND
S

Not Detected at the Reporting Limit
Spike Recovery outside accepted recovery limits

Page 31 of 66

31628 Glendale St.

Analytical Report

Livonia, Michigan 48150
TEL: 734.422.8000
FAX: 734.422.5342
Website: www.rtilab.com

(consolidated)

WO#:

0604884

Date Reported:

5/5/2006

Collection Date: 4/27/2006 1:00:00 PM

CLIENT:

PM Environmental, Inc.

Project:

7876 Van Dyke - 22-692A

Lab ID:

0604884-008

Matrix: SOIL

Client Sample ID SB-8 1-2'
Analyses

Result

RL Qual Units

Volatile Organic Compounds

DF

Date Analyzed
Analyst: JW

SW8260B

Acrylonitrile

ND

310

µg/Kg-dry

53

5/2/2006 2:30:00 AM

Benzene

ND

62

µg/Kg-dry

53

5/2/2006 2:30:00 AM

Bromobenzene

ND

62

µg/Kg-dry

53

5/2/2006 2:30:00 AM

Bromochloromethane

ND

62

µg/Kg-dry

53

5/2/2006 2:30:00 AM

Bromodichloromethane

ND

62

µg/Kg-dry

53

5/2/2006 2:30:00 AM

Bromoform

ND

62

µg/Kg-dry

53

5/2/2006 2:30:00 AM

Bromomethane

ND

310

µg/Kg-dry

53

5/2/2006 2:30:00 AM

Carbon disulfide

ND

310

µg/Kg-dry

53

5/2/2006 2:30:00 AM

Carbon tetrachloride

ND

62

µg/Kg-dry

53

5/2/2006 2:30:00 AM

Chlorobenzene

ND

62

µg/Kg-dry

53

5/2/2006 2:30:00 AM

Chloroethane

ND

310

µg/Kg-dry

53

5/2/2006 2:30:00 AM

Chloroform

ND

62

µg/Kg-dry

53

5/2/2006 2:30:00 AM

Chloromethane

ND

62

µg/Kg-dry

53

5/2/2006 2:30:00 AM

cis-1,2-Dichloroethene

ND

62

µg/Kg-dry

53

5/2/2006 2:30:00 AM

cis-1,3-Dichloropropene

ND

62

µg/Kg-dry

53

5/2/2006 2:30:00 AM

Dibromochloromethane

ND

62

µg/Kg-dry

53

5/2/2006 2:30:00 AM

Dibromomethane

ND

62

µg/Kg-dry

53

5/2/2006 2:30:00 AM

Dichlorodifluoromethane

ND

62

µg/Kg-dry

53

5/2/2006 2:30:00 AM

Dichloromethane

ND

310

µg/Kg-dry

53

5/2/2006 2:30:00 AM

Diethyl ether

ND

310

µg/Kg-dry

53

5/2/2006 2:30:00 AM

Ethyl methacrylate

ND

62

µg/Kg-dry

53

5/2/2006 2:30:00 AM

Ethylbenzene

ND

62

µg/Kg-dry

53

5/2/2006 2:30:00 AM

Ethylene dibromide

ND

62

µg/Kg-dry

53

5/2/2006 2:30:00 AM

Hexachlorobutadiene

ND

310

µg/Kg-dry

53

5/2/2006 2:30:00 AM

Hexachloroethane

ND

62

µg/Kg-dry

53

5/2/2006 2:30:00 AM

Isopropyl ether

ND

310

µg/Kg-dry

53

5/2/2006 2:30:00 AM

Isopropylbenzene

ND

62

µg/Kg-dry

53

5/2/2006 2:30:00 AM

m,p-Xylene

ND

120

µg/Kg-dry

53

5/2/2006 2:30:00 AM

Methyl ethyl ketone

ND

310

µg/Kg-dry

53

5/2/2006 2:30:00 AM

Methyl Iodide

ND

310

µg/Kg-dry

53

5/2/2006 2:30:00 AM

Methyl isobutyl ketone

ND

620

µg/Kg-dry

53

5/2/2006 2:30:00 AM

Methyl tert-butyl ether

ND

310

µg/Kg-dry

53

5/2/2006 2:30:00 AM

Naphthalene

ND

310

µg/Kg-dry

53

5/2/2006 2:30:00 AM

n-Butylbenzene

ND

62

µg/Kg-dry

53

5/2/2006 2:30:00 AM

n-Propylbenzene

ND

62

µg/Kg-dry

53

5/2/2006 2:30:00 AM

Qualifiers:

*

Value exceeds Maximum Contaminant Level

B

Analyte detected in the associated Method Blank

E

Value above quantitation range

H

Holding times for preparation or analysis exceeded

M

Manual Integration used to determine area response

RL

Reporting Detection Limit

ND
S

Not Detected at the Reporting Limit
Spike Recovery outside accepted recovery limits

Page 32 of 66

31628 Glendale St.

Analytical Report

Livonia, Michigan 48150
TEL: 734.422.8000
FAX: 734.422.5342
Website: www.rtilab.com

(consolidated)

WO#:

0604884

Date Reported:

5/5/2006

Collection Date: 4/27/2006 1:00:00 PM

CLIENT:

PM Environmental, Inc.

Project:

7876 Van Dyke - 22-692A

Lab ID:

0604884-008

Matrix: SOIL

Client Sample ID SB-8 1-2'
Analyses

Result

RL Qual Units

Volatile Organic Compounds

DF

Date Analyzed
Analyst: JW

SW8260B

o-Xylene

ND

62

µg/Kg-dry

53

5/2/2006 2:30:00 AM

p-Isopropyltoluene

ND

62

µg/Kg-dry

53

5/2/2006 2:30:00 AM

sec-Butylbenzene

ND

62

µg/Kg-dry

53

5/2/2006 2:30:00 AM

Styrene

ND

62

µg/Kg-dry

53

5/2/2006 2:30:00 AM

t-Butyl alcohol

ND

2,500

µg/Kg-dry

53

5/2/2006 2:30:00 AM

tert-Amyl Methyl Ether

ND

250

µg/Kg-dry

53

5/2/2006 2:30:00 AM

tert-Butyl Ethyl Ether

ND

310

µg/Kg-dry

53

5/2/2006 2:30:00 AM

tert-Butylbenzene

ND

62

µg/Kg-dry

53

5/2/2006 2:30:00 AM

Tetrachloroethene

ND

62

µg/Kg-dry

53

5/2/2006 2:30:00 AM

Toluene

ND

62

µg/Kg-dry

53

5/2/2006 2:30:00 AM

trans-1,2-Dichloroethene

ND

62

µg/Kg-dry

53

5/2/2006 2:30:00 AM

trans-1,3-Dichloropropene

ND

62

µg/Kg-dry

53

5/2/2006 2:30:00 AM

trans-1,4-Dichloro-2-butene

ND

62

µg/Kg-dry

53

5/2/2006 2:30:00 AM

Trichloroethene

ND

62

µg/Kg-dry

53

5/2/2006 2:30:00 AM

Trichlorofluoromethane

ND

62

µg/Kg-dry

53

5/2/2006 2:30:00 AM

Vinyl chloride

ND

49

µg/Kg-dry

53

5/2/2006 2:30:00 AM

Xylenes, Total

ND

190

µg/Kg-dry

53

5/2/2006 2:30:00 AM

Surr: 4-Bromofluorobenzene

113

70-130

%REC

53

5/2/2006 2:30:00 AM

Surr: Dibromofluoromethane

109

70-130

%REC

53

5/2/2006 2:30:00 AM

Surr: Toluene-d8

115

70-130

%REC

53

5/2/2006 2:30:00 AM

14

1.0

1

5/1/2006

PERCENT MOISTURE
Percent Moisture

Qualifiers:

Analyst: MT3

D2216 wt% *

Value exceeds Maximum Contaminant Level

B

Analyte detected in the associated Method Blank

E

Value above quantitation range

H

Holding times for preparation or analysis exceeded

M

Manual Integration used to determine area response

RL

Reporting Detection Limit

ND
S

Not Detected at the Reporting Limit
Spike Recovery outside accepted recovery limits

Page 33 of 66

31628 Glendale St.

Analytical Report

Livonia, Michigan 48150
TEL: 734.422.8000
FAX: 734.422.5342
Website: www.rtilab.com

(consolidated)

WO#:

0604884

Date Reported:

5/5/2006

Collection Date: 4/27/2006 1:20:00 PM

CLIENT:

PM Environmental, Inc.

Project:

7876 Van Dyke - 22-692A

Lab ID:

0604884-009

Matrix: SOIL

Client Sample ID SB-9 5-6'
Analyses

Result

RL Qual Units

DF

Polychlorinated Biphenyls

Date Analyzed
Analyst: MB

SW8082

Aroclor 1016

ND

40

µg/Kg-dry

1

5/3/2006 2:48:10 AM

Aroclor 1221

ND

40

µg/Kg-dry

1

5/3/2006 2:48:10 AM

Aroclor 1232

ND

40

µg/Kg-dry

1

5/3/2006 2:48:10 AM

Aroclor 1242

ND

40

µg/Kg-dry

1

5/3/2006 2:48:10 AM

Aroclor 1248

ND

40

µg/Kg-dry

1

5/3/2006 2:48:10 AM

Aroclor 1254

ND

40

µg/Kg-dry

1

5/3/2006 2:48:10 AM

Aroclor 1260

ND

40

µg/Kg-dry

1

5/3/2006 2:48:10 AM

Surr: Decachlorobiphenyl

83.9

70-130

%REC

1

5/3/2006 2:48:10 AM

Surr: Tetrachloro-m-xylene

73.1

70-130

%REC

1

5/3/2006 2:48:10 AM

590

470

µg/Kg-dry

20

5/1/2006 2:07:59 PM

Chromium

16,000

2,300

µg/Kg-dry

20

5/1/2006 2:07:59 PM

Lead

13,000

2,300

µg/Kg-dry

20

5/1/2006 2:07:59 PM

Metals, ICP/MS

Analyst: AB2

SW6020A

Cadmium

Polynuclear Aromatic Hydrocarbons
Semi-Volatile Organic Compounds

Analyst: JG3

SW8270C

2-Methylnaphthalene

ND

400

µg/Kg-dry

1

5/2/2006 9:42:00 PM

Acenaphthene

ND

400

µg/Kg-dry

1

5/2/2006 9:42:00 PM

Acenaphthylene

ND

400

µg/Kg-dry

1

5/2/2006 9:42:00 PM

Anthracene

ND

400

µg/Kg-dry

1

5/2/2006 9:42:00 PM

Benz(a)anthracene

ND

400

µg/Kg-dry

1

5/2/2006 9:42:00 PM

Benzo(a)pyrene

ND

400

µg/Kg-dry

1

5/2/2006 9:42:00 PM

Benzo(b)fluoranthene

ND

400

µg/Kg-dry

1

5/2/2006 9:42:00 PM

Benzo(g,h,i)perylene

ND

400

µg/Kg-dry

1

5/2/2006 9:42:00 PM

Benzo(k)fluoranthene

ND

400

µg/Kg-dry

1

5/2/2006 9:42:00 PM

Chrysene

ND

400

µg/Kg-dry

1

5/2/2006 9:42:00 PM

Dibenz(a,h)anthracene

ND

400

µg/Kg-dry

1

5/2/2006 9:42:00 PM

Fluoranthene

ND

400

µg/Kg-dry

1

5/2/2006 9:42:00 PM

Fluorene

ND

400

µg/Kg-dry

1

5/2/2006 9:42:00 PM

Indeno(1,2,3-cd)pyrene

ND

400

µg/Kg-dry

1

5/2/2006 9:42:00 PM

Naphthalene

ND

400

µg/Kg-dry

1

5/2/2006 9:42:00 PM

Phenanthrene

ND

400

µg/Kg-dry

1

5/2/2006 9:42:00 PM

Pyrene

ND

400

µg/Kg-dry

1

5/2/2006 9:42:00 PM

Surr: 2,4,6-Tribromophenol

83.7

25-93.9

%REC

1

5/2/2006 9:42:00 PM

Surr: 2-Fluorobiphenyl

100

26-105

%REC

1

5/2/2006 9:42:00 PM

Qualifiers:

*

Value exceeds Maximum Contaminant Level

B

Analyte detected in the associated Method Blank

E

Value above quantitation range

H

Holding times for preparation or analysis exceeded

M

Manual Integration used to determine area response

RL

Reporting Detection Limit

ND
S

Not Detected at the Reporting Limit
Spike Recovery outside accepted recovery limits

Page 34 of 66

31628 Glendale St.

Analytical Report

Livonia, Michigan 48150
TEL: 734.422.8000
FAX: 734.422.5342
Website: www.rtilab.com

(consolidated)

WO#:

0604884

Date Reported:

5/5/2006

Collection Date: 4/27/2006 1:20:00 PM

CLIENT:

PM Environmental, Inc.

Project:

7876 Van Dyke - 22-692A

Lab ID:

0604884-009

Matrix: SOIL

Client Sample ID SB-9 5-6'
Analyses

Result

RL Qual Units

Polynuclear Aromatic Hydrocarbons
Semi-Volatile Organic Compounds

DF

Date Analyzed
Analyst: JG3

SW8270C

Surr: 2-Fluorophenol

106

25-120

%REC

1

5/2/2006 9:42:00 PM

Surr: Nitrobenzene-d5

97.6

30.1-104

%REC

1

5/2/2006 9:42:00 PM

Surr: Phenol-d5

107

25-118

%REC

1

5/2/2006 9:42:00 PM

Surr: Terphenyl-d14

102

27.1-115

%REC

1

5/2/2006 9:42:00 PM

1,1,1,2-Tetrachloroethane

ND

62

µg/Kg-dry

51.9

5/2/2006 3:03:00 AM

1,1,1-Trichloroethane

ND

62

µg/Kg-dry

51.9

5/2/2006 3:03:00 AM

1,1,2,2-Tetrachloroethane

ND

62

µg/Kg-dry

51.9

5/2/2006 3:03:00 AM

1,1,2-Trichloro-1,2,2-trifluoroethane

ND

62

µg/Kg-dry

51.9

5/2/2006 3:03:00 AM

1,1,2-Trichloroethane

ND

62

µg/Kg-dry

51.9

5/2/2006 3:03:00 AM

1,1-Dichloroethane

ND

62

µg/Kg-dry

51.9

5/2/2006 3:03:00 AM

1,1-Dichloroethene

ND

62

µg/Kg-dry

51.9

5/2/2006 3:03:00 AM

1,1-Dichloropropene

ND

62

µg/Kg-dry

51.9

5/2/2006 3:03:00 AM

1,2,3-Trichlorobenzene

ND

62

µg/Kg-dry

51.9

5/2/2006 3:03:00 AM

1,2,3-Trichloropropane

ND

62

µg/Kg-dry

51.9

5/2/2006 3:03:00 AM

1,2,3-Trimethylbenzene

ND

62

µg/Kg-dry

51.9

5/2/2006 3:03:00 AM

1,2,4-Trichlorobenzene

ND

310

µg/Kg-dry

51.9

5/2/2006 3:03:00 AM

1,2,4-Trimethylbenzene

ND

62

µg/Kg-dry

51.9

5/2/2006 3:03:00 AM

1,2-Dibromo-3-chloropropane

ND

62

µg/Kg-dry

51.9

5/2/2006 3:03:00 AM

1,2-Dichlorobenzene

ND

62

µg/Kg-dry

51.9

5/2/2006 3:03:00 AM

1,2-Dichloroethane

ND

62

µg/Kg-dry

51.9

5/2/2006 3:03:00 AM

1,2-Dichloropropane

ND

62

µg/Kg-dry

51.9

5/2/2006 3:03:00 AM

1,3,5-Trimethylbenzene

ND

62

µg/Kg-dry

51.9

5/2/2006 3:03:00 AM

1,3-Dichlorobenzene

ND

62

µg/Kg-dry

51.9

5/2/2006 3:03:00 AM

1,3-Dichloropropane

ND

62

µg/Kg-dry

51.9

5/2/2006 3:03:00 AM

1,4-Dichlorobenzene

ND

62

µg/Kg-dry

51.9

5/2/2006 3:03:00 AM

2,2-Dichloropropane

ND

62

µg/Kg-dry

51.9

5/2/2006 3:03:00 AM

2-Chloroethyl vinyl ether

ND

620

µg/Kg-dry

51.9

5/2/2006 3:03:00 AM

2-Chlorotoluene

ND

62

µg/Kg-dry

51.9

5/2/2006 3:03:00 AM

2-Hexanone

ND

3,100

µg/Kg-dry

51.9

5/2/2006 3:03:00 AM

2-Methylnaphthalene

ND

310

µg/Kg-dry

51.9

5/2/2006 3:03:00 AM

2-Nitropropane

ND

250

µg/Kg-dry

51.9

5/2/2006 3:03:00 AM

4-Chlorotoluene

ND

62

µg/Kg-dry

51.9

5/2/2006 3:03:00 AM

Acetone

ND

3,100

µg/Kg-dry

51.9

5/2/2006 3:03:00 AM

Volatile Organic Compounds

Qualifiers:

Analyst: JW

SW8260B

*

Value exceeds Maximum Contaminant Level

B

Analyte detected in the associated Method Blank

E

Value above quantitation range

H

Holding times for preparation or analysis exceeded

M

Manual Integration used to determine area response

RL

Reporting Detection Limit

ND
S

Not Detected at the Reporting Limit
Spike Recovery outside accepted recovery limits

Page 35 of 66

31628 Glendale St.

Analytical Report

Livonia, Michigan 48150
TEL: 734.422.8000
FAX: 734.422.5342
Website: www.rtilab.com

(consolidated)

WO#:

0604884

Date Reported:

5/5/2006

Collection Date: 4/27/2006 1:20:00 PM

CLIENT:

PM Environmental, Inc.

Project:

7876 Van Dyke - 22-692A

Lab ID:

0604884-009

Matrix: SOIL

Client Sample ID SB-9 5-6'
Analyses

Result

RL Qual Units

Volatile Organic Compounds

DF

Date Analyzed
Analyst: JW

SW8260B

Acrylonitrile

ND

310

µg/Kg-dry

51.9

5/2/2006 3:03:00 AM

Benzene

ND

62

µg/Kg-dry

51.9

5/2/2006 3:03:00 AM

Bromobenzene

ND

62

µg/Kg-dry

51.9

5/2/2006 3:03:00 AM

Bromochloromethane

ND

62

µg/Kg-dry

51.9

5/2/2006 3:03:00 AM

Bromodichloromethane

ND

62

µg/Kg-dry

51.9

5/2/2006 3:03:00 AM

Bromoform

ND

62

µg/Kg-dry

51.9

5/2/2006 3:03:00 AM

Bromomethane

ND

310

µg/Kg-dry

51.9

5/2/2006 3:03:00 AM

Carbon disulfide

ND

310

µg/Kg-dry

51.9

5/2/2006 3:03:00 AM

Carbon tetrachloride

ND

62

µg/Kg-dry

51.9

5/2/2006 3:03:00 AM

Chlorobenzene

ND

62

µg/Kg-dry

51.9

5/2/2006 3:03:00 AM

Chloroethane

ND

310

µg/Kg-dry

51.9

5/2/2006 3:03:00 AM

Chloroform

ND

62

µg/Kg-dry

51.9

5/2/2006 3:03:00 AM

Chloromethane

ND

62

µg/Kg-dry

51.9

5/2/2006 3:03:00 AM

cis-1,2-Dichloroethene

ND

62

µg/Kg-dry

51.9

5/2/2006 3:03:00 AM

cis-1,3-Dichloropropene

ND

62

µg/Kg-dry

51.9

5/2/2006 3:03:00 AM

Dibromochloromethane

ND

62

µg/Kg-dry

51.9

5/2/2006 3:03:00 AM

Dibromomethane

ND

62

µg/Kg-dry

51.9

5/2/2006 3:03:00 AM

Dichlorodifluoromethane

ND

62

µg/Kg-dry

51.9

5/2/2006 3:03:00 AM

Dichloromethane

ND

310

µg/Kg-dry

51.9

5/2/2006 3:03:00 AM

Diethyl ether

ND

310

µg/Kg-dry

51.9

5/2/2006 3:03:00 AM

Ethyl methacrylate

ND

62

µg/Kg-dry

51.9

5/2/2006 3:03:00 AM

Ethylbenzene

ND

62

µg/Kg-dry

51.9

5/2/2006 3:03:00 AM

Ethylene dibromide

ND

62

µg/Kg-dry

51.9

5/2/2006 3:03:00 AM

Hexachlorobutadiene

ND

310

µg/Kg-dry

51.9

5/2/2006 3:03:00 AM

Hexachloroethane

ND

62

µg/Kg-dry

51.9

5/2/2006 3:03:00 AM

Isopropyl ether

ND

310

µg/Kg-dry

51.9

5/2/2006 3:03:00 AM

Isopropylbenzene

ND

62

µg/Kg-dry

51.9

5/2/2006 3:03:00 AM

m,p-Xylene

ND

120

µg/Kg-dry

51.9

5/2/2006 3:03:00 AM

Methyl ethyl ketone

ND

310

µg/Kg-dry

51.9

5/2/2006 3:03:00 AM

Methyl Iodide

ND

310

µg/Kg-dry

51.9

5/2/2006 3:03:00 AM

Methyl isobutyl ketone

ND

620

µg/Kg-dry

51.9

5/2/2006 3:03:00 AM

Methyl tert-butyl ether

ND

310

µg/Kg-dry

51.9

5/2/2006 3:03:00 AM

Naphthalene

ND

310

µg/Kg-dry

51.9

5/2/2006 3:03:00 AM

n-Butylbenzene

ND

62

µg/Kg-dry

51.9

5/2/2006 3:03:00 AM

n-Propylbenzene

ND

62

µg/Kg-dry

51.9

5/2/2006 3:03:00 AM

Qualifiers:

*

Value exceeds Maximum Contaminant Level

B

Analyte detected in the associated Method Blank

E

Value above quantitation range

H

Holding times for preparation or analysis exceeded

M

Manual Integration used to determine area response

RL

Reporting Detection Limit

ND
S

Not Detected at the Reporting Limit
Spike Recovery outside accepted recovery limits

Page 36 of 66

31628 Glendale St.

Analytical Report

Livonia, Michigan 48150
TEL: 734.422.8000
FAX: 734.422.5342
Website: www.rtilab.com

(consolidated)

WO#:

0604884

Date Reported:

5/5/2006

Collection Date: 4/27/2006 1:20:00 PM

CLIENT:

PM Environmental, Inc.

Project:

7876 Van Dyke - 22-692A

Lab ID:

0604884-009

Matrix: SOIL

Client Sample ID SB-9 5-6'
Analyses

Result

RL Qual Units

Volatile Organic Compounds

DF

Date Analyzed
Analyst: JW

SW8260B

o-Xylene

ND

62

µg/Kg-dry

51.9

5/2/2006 3:03:00 AM

p-Isopropyltoluene

ND

62

µg/Kg-dry

51.9

5/2/2006 3:03:00 AM

sec-Butylbenzene

ND

62

µg/Kg-dry

51.9

5/2/2006 3:03:00 AM

Styrene

ND

62

µg/Kg-dry

51.9

5/2/2006 3:03:00 AM

t-Butyl alcohol

ND

2,500

µg/Kg-dry

51.9

5/2/2006 3:03:00 AM

tert-Amyl Methyl Ether

ND

250

µg/Kg-dry

51.9

5/2/2006 3:03:00 AM

tert-Butyl Ethyl Ether

ND

310

µg/Kg-dry

51.9

5/2/2006 3:03:00 AM

tert-Butylbenzene

ND

62

µg/Kg-dry

51.9

5/2/2006 3:03:00 AM

Tetrachloroethene

ND

62

µg/Kg-dry

51.9

5/2/2006 3:03:00 AM

Toluene

ND

62

µg/Kg-dry

51.9

5/2/2006 3:03:00 AM

trans-1,2-Dichloroethene

ND

62

µg/Kg-dry

51.9

5/2/2006 3:03:00 AM

trans-1,3-Dichloropropene

ND

62

µg/Kg-dry

51.9

5/2/2006 3:03:00 AM

trans-1,4-Dichloro-2-butene

ND

62

µg/Kg-dry

51.9

5/2/2006 3:03:00 AM

Trichloroethene

ND

62

µg/Kg-dry

51.9

5/2/2006 3:03:00 AM

Trichlorofluoromethane

ND

62

µg/Kg-dry

51.9

5/2/2006 3:03:00 AM

Vinyl chloride

ND

50

µg/Kg-dry

51.9

5/2/2006 3:03:00 AM

Xylenes, Total

ND

190

µg/Kg-dry

51.9

5/2/2006 3:03:00 AM

Surr: 4-Bromofluorobenzene

115

70-130

%REC

51.9

5/2/2006 3:03:00 AM

Surr: Dibromofluoromethane

112

70-130

%REC

51.9

5/2/2006 3:03:00 AM

Surr: Toluene-d8

107

70-130

%REC

51.9

5/2/2006 3:03:00 AM

17

1.0

1

5/1/2006

PERCENT MOISTURE
Percent Moisture

Qualifiers:

Analyst: MT3

D2216 wt% *

Value exceeds Maximum Contaminant Level

B

Analyte detected in the associated Method Blank

E

Value above quantitation range

H

Holding times for preparation or analysis exceeded

M

Manual Integration used to determine area response

RL

Reporting Detection Limit

ND
S

Not Detected at the Reporting Limit
Spike Recovery outside accepted recovery limits

Page 37 of 66

31628 Glendale St.

Analytical Report

Livonia, Michigan 48150
TEL: 734.422.8000
FAX: 734.422.5342
Website: www.rtilab.com

(consolidated)

WO#:

0604884

Date Reported:

5/5/2006

Collection Date: 4/27/2006 1:45:00 PM

CLIENT:

PM Environmental, Inc.

Project:

7876 Van Dyke - 22-692A

Lab ID:

0604884-010

Matrix: SOIL

Client Sample ID SB-10 1-2'
Analyses

Result

RL Qual Units

DF

Polychlorinated Biphenyls

Date Analyzed
Analyst: MB

SW8082

Aroclor 1016

ND

38

µg/Kg-dry

1

5/3/2006 3:27:47 AM

Aroclor 1221

ND

38

µg/Kg-dry

1

5/3/2006 3:27:47 AM

Aroclor 1232

ND

38

µg/Kg-dry

1

5/3/2006 3:27:47 AM

Aroclor 1242

ND

38

µg/Kg-dry

1

5/3/2006 3:27:47 AM

Aroclor 1248

ND

38

µg/Kg-dry

1

5/3/2006 3:27:47 AM

Aroclor 1254

ND

38

µg/Kg-dry

1

5/3/2006 3:27:47 AM

Aroclor 1260

ND

38

µg/Kg-dry

1

5/3/2006 3:27:47 AM

Surr: Decachlorobiphenyl

84.3

70-130

%REC

1

5/3/2006 3:27:47 AM

Surr: Tetrachloro-m-xylene

73.1

70-130

%REC

1

5/3/2006 3:27:47 AM

790

450

µg/Kg-dry

20

5/1/2006 2:10:17 PM

Chromium

16,000

2,300

µg/Kg-dry

20

5/1/2006 2:10:17 PM

Lead

18,000

2,300

µg/Kg-dry

20

5/1/2006 2:10:17 PM

Metals, ICP/MS

Analyst: AB2

SW6020A

Cadmium

Polynuclear Aromatic Hydrocarbons
Semi-Volatile Organic Compounds

Analyst: JG3

SW8270C

2-Methylnaphthalene

ND

380

µg/Kg-dry

1

5/2/2006 10:19:00 PM

Acenaphthene

ND

380

µg/Kg-dry

1

5/2/2006 10:19:00 PM

Acenaphthylene

ND

380

µg/Kg-dry

1

5/2/2006 10:19:00 PM

Anthracene

ND

380

µg/Kg-dry

1

5/2/2006 10:19:00 PM

Benz(a)anthracene

ND

380

µg/Kg-dry

1

5/2/2006 10:19:00 PM

Benzo(a)pyrene

ND

380

µg/Kg-dry

1

5/2/2006 10:19:00 PM

Benzo(b)fluoranthene

ND

380

µg/Kg-dry

1

5/2/2006 10:19:00 PM

Benzo(g,h,i)perylene

ND

380

µg/Kg-dry

1

5/2/2006 10:19:00 PM

Benzo(k)fluoranthene

ND

380

µg/Kg-dry

1

5/2/2006 10:19:00 PM

Chrysene

ND

380

µg/Kg-dry

1

5/2/2006 10:19:00 PM

Dibenz(a,h)anthracene

ND

380

µg/Kg-dry

1

5/2/2006 10:19:00 PM

Fluoranthene

ND

380

µg/Kg-dry

1

5/2/2006 10:19:00 PM

Fluorene

ND

380

µg/Kg-dry

1

5/2/2006 10:19:00 PM

Indeno(1,2,3-cd)pyrene

ND

380

µg/Kg-dry

1

5/2/2006 10:19:00 PM

Naphthalene

ND

380

µg/Kg-dry

1

5/2/2006 10:19:00 PM

Phenanthrene

ND

380

µg/Kg-dry

1

5/2/2006 10:19:00 PM

Pyrene

ND

380

µg/Kg-dry

1

5/2/2006 10:19:00 PM

Surr: 2,4,6-Tribromophenol

91.6

25-93.9

%REC

1

5/2/2006 10:19:00 PM

Surr: 2-Fluorobiphenyl

82.4

26-105

%REC

1

5/2/2006 10:19:00 PM

Qualifiers:

*

Value exceeds Maximum Contaminant Level

B

Analyte detected in the associated Method Blank

E

Value above quantitation range

H

Holding times for preparation or analysis exceeded

M

Manual Integration used to determine area response

RL

Reporting Detection Limit

ND
S

Not Detected at the Reporting Limit
Spike Recovery outside accepted recovery limits

Page 38 of 66

31628 Glendale St.

Analytical Report

Livonia, Michigan 48150
TEL: 734.422.8000
FAX: 734.422.5342
Website: www.rtilab.com

(consolidated)

WO#:

0604884

Date Reported:

5/5/2006

Collection Date: 4/27/2006 1:45:00 PM

CLIENT:

PM Environmental, Inc.

Project:

7876 Van Dyke - 22-692A

Lab ID:

0604884-010

Matrix: SOIL

Client Sample ID SB-10 1-2'
Analyses

Result

RL Qual Units

Polynuclear Aromatic Hydrocarbons
Semi-Volatile Organic Compounds

DF

Date Analyzed
Analyst: JG3

SW8270C

Surr: 2-Fluorophenol

95.9

25-120

%REC

1

5/2/2006 10:19:00 PM

Surr: Nitrobenzene-d5

33.9

30.1-104

%REC

1

5/2/2006 10:19:00 PM

Surr: Phenol-d5

102

25-118

%REC

1

5/2/2006 10:19:00 PM

Surr: Terphenyl-d14

107

27.1-115

%REC

1

5/2/2006 10:19:00 PM

1,1,1,2-Tetrachloroethane

ND

63

µg/Kg-dry

55.1

5/2/2006 3:37:00 AM

1,1,1-Trichloroethane

ND

63

µg/Kg-dry

55.1

5/2/2006 3:37:00 AM

1,1,2,2-Tetrachloroethane

ND

63

µg/Kg-dry

55.1

5/2/2006 3:37:00 AM

1,1,2-Trichloro-1,2,2-trifluoroethane

ND

63

µg/Kg-dry

55.1

5/2/2006 3:37:00 AM

1,1,2-Trichloroethane

ND

63

µg/Kg-dry

55.1

5/2/2006 3:37:00 AM

1,1-Dichloroethane

ND

63

µg/Kg-dry

55.1

5/2/2006 3:37:00 AM

1,1-Dichloroethene

ND

63

µg/Kg-dry

55.1

5/2/2006 3:37:00 AM

1,1-Dichloropropene

ND

63

µg/Kg-dry

55.1

5/2/2006 3:37:00 AM

1,2,3-Trichlorobenzene

ND

63

µg/Kg-dry

55.1

5/2/2006 3:37:00 AM

1,2,3-Trichloropropane

ND

63

µg/Kg-dry

55.1

5/2/2006 3:37:00 AM

1,2,3-Trimethylbenzene

ND

63

µg/Kg-dry

55.1

5/2/2006 3:37:00 AM

1,2,4-Trichlorobenzene

ND

320

µg/Kg-dry

55.1

5/2/2006 3:37:00 AM

1,2,4-Trimethylbenzene

ND

63

µg/Kg-dry

55.1

5/2/2006 3:37:00 AM

1,2-Dibromo-3-chloropropane

ND

63

µg/Kg-dry

55.1

5/2/2006 3:37:00 AM

1,2-Dichlorobenzene

ND

63

µg/Kg-dry

55.1

5/2/2006 3:37:00 AM

1,2-Dichloroethane

ND

63

µg/Kg-dry

55.1

5/2/2006 3:37:00 AM

1,2-Dichloropropane

ND

63

µg/Kg-dry

55.1

5/2/2006 3:37:00 AM

1,3,5-Trimethylbenzene

ND

63

µg/Kg-dry

55.1

5/2/2006 3:37:00 AM

1,3-Dichlorobenzene

ND

63

µg/Kg-dry

55.1

5/2/2006 3:37:00 AM

1,3-Dichloropropane

ND

63

µg/Kg-dry

55.1

5/2/2006 3:37:00 AM

1,4-Dichlorobenzene

ND

63

µg/Kg-dry

55.1

5/2/2006 3:37:00 AM

2,2-Dichloropropane

ND

63

µg/Kg-dry

55.1

5/2/2006 3:37:00 AM

2-Chloroethyl vinyl ether

ND

630

µg/Kg-dry

55.1

5/2/2006 3:37:00 AM

2-Chlorotoluene

ND

63

µg/Kg-dry

55.1

5/2/2006 3:37:00 AM

2-Hexanone

ND

3,200

µg/Kg-dry

55.1

5/2/2006 3:37:00 AM

2-Methylnaphthalene

ND

320

µg/Kg-dry

55.1

5/2/2006 3:37:00 AM

2-Nitropropane

ND

250

µg/Kg-dry

55.1

5/2/2006 3:37:00 AM

4-Chlorotoluene

ND

63

µg/Kg-dry

55.1

5/2/2006 3:37:00 AM

Acetone

ND

3,200

µg/Kg-dry

55.1

5/2/2006 3:37:00 AM

Volatile Organic Compounds

Qualifiers:

Analyst: JW

SW8260B

*

Value exceeds Maximum Contaminant Level

B

Analyte detected in the associated Method Blank

E

Value above quantitation range

H

Holding times for preparation or analysis exceeded

M

Manual Integration used to determine area response

RL

Reporting Detection Limit

ND
S

Not Detected at the Reporting Limit
Spike Recovery outside accepted recovery limits

Page 39 of 66

31628 Glendale St.

Analytical Report

Livonia, Michigan 48150
TEL: 734.422.8000
FAX: 734.422.5342
Website: www.rtilab.com

(consolidated)

WO#:

0604884

Date Reported:

5/5/2006

Collection Date: 4/27/2006 1:45:00 PM

CLIENT:

PM Environmental, Inc.

Project:

7876 Van Dyke - 22-692A

Lab ID:

0604884-010

Matrix: SOIL

Client Sample ID SB-10 1-2'
Analyses

Result

RL Qual Units

Volatile Organic Compounds

DF

Date Analyzed
Analyst: JW

SW8260B

Acrylonitrile

ND

320

µg/Kg-dry

55.1

5/2/2006 3:37:00 AM

Benzene

ND

63

µg/Kg-dry

55.1

5/2/2006 3:37:00 AM

Bromobenzene

ND

63

µg/Kg-dry

55.1

5/2/2006 3:37:00 AM

Bromochloromethane

ND

63

µg/Kg-dry

55.1

5/2/2006 3:37:00 AM

Bromodichloromethane

ND

63

µg/Kg-dry

55.1

5/2/2006 3:37:00 AM

Bromoform

ND

63

µg/Kg-dry

55.1

5/2/2006 3:37:00 AM

Bromomethane

ND

320

µg/Kg-dry

55.1

5/2/2006 3:37:00 AM

Carbon disulfide

ND

320

µg/Kg-dry

55.1

5/2/2006 3:37:00 AM

Carbon tetrachloride

ND

63

µg/Kg-dry

55.1

5/2/2006 3:37:00 AM

Chlorobenzene

ND

63

µg/Kg-dry

55.1

5/2/2006 3:37:00 AM

Chloroethane

ND

320

µg/Kg-dry

55.1

5/2/2006 3:37:00 AM

Chloroform

ND

63

µg/Kg-dry

55.1

5/2/2006 3:37:00 AM

Chloromethane

ND

63

µg/Kg-dry

55.1

5/2/2006 3:37:00 AM

cis-1,2-Dichloroethene

ND

63

µg/Kg-dry

55.1

5/2/2006 3:37:00 AM

cis-1,3-Dichloropropene

ND

63

µg/Kg-dry

55.1

5/2/2006 3:37:00 AM

Dibromochloromethane

ND

63

µg/Kg-dry

55.1

5/2/2006 3:37:00 AM

Dibromomethane

ND

63

µg/Kg-dry

55.1

5/2/2006 3:37:00 AM

Dichlorodifluoromethane

ND

63

µg/Kg-dry

55.1

5/2/2006 3:37:00 AM

Dichloromethane

ND

320

µg/Kg-dry

55.1

5/2/2006 3:37:00 AM

Diethyl ether

ND

320

µg/Kg-dry

55.1

5/2/2006 3:37:00 AM

Ethyl methacrylate

ND

63

µg/Kg-dry

55.1

5/2/2006 3:37:00 AM

Ethylbenzene

ND

63

µg/Kg-dry

55.1

5/2/2006 3:37:00 AM

Ethylene dibromide

ND

63

µg/Kg-dry

55.1

5/2/2006 3:37:00 AM

Hexachlorobutadiene

ND

320

µg/Kg-dry

55.1

5/2/2006 3:37:00 AM

Hexachloroethane

ND

63

µg/Kg-dry

55.1

5/2/2006 3:37:00 AM

Isopropyl ether

ND

320

µg/Kg-dry

55.1

5/2/2006 3:37:00 AM

Isopropylbenzene

ND

63

µg/Kg-dry

55.1

5/2/2006 3:37:00 AM

m,p-Xylene

ND

130

µg/Kg-dry

55.1

5/2/2006 3:37:00 AM

Methyl ethyl ketone

ND

320

µg/Kg-dry

55.1

5/2/2006 3:37:00 AM

Methyl Iodide

ND

320

µg/Kg-dry

55.1

5/2/2006 3:37:00 AM

Methyl isobutyl ketone

ND

630

µg/Kg-dry

55.1

5/2/2006 3:37:00 AM

Methyl tert-butyl ether

ND

320

µg/Kg-dry

55.1

5/2/2006 3:37:00 AM

Naphthalene

ND

320

µg/Kg-dry

55.1

5/2/2006 3:37:00 AM

n-Butylbenzene

ND

63

µg/Kg-dry

55.1

5/2/2006 3:37:00 AM

n-Propylbenzene

ND

63

µg/Kg-dry

55.1

5/2/2006 3:37:00 AM

Qualifiers:

*

Value exceeds Maximum Contaminant Level

B

Analyte detected in the associated Method Blank

E

Value above quantitation range

H

Holding times for preparation or analysis exceeded

M

Manual Integration used to determine area response

RL

Reporting Detection Limit

ND
S

Not Detected at the Reporting Limit
Spike Recovery outside accepted recovery limits

Page 40 of 66

31628 Glendale St.

Analytical Report

Livonia, Michigan 48150
TEL: 734.422.8000
FAX: 734.422.5342
Website: www.rtilab.com

(consolidated)

WO#:

0604884

Date Reported:

5/5/2006

Collection Date: 4/27/2006 1:45:00 PM

CLIENT:

PM Environmental, Inc.

Project:

7876 Van Dyke - 22-692A

Lab ID:

0604884-010

Matrix: SOIL

Client Sample ID SB-10 1-2'
Analyses

Result

RL Qual Units

Volatile Organic Compounds

DF

Date Analyzed
Analyst: JW

SW8260B

o-Xylene

ND

63

µg/Kg-dry

55.1

5/2/2006 3:37:00 AM

p-Isopropyltoluene

ND

63

µg/Kg-dry

55.1

5/2/2006 3:37:00 AM

sec-Butylbenzene

ND

63

µg/Kg-dry

55.1

5/2/2006 3:37:00 AM

Styrene

ND

63

µg/Kg-dry

55.1

5/2/2006 3:37:00 AM

t-Butyl alcohol

ND

2,500

µg/Kg-dry

55.1

5/2/2006 3:37:00 AM

tert-Amyl Methyl Ether

ND

250

µg/Kg-dry

55.1

5/2/2006 3:37:00 AM

tert-Butyl Ethyl Ether

ND

320

µg/Kg-dry

55.1

5/2/2006 3:37:00 AM

tert-Butylbenzene

ND

63

µg/Kg-dry

55.1

5/2/2006 3:37:00 AM

Tetrachloroethene

ND

63

µg/Kg-dry

55.1

5/2/2006 3:37:00 AM

Toluene

ND

63

µg/Kg-dry

55.1

5/2/2006 3:37:00 AM

trans-1,2-Dichloroethene

ND

63

µg/Kg-dry

55.1

5/2/2006 3:37:00 AM

trans-1,3-Dichloropropene

ND

63

µg/Kg-dry

55.1

5/2/2006 3:37:00 AM

trans-1,4-Dichloro-2-butene

ND

63

µg/Kg-dry

55.1

5/2/2006 3:37:00 AM

Trichloroethene

ND

63

µg/Kg-dry

55.1

5/2/2006 3:37:00 AM

Trichlorofluoromethane

ND

63

µg/Kg-dry

55.1

5/2/2006 3:37:00 AM

Vinyl chloride

ND

51

µg/Kg-dry

55.1

5/2/2006 3:37:00 AM

Xylenes, Total

ND

190

µg/Kg-dry

55.1

5/2/2006 3:37:00 AM

Surr: 4-Bromofluorobenzene

114

70-130

%REC

55.1

5/2/2006 3:37:00 AM

Surr: Dibromofluoromethane

113

70-130

%REC

55.1

5/2/2006 3:37:00 AM

Surr: Toluene-d8

112

70-130

%REC

55.1

5/2/2006 3:37:00 AM

13

1.0

1

5/1/2006

PERCENT MOISTURE
Percent Moisture

Qualifiers:

Analyst: MT3

D2216 wt% *

Value exceeds Maximum Contaminant Level

B

Analyte detected in the associated Method Blank

E

Value above quantitation range

H

Holding times for preparation or analysis exceeded

M

Manual Integration used to determine area response

RL

Reporting Detection Limit

ND
S

Not Detected at the Reporting Limit
Spike Recovery outside accepted recovery limits

Page 41 of 66

Date: 5/5/2006

RTI Laboratories, Inc.
PM Environmental, Inc.
0604884
7876 Van Dyke - 22-692A

CLIENT:
Work Order:
Project:

Sample ID: 0604884-001C-MS
Client ID:

SB-1 1-2'

QC SUMMARY REPORT
TestCode: SW_6020S

SampType: MS

TestCode: SW_6020S

Batch ID: 2819

Analyte

Units: µg/Kg-dry

Prep Date:

TestNo: SW6020A

Analysis Date:

Result

PQL

SPK value

SPK Ref Val

%REC

4/29/2006

RunNo: 5946

5/1/2006

SeqNo: 88320

LowLimit

HighLimit

RPD Ref Val

%RPD

RPDLimit

Qual

Aluminum

ND

2,200

55,080

0

0

75

125

S

Antimony

ND

660

55,080

0

0

75

125

S

Arsenic

ND

220

55,080

0

0

75

125

S

Barium

ND

2,200

55,080

0

0

75

125

S

Beryllium

ND

1,100

55,080

0

0

75

125

S

Boron

ND

11,000

55,080

0

0

75

125

S

61,000

440

55,080

475.1

110

75

125

ND

110,000

550,800

0

0

75

125

76,000

2,200

55,080

13,210

114

75

125

Cadmium
Calcium
Chromium

S

Cobalt

ND

1,100

55,080

0

0

75

125

S

Copper

ND

2,200

55,080

0

0

75

125

S
S

Iron

ND

44,000

55,080

0

0

75

125

63,000

2,200

55,080

6,626

103

75

125

Magnesium

ND

55,000

550,800

0

0

75

125

S

Manganese
Molybdenum

ND
ND

2,200
2,200

55,080
55,080

0
0

0
0

75
75

125
125

S
S

Nickel

ND

2,200

55,080

0

0

75

125

S

Potassium

ND

44,000

550,800

0

0

75

125

S

Selenium

ND

440

55,080

0

0

75

125

S

Silicon

ND

110,000

550,800

0

0

75

125

S

Silver

ND

220

55,080

0

0

75

125

S

Sodium

ND

66,000

550,800

0

0

75

125

S

Thallium

ND

1,100

55,080

0

0

75

125

S

Titanium

ND

22,000

55,080

0

0

75

125

S

Vanadium

ND

2,200

55,080

0

0

75

125

S

Zinc

ND

2,200

55,080

0

0

75

125

S

Lead

Qualifiers:

E
ND
S

Value above quantitation range

H

Holding times for preparation or analysis exceeded

M

Manual Integration used to determine area response

Not Detected at the Reporting Limit

R

RPD outside accepted recovery limits

RL

Reporting Detection Limit

Spike Recovery outside accepted recovery limits

Page 42 of 66

PM Environmental, Inc.
0604884
7876 Van Dyke - 22-692A

CLIENT:
Work Order:
Project:

Sample ID: 0604884-001C-MSD
Client ID:

SB-1 1-2'

QC SUMMARY REPORT
TestCode: SW_6020S

SampType: MSD

TestCode: SW_6020S

Batch ID: 2819

Analyte

Units: µg/Kg-dry

Prep Date:

TestNo: SW6020A

Analysis Date:

Result

PQL

SPK value

SPK Ref Val

Aluminum

ND

2,100

52,500

0

Antimony

ND

630

52,500

0

Arsenic

ND

210

52,500

Barium

ND

2,100

Beryllium

ND

Boron

RunNo: 5946

5/1/2006

SeqNo: 88323

LowLimit

HighLimit

RPD Ref Val

%RPD

RPDLimit

0

75

125

0

0

25

S

0

75

125

0

0

25

S

0

0

75

125

0

0

25

S

52,500

0

0

75

125

0

0

25

S

1,100

52,500

0

0

75

125

0

0

25

S

ND

11,000

52,500

0

0

75

125

0

0

25

S

58,000

Cadmium

420

52,500

475.1

109

75

125

54,310

5.73

25

Calcium

%REC

4/29/2006

Qual

ND

110,000

525,000

0

0

75

125

0

0

25

74,000

2,100

52,500

13,210

116

75

125

67,790

8.57

25

Cobalt

ND

1,100

52,500

0

0

75

125

0

0

25

S

Copper

ND

2,100

52,500

0

0

75

125

0

0

25

S

Iron

ND

42,000

52,500

0

0

75

125

0

0

25

S

61,000

2,100

52,500

6,626

104

75

125

56,320

8.73

25

Magnesium

ND

53,000

525,000

0

0

75

125

0

0

25

S

Manganese

ND

2,100

52,500

0

0

75

125

0

0

25

S

Molybdenum
Nickel

ND
ND

2,100
2,100

52,500
52,500

0
0

0
0

75
75

125
125

0
0

0
0

25
25

S
S

Potassium

ND

42,000

525,000

0

0

75

125

0

0

25

S

Selenium

ND

420

52,500

0

0

75

125

0

0

25

S

Silicon

ND

110,000

525,000

0

0

75

125

0

0

25

S

Silver

ND

210

52,500

0

0

75

125

0

0

25

S

Sodium

ND

63,000

525,000

0

0

75

125

0

0

25

S

Thallium

ND

1,100

52,500

0

0

75

125

0

0

25

S

Titanium

ND

21,000

52,500

0

0

75

125

0

0

25

S

Vanadium

ND

2,100

52,500

0

0

75

125

0

0

25

S

Zinc

ND

2,100

52,500

0

0

75

125

0

0

25

S

Chromium

Lead

Sample ID: LCS-2819
Client ID:

LCSS

SampType: LCS
Batch ID: 2819

Analyte
Qualifiers:

Result
E
ND
S

TestCode: SW_6020S

Units: µg/Kg

Prep Date:

TestNo: SW6020A
PQL

SPK value

Analysis Date:
SPK Ref Val

%REC

LowLimit

4/29/2006

RunNo: 5946

5/1/2006

S

SeqNo: 88358

HighLimit

RPD Ref Val

%RPD

RPDLimit

Value above quantitation range

H

Holding times for preparation or analysis exceeded

M

Manual Integration used to determine area response

Not Detected at the Reporting Limit

R

RPD outside accepted recovery limits

RL

Reporting Detection Limit

Qual

Spike Recovery outside accepted recovery limits

Page 43 of 66

PM Environmental, Inc.
0604884
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CLIENT:
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Project:

Sample ID: LCS-2819
Client ID:

LCSS

QC SUMMARY REPORT
TestCode: SW_6020S

SampType: LCS
Batch ID: 2819

Analyte

TestCode: SW_6020S

Units: µg/Kg

Prep Date:

TestNo: SW6020A

Result

PQL

Analysis Date:

SPK value

SPK Ref Val

%REC

4/29/2006

RunNo: 5946

5/1/2006

SeqNo: 88358

LowLimit

HighLimit

Cadmium

1,000

8.0

1,000

0

103

80

1,000

40

1,000

0

101

80

1,000

40

1,000

0

102

80

RPDLimit

Qual

120

Lead

%RPD

120

Chromium

RPD Ref Val

120

Sample ID: MB-2819
Client ID:

PBS

SampType: MBLK

TestCode: SW_6020S

Batch ID: 2819

TestNo: SW6020A

Analyte

Result

PQL

Cadmium

ND
ND
ND

Analysis Date:
SPK Ref Val

%REC

LowLimit

4/29/2006

RunNo: 5946

5/1/2006

SeqNo: 88360

HighLimit

RPD Ref Val

%RPD

RPDLimit

Qual

2.0

Lead

Prep Date:

0.40

Chromium

SPK value

Units: µg/Kg

2.0

Qualifiers:

E
ND
S

Value above quantitation range

H

Holding times for preparation or analysis exceeded

M

Manual Integration used to determine area response

Not Detected at the Reporting Limit

R

RPD outside accepted recovery limits

RL

Reporting Detection Limit

Spike Recovery outside accepted recovery limits

Page 44 of 66

PM Environmental, Inc.
0604884
7876 Van Dyke - 22-692A

CLIENT:
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Project:

Sample ID: lcs-2826
Client ID:

QC SUMMARY REPORT
TestCode: SW_8082S

SampType: lcs

LCSS

TestCode: sw_8082s

Batch ID: 2826

Analyte

Units: µg/Kg

Prep Date:

Result

PQL

SPK value

SPK Ref Val

%REC

RunNo: 6070

Analysis Date:

TestNo: SW8082

5/1/2006
5/2/2006

SeqNo: 90033

LowLimit

HighLimit

Aroclor 1016

130

33

166.7

0

79.7

70

130

33

166.7

0

77.2

70

130

33

166.7

0

79.8

70

130

33

166.7

0

76.5

70

130

AROCLOR-1016-3

140

33

166.7

0

81.9

70

130

AROCLOR-1016-4

140

33

166.7

0

81.7

70

130

AROCLOR-1016-5

130

33

166.7

0

78.6

70

130

AROCLOR-1260-1

130

33

166.7

0

77.7

70

130

AROCLOR-1260-2

130

33

166.7

0

78.0

70

130

AROCLOR-1260-3

130

33

166.7

0

78.5

70

130

AROCLOR-1260-4

130

33

166.7

0

75.6

70

130

AROCLOR-1260-5

130

33

166.7

0

76.0

70

Qual

130

AROCLOR-1016-2

RPDLimit

130

AROCLOR-1016-1

%RPD

130

Aroclor 1260

RPD Ref Val

130

Surr: Decachlorobiphenyl

6.8

8.300

81.4

70

130

Surr: Tetrachloro-m-xylene

5.9

8.300

70.9

70

130

Prep Date:

5/1/2006

RunNo: 6070

Analysis Date:

5/2/2006

SeqNo: 90034

Sample ID: mb-2826
Client ID:

PBS

SampType: mblk
Batch ID: 2826

Analyte

TestCode: sw_8082s

Units: µg/Kg

TestNo: SW8082

Result

PQL

Aroclor 1016

ND
ND
ND
ND
ND
ND
ND
ND
ND

33

AROCLOR-1016-3

ND

33

AROCLOR-1016-4

ND

33

AROCLOR-1016-5

ND

Qual

33

AROCLOR-1016-2

RPDLimit

33

AROCLOR-1016-1

%RPD

33

Aroclor 1260

RPD Ref Val

33

Aroclor 1254

HighLimit

33

Aroclor 1248

LowLimit

33

Aroclor 1242

%REC

33

Aroclor 1232

SPK Ref Val

33

Aroclor 1221

SPK value

33

Qualifiers:

E
ND
S

Value above quantitation range

H

Holding times for preparation or analysis exceeded

M

Manual Integration used to determine area response

Not Detected at the Reporting Limit

R

RPD outside accepted recovery limits

RL

Reporting Detection Limit

Spike Recovery outside accepted recovery limits

Page 45 of 66

PM Environmental, Inc.
0604884
7876 Van Dyke - 22-692A

CLIENT:
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Sample ID: mb-2826
Client ID:

QC SUMMARY REPORT
TestCode: SW_8082S

SampType: mblk

PBS

Batch ID: 2826

Analyte

TestCode: sw_8082s

Units: µg/Kg

Prep Date:

Result

PQL

AROCLOR-1221-1

ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND

33

AROCLOR-1242-2

ND

33

AROCLOR-1242-3

ND

33

AROCLOR-1242-4

ND

33

AROCLOR-1242-5

ND

33

AROCLOR-1248-1
AROCLOR-1248-2

ND
ND

33
33

AROCLOR-1248-3

ND

33

AROCLOR-1248-4

ND

33

AROCLOR-1248-5

ND

33

AROCLOR-1254-1

ND

33

AROCLOR-1254-2

ND

33

AROCLOR-1254-3

ND

33

AROCLOR-1254-4

ND

33

AROCLOR-1254-5

ND

33

AROCLOR-1260-1

ND

33

AROCLOR-1260-2

ND

33

AROCLOR-1260-3

ND

33

AROCLOR-1260-4

ND

33

AROCLOR-1260-5

ND

130

33

AROCLOR-1242-1

70

33

AROCLOR-1232-5

Qual

33

AROCLOR-1232-4

RPDLimit

33

AROCLOR-1232-3

%RPD

33

AROCLOR-1232-2

RPD Ref Val

33

AROCLOR-1232-1

HighLimit

33

AROCLOR-1221-5

LowLimit

33

AROCLOR-1221-4

%REC

SeqNo: 90034

33

AROCLOR-1221-3

SPK Ref Val

5/2/2006

33

AROCLOR-1221-2

SPK value

RunNo: 6070

Analysis Date:

TestNo: SW8082

5/1/2006

33

Surr: Decachlorobiphenyl
Qualifiers:

E
ND
S

6.9

8.300

83.1

Value above quantitation range

H

Holding times for preparation or analysis exceeded

M

Manual Integration used to determine area response

Not Detected at the Reporting Limit

R

RPD outside accepted recovery limits

RL

Reporting Detection Limit

Spike Recovery outside accepted recovery limits

Page 46 of 66

PM Environmental, Inc.
0604884
7876 Van Dyke - 22-692A

CLIENT:
Work Order:
Project:

Sample ID: mb-2826
Client ID:

TestCode: SW_8082S

SampType: mblk

PBS

Batch ID: 2826

Analyte

Result

Surr: Tetrachloro-m-xylene
Sample ID: 0604884-002b-ms
Client ID:

QC SUMMARY REPORT

SB-2 2-3'

TestCode: sw_8082s

PQL

SPK value

Analyte

SPK Ref Val

%REC

PQL

Aroclor 1016

160

Aroclor 1260

160

RunNo: 6070

5/2/2006

SeqNo: 90034

LowLimit

HighLimit

70

130

Prep Date:

5/1/2006

RunNo: 6070

Analysis Date:

5/3/2006

SeqNo: 90042

75.7
Units: µg/Kg-dry

TestNo: SW8082

Result

5/1/2006

Analysis Date:

8.300
TestCode: sw_8082s

Batch ID: 2826

Prep Date:

TestNo: SW8082

6.3
SampType: ms

Units: µg/Kg

SPK value

SPK Ref Val

38

191.6

0

38

191.6

%REC

0

LowLimit

HighLimit

81.2

70
70

RPD Ref Val

%RPD

%RPD

RPDLimit

RPDLimit

Qual

130

85.9

RPD Ref Val

130

Surr: Decachlorobiphenyl

8.6

9.540

90.1

70

130

Surr: Tetrachloro-m-xylene

6.9

9.540

72.2

70

130

Prep Date:

5/1/2006

RunNo: 6070

Analysis Date:

5/3/2006

Qual

SeqNo: 90043

Sample ID: 0604884-002b-msd
Client ID:

SB-2 2-3'

SampType: msd
Batch ID: 2826

TestCode: sw_8082s

Units: µg/Kg-dry

TestNo: SW8082

Result

Aroclor 1016
Aroclor 1260

PQL

SPK value

SPK Ref Val

160
170

Analyte

38
38

191.6
191.6

0
0

%REC

LowLimit

HighLimit

RPD Ref Val

%RPD

RPDLimit

84.6
86.5

70
70

130
130

155.6
164.5

4.04
0.711

25
25

Surr: Decachlorobiphenyl

8.5

9.540

89.0

70

130

0

25

Surr: Tetrachloro-m-xylene

7.1

9.540

74.4

70

130

0

Qual

25

Qualifiers:

E
ND
S

Value above quantitation range

H

Holding times for preparation or analysis exceeded

M

Manual Integration used to determine area response

Not Detected at the Reporting Limit

R

RPD outside accepted recovery limits

RL

Reporting Detection Limit

Spike Recovery outside accepted recovery limits

Page 47 of 66

PM Environmental, Inc.
0604884
7876 Van Dyke - 22-692A

CLIENT:
Work Order:
Project:

Sample ID: 0604884-001A
Client ID:

SB-1 1-2'

QC SUMMARY REPORT
TestCode: SW_8260S

SampType: MS

TestCode: SW_8260S

Batch ID: R5970

Analyte

Units: µg/Kg-dry

Prep Date:

TestNo: SW8260B

Result

PQL

Analysis Date:

SPK value

SPK Ref Val

%REC

RunNo: 5970
5/1/2006

LowLimit

HighLimit

1,1,1,2-Tetrachloroethane

490

56

562.9

0

87.3

70

550

56

562.9

0

97.1

70

520

56

562.9

0

92.2

70

600

56

562.9

0

107

70

540

56

562.9

0

95.4

70

130

1,1-Dichloroethane

560

56

562.9

0

99.0

70

130

1,1-Dichloroethene

540

56

562.9

0

96.1

70

130

1,1-Dichloropropene

570

56

562.9

0

101

70

130

1,2,3-Trichlorobenzene

510

56

562.9

0

91.3

70

130

1,2,3-Trichloropropane

560

56

562.9

0

98.7

70

130

1,2,3-Trimethylbenzene

510

56

562.9

0

89.9

70

130

1,2,4-Trichlorobenzene

520

280

562.9

0

92.0

70

130

1,2,4-Trimethylbenzene

530

56

562.9

0

93.8

70

130

1,2-Dibromo-3-chloropropane

460

56

562.9

0

82.4

70

130

1,2-Dichlorobenzene

540

56

562.9

0

96.6

70

130

1,2-Dichloroethane
1,2-Dichloropropane

600
560

56
56

562.9
562.9

0
0

107
99.3

70
70

130
130

1,3,5-Trimethylbenzene

530

56

562.9

0

93.9

70

130

1,3-Dichlorobenzene

520

56

562.9

0

91.6

70

130

1,3-Dichloropropane

560

56

562.9

0

98.9

70

130

1,4-Dichlorobenzene

540

56

562.9

0

95.6

70

130

2,2-Dichloropropane

770

56

562.9

0

137

70

130

2-Chloroethyl vinyl ether

ND

560

562.9

0

77.0

70

Qual

130

1,1,2-Trichloroethane

RPDLimit

130

1,1,2-Trichloro-1,2,2-trifluoroethane

%RPD

130

1,1,2,2-Tetrachloroethane

RPD Ref Val

130

1,1,1-Trichloroethane

SeqNo: 88569

130

2-Chlorotoluene

520

56

562.9

0

93.1

70

130

2-Hexanone

ND

2,800

562.9

0

145

70

130

2-Methylnaphthalene

460

280

562.9

0

81.9

70

130

2-Nitropropane

470

230

562.9

0

84.2

70

130

4-Chlorotoluene

510

56

562.9

0

90.9

70

130

Acetone

ND

2,800

562.9

0

273

70

130

Acrylonitrile

580

280

562.9

0

104

70

130

Benzene

580

56

562.9

0

103

70

S

130

Qualifiers:

E
ND
S

S

S

Value above quantitation range

H

Holding times for preparation or analysis exceeded

M

Manual Integration used to determine area response

Not Detected at the Reporting Limit

R

RPD outside accepted recovery limits

RL

Reporting Detection Limit

Spike Recovery outside accepted recovery limits

Page 48 of 66

PM Environmental, Inc.
0604884
7876 Van Dyke - 22-692A

CLIENT:
Work Order:
Project:

Sample ID: 0604884-001A
Client ID:

SB-1 1-2'

QC SUMMARY REPORT
TestCode: SW_8260S

SampType: MS

TestCode: SW_8260S

Batch ID: R5970

Analyte

Units: µg/Kg-dry

Prep Date:

TestNo: SW8260B

Result

PQL

Analysis Date:

SPK value

SPK Ref Val

%REC

RunNo: 5970
5/1/2006

LowLimit

HighLimit

Bromobenzene

530

56

562.9

0

94.3

70

580

56

562.9

0

102

70

470

56

562.9

0

83.1

70

420

56

562.9

0

74.7

70

650

280

562.9

0

116

70

130

Carbon disulfide

560

280

562.9

0

99.4

70

130

Carbon tetrachloride

520

56

562.9

0

92.8

70

130

Chlorobenzene

560

56

562.9

0

98.6

70

130

Chloroethane

590

280

562.9

0

104

70

130

Chloroform

550

56

562.9

0

98.3

70

130

Chloromethane

430

56

562.9

0

76.8

70

130

cis-1,2-Dichloroethene

600

56

562.9

0

106

70

130

cis-1,3-Dichloropropene

530

56

562.9

0

93.4

70

130

Dibromochloromethane

470

56

562.9

0

83.9

70

130

Dibromomethane

550

56

562.9

0

97.8

70

130

Dichlorodifluoromethane
Dichloromethane

350
580

56
280

562.9
562.9

0
0

61.9
104

70
70

130
130

Diethyl ether

590

280

562.9

0

105

70

130

Ethyl methacrylate

550

56

562.9

0

98.3

70

130

Ethylbenzene

550

56

562.9

0

97.4

70

130

Ethylene dibromide

570

56

562.9

0

100

70

130

Hexachlorobutadiene

480

280

562.9

0

85.5

70

130

Hexachloroethane

420

56

562.9

0

74.8

70

130

Isopropyl ether

600

280

562.9

0

106

70

130

Isopropylbenzene

580

56

562.9

0

102

70

130

m,p-Xylene

1,100

110

1,126

0

93.7

70

130

Methyl ethyl ketone

1,600

280

562.9

0

278

70

130

530

280

562.9

0

94.9

70

130

Methyl isobutyl ketone

ND

560

562.9

0

99.8

70

130

Methyl tert-butyl ether

1,100

280

1,126

0

100

70

130

540

280

562.9

0

96.4

70

Qual

130

Bromomethane

RPDLimit

130

Bromoform

%RPD

130

Bromodichloromethane

RPD Ref Val

130

Bromochloromethane

SeqNo: 88569

130

Methyl Iodide

Naphthalene
Qualifiers:

E
ND
S

S

S

Value above quantitation range

H

Holding times for preparation or analysis exceeded

M

Manual Integration used to determine area response

Not Detected at the Reporting Limit

R

RPD outside accepted recovery limits

RL

Reporting Detection Limit

Spike Recovery outside accepted recovery limits

Page 49 of 66

PM Environmental, Inc.
0604884
7876 Van Dyke - 22-692A

CLIENT:
Work Order:
Project:

Sample ID: 0604884-001A
Client ID:

SB-1 1-2'

QC SUMMARY REPORT
TestCode: SW_8260S

SampType: MS
Batch ID: R5970

Analyte

TestCode: SW_8260S

Units: µg/Kg-dry

Prep Date:

TestNo: SW8260B

Result

PQL

Analysis Date:

SPK value

SPK Ref Val

%REC

RunNo: 5970
5/1/2006

LowLimit

HighLimit

n-Butylbenzene

530

56

562.9

0

94.3

70

550

56

562.9

0

97.4

70

510

56

562.9

0

91.2

70

520

56

562.9

0

92.2

70

520

56

562.9

0

92.2

70

130

Styrene

540

56

562.9

0

95.5

70

130

2,800

2,300

2,815

0

98.6

70

130

tert-Amyl Methyl Ether

570

230

562.9

0

102

70

130

tert-Butyl Ethyl Ether

570

280

562.9

0

102

70

130

tert-Butylbenzene

530

56

562.9

0

94.4

70

130

Tetrachloroethene

720

56

562.9

0

129

70

130

Toluene

630

56

562.9

69.24

99.4

70

130

trans-1,2-Dichloroethene

570

56

562.9

0

102

70

130

trans-1,3-Dichloropropene

550

56

562.9

0

98.1

70

130

trans-1,4-Dichloro-2-butene

620

56

562.9

0

110

70

130

Trichloroethene
Trichlorofluoromethane

540
510

56
56

562.9
562.9

0
0

96.1
90.5

70
70

130
130

510

45

562.9

0

90.1

70

130

1,600

170

1,689

0

92.9

70

Qual

130

sec-Butylbenzene

RPDLimit

130

p-Isopropyltoluene

%RPD

130

o-Xylene

RPD Ref Val

130

n-Propylbenzene

SeqNo: 88569

130

t-Butyl alcohol

Vinyl chloride
Xylenes, Total
Surr: 4-Bromofluorobenzene

3,200

2,815

114

70

130

Surr: Dibromofluoromethane

3,100

2,815

109

70

130

Surr: Toluene-d8

3,100

2,815

111

70

130

Sample ID: 0604884-001A
Client ID:

SB-1 1-2'

SampType: MSD
Batch ID: R5970

Analyte

TestCode: SW_8260S

Units: µg/Kg-dry

TestNo: SW8260B

Analysis Date:

Result

PQL

SPK value

SPK Ref Val

1,1,1,2-Tetrachloroethane

500

56

562.9

0

1,1,1-Trichloroethane

590

56

562.9

0

1,1,2,2-Tetrachloroethane

510

56

562.9

1,1,2-Trichloro-1,2,2-trifluoroethane

640

56

562.9

Qualifiers:

E
ND
S

Prep Date:

%REC

RunNo: 5970
5/1/2006

SeqNo: 88570

LowLimit

HighLimit

RPD Ref Val

%RPD

RPDLimit

88.5

70

130

491.4

1.37

25

105

70

130

546.6

8.10

25

0

90.5

70

130

519.0

1.86

25

0

114

70

130

600.6

6.88

25

Value above quantitation range

H

Holding times for preparation or analysis exceeded

M

Manual Integration used to determine area response

Not Detected at the Reporting Limit

R

RPD outside accepted recovery limits

RL

Reporting Detection Limit

Qual

Spike Recovery outside accepted recovery limits

Page 50 of 66

PM Environmental, Inc.
0604884
7876 Van Dyke - 22-692A

CLIENT:
Work Order:
Project:

Sample ID: 0604884-001A
Client ID:

SB-1 1-2'

QC SUMMARY REPORT
TestCode: SW_8260S

SampType: MSD
Batch ID: R5970

Analyte

TestCode: SW_8260S

Units: µg/Kg-dry

Prep Date:

TestNo: SW8260B

Analysis Date:

Result

PQL

SPK value

SPK Ref Val

1,1,2-Trichloroethane

570

56

562.9

0

1,1-Dichloroethane

580

56

562.9

0

1,1-Dichloroethene

550

56

562.9

1,1-Dichloropropene

640

56

1,2,3-Trichlorobenzene

530

1,2,3-Trichloropropane

530

1,2,3-Trimethylbenzene

%REC

RunNo: 5970
5/1/2006

SeqNo: 88570

LowLimit

HighLimit

RPD Ref Val

%RPD

RPDLimit

101

70

130

537.0

5.90

25

103

70

130

557.3

4.06

25

0

98.3

70

130

541.0

2.26

25

562.9

0

114

70

130

570.2

11.6

25

56

562.9

0

94.3

70

130

513.9

3.23

25

56

562.9

0

94.0

70

130

555.6

4.88

25

490

56

562.9

0

87.6

70

130

506.1

2.59

25

1,2,4-Trichlorobenzene

530

280

562.9

0

93.9

70

130

517.9

2.04

25

1,2,4-Trimethylbenzene

540

56

562.9

0

95.5

70

130

528.0

1.80

25

1,2-Dibromo-3-chloropropane

470

56

562.9

0

82.8

70

130

463.8

0.484

25

1,2-Dichlorobenzene

550

56

562.9

0

96.9

70

130

543.8

0.310

25

1,2-Dichloroethane

610

56

562.9

0

108

70

130

602.3

0.652

25

1,2-Dichloropropane

580

56

562.9

0

104

70

130

559.0

4.33

25

1,3,5-Trimethylbenzene

540

56

562.9

0

96.7

70

130

528.6

2.94

25

1,3-Dichlorobenzene

510

56

562.9

0

91.3

70

130

515.6

0.328

25

1,3-Dichloropropane
1,4-Dichlorobenzene

580
570

56
56

562.9
562.9

0
0

103
101

70
70

130
130

556.7
538.2

4.06
5.20

25
25

2,2-Dichloropropane

790

56

562.9

0

141

70

130

771.2

2.59

25

2-Chloroethyl vinyl ether

ND

560

562.9

0

76.1

70

130

433.4

0

25

2-Chlorotoluene

640

56

562.9

0

113

70

130

524.1

19.3

25

2-Hexanone

ND

2,800

562.9

0

145

70

130

817.4

0

25

2-Methylnaphthalene

540

280

562.9

0

95.7

70

130

461.0

15.5

25

2-Nitropropane

450

230

3,940

0

11.4

70

130

474.0

5.24

0

4-Chlorotoluene

620

56

562.9

0

110

70

130

511.7

19.2

25

Acetone

ND

2,800

562.9

0

259

70

130

1,537

0

25

Acrylonitrile

560

280

562.9

0

98.7

70

130

583.7

4.94

600

56

562.9

0

106

70

130

578.7

2.78

510

56

562.9

0

91.1

70

130

530.8

3.45

610

56

562.9

0

109

70

130

575.9

6.16

25

Bromodichloromethane

480

56

562.9

0

84.7

70

130

467.8

1.91

25

Bromoform

410

56

562.9

0

73.4

70

130

420.5

1.76

S

25

Bromochloromethane

S

25

Bromobenzene

S

25

Benzene

Qual

25

Qualifiers:

E
ND
S

Value above quantitation range

H

Holding times for preparation or analysis exceeded

M

Manual Integration used to determine area response

Not Detected at the Reporting Limit

R

RPD outside accepted recovery limits

RL

Reporting Detection Limit

S

Spike Recovery outside accepted recovery limits

Page 51 of 66

PM Environmental, Inc.
0604884
7876 Van Dyke - 22-692A

CLIENT:
Work Order:
Project:

Sample ID: 0604884-001A
Client ID:

SB-1 1-2'

QC SUMMARY REPORT
TestCode: SW_8260S

SampType: MSD
Batch ID: R5970

Analyte

TestCode: SW_8260S

Units: µg/Kg-dry

Prep Date:

TestNo: SW8260B

Analysis Date:

Result

PQL

SPK value

SPK Ref Val

Bromomethane

630

280

562.9

0

Carbon disulfide

570

280

562.9

0

Carbon tetrachloride

560

56

562.9

Chlorobenzene

560

56

Chloroethane

530

Chloroform
Chloromethane

5/1/2006

SeqNo: 88570

LowLimit

HighLimit

RPD Ref Val

%RPD

RPDLimit

112

70

130

653.6

3.86

25

101

70

130

559.5

1.30

25

0

98.7

70

130

522.4

6.16

25

562.9

0

98.6

70

130

555.0

0

25

280

562.9

0

94.7

70

130

587.1

9.65

25

590

56

562.9

0

104

70

130

553.4

5.92

25

460

56

562.9

0

82.5

70

130

432.3

7.16

25

cis-1,2-Dichloroethene

560

56

562.9

0

99.7

70

130

595.6

5.94

25

cis-1,3-Dichloropropene

550

56

562.9

0

98.2

70

130

525.8

5.01

25

Dibromochloromethane

490

56

562.9

0

86.8

70

130

472.3

3.40

25

Dibromomethane

550

56

562.9

0

97.1

70

130

550.5

0.718

25

Dichlorodifluoromethane

370

56

562.9

0

66.3

70

130

348.4

6.86

25

Dichloromethane

600

280

562.9

0

106

70

130

583.7

2.29

25

Diethyl ether

580

280

562.9

0

103

70

130

588.8

1.06

25

Ethyl methacrylate

540

56

562.9

0

95.7

70

130

553.4

2.68

25

Ethylbenzene
Ethylene dibromide

530
530

56
56

562.9
562.9

0
0

93.6
95.0

70
70

130
130

548.3
565.7

3.98
5.63

25
25

Hexachlorobutadiene

550

280

562.9

0

97.4

70

130

481.3

13.0

25

Hexachloroethane

400

56

562.9

0

71.5

70

130

421.1

4.51

25

Isopropyl ether

610

280

562.9

0

109

70

130

599.5

2.50

25
25

Isopropylbenzene

%REC

RunNo: 5970

570

56

562.9

0

100

70

130

576.4

1.87

m,p-Xylene

1,100

110

1,126

0

97.1

70

130

1,055

3.51

1,500

280

562.9

0

270

70

130

1,563

2.66

25

570

280

562.9

0

101

70

130

534.2

5.93

S

25

Methyl ethyl ketone

Qual

25

Methyl Iodide
Methyl isobutyl ketone

ND

560

562.9

0

92.4

70

130

561.8

0

25

Methyl tert-butyl ether

1,100

280

1,126

0

98.4

70

130

1,129

1.81

25

Naphthalene

550

280

562.9

0

98.5

70

130

542.7

2.15

25

n-Butylbenzene

560

56

562.9

0

99.6

70

130

530.8

5.47

25

n-Propylbenzene

550

56

562.9

0

97.2

70

130

548.3

0.206

25

o-Xylene

530

56

562.9

0

94.1

70

130

513.4

3.13

25

p-Isopropyltoluene

530

56

562.9

0

94.0

70

130

519.0

1.93

S

25

Qualifiers:

E
ND
S

Value above quantitation range

H

Holding times for preparation or analysis exceeded

M

Manual Integration used to determine area response

Not Detected at the Reporting Limit

R

RPD outside accepted recovery limits

RL

Reporting Detection Limit

Spike Recovery outside accepted recovery limits

Page 52 of 66

PM Environmental, Inc.
0604884
7876 Van Dyke - 22-692A

CLIENT:
Work Order:
Project:

Sample ID: 0604884-001A
Client ID:

SB-1 1-2'

QC SUMMARY REPORT
TestCode: SW_8260S

SampType: MSD
Batch ID: R5970

Analyte

TestCode: SW_8260S

Units: µg/Kg-dry

Prep Date:

TestNo: SW8260B

Analysis Date:

Result

PQL

SPK value

SPK Ref Val

sec-Butylbenzene

540

56

562.9

0

Styrene

550

56

562.9

0

2,600

2,300

2,815

tert-Amyl Methyl Ether

570

230

tert-Butyl Ethyl Ether

570

tert-Butylbenzene

530

Tetrachloroethene

5/1/2006

SeqNo: 88570

LowLimit

HighLimit

RPD Ref Val

%RPD

RPDLimit

95.3

70

130

519.0

3.31

25

97.2

70

130

537.6

1.76

25

0

93.9

70

130

2,775

4.90

25

562.9

0

101

70

130

571.9

0.296

25

280

562.9

0

101

70

130

574.7

0.885

25

56

562.9

0

94.5

70

130

531.4

0.106

25

880

56

562.9

0

155

70

130

723.9

18.9

25

Toluene

610

56

562.9

69.24

95.5

70

130

628.8

3.55

25

trans-1,2-Dichloroethene

610

56

562.9

0

109

70

130

573.1

6.83

25

trans-1,3-Dichloropropene

560

56

562.9

0

99.4

70

130

552.2

1.32

25

trans-1,4-Dichloro-2-butene

560

56

562.9

0

99.3

70

130

620.3

10.4

25

Trichloroethene

580

56

562.9

0

103

70

130

541.0

7.22

25

Trichlorofluoromethane

560

56

562.9

0

99.4

70

130

509.4

9.37

25

Vinyl chloride

540

45

562.9

0

95.9

70

130

507.2

6.24

25

1,600

170

1,689

0

96.1

70

130

1,569

3.39

25

t-Butyl alcohol

Xylenes, Total

%REC

RunNo: 5970

Surr: 4-Bromofluorobenzene
Surr: Dibromofluoromethane

3,200
3,100

2,815
2,815

113
111

70
70

130
130

0
0

3,000

2,815

107

70

130

0

S

25
25

Surr: Toluene-d8

Qual

25

Sample ID: 10ug/L LCS1
Client ID:

LCSS

SampType: LCS
Batch ID: R5970

Analyte

TestCode: SW_8260S

Units: µg/Kg

Prep Date:

TestNo: SW8260B

Result

PQL

Analysis Date:

SPK value

SPK Ref Val

%REC

RunNo: 5970
5/1/2006

LowLimit

HighLimit

1,1,1,2-Tetrachloroethane

460

50

500.0

0

91.3

70

490

50

500.0

0

98.4

70

480

50

500.0

0

96.3

70

570

50

500.0

0

115

70

510

50

500.0

0

102

70

130

1,1-Dichloroethane

530

50

500.0

0

105

70

130

1,1-Dichloroethene

520

50

500.0

0

104

70

130

1,1-Dichloropropene

520

50

500.0

0

105

70

Qual

130

1,1,2-Trichloroethane

RPDLimit

130

1,1,2-Trichloro-1,2,2-trifluoroethane

%RPD

130

1,1,2,2-Tetrachloroethane

RPD Ref Val

130

1,1,1-Trichloroethane

SeqNo: 88582

130

Qualifiers:

E
ND
S

Value above quantitation range

H

Holding times for preparation or analysis exceeded

M

Manual Integration used to determine area response

Not Detected at the Reporting Limit

R

RPD outside accepted recovery limits

RL

Reporting Detection Limit

Spike Recovery outside accepted recovery limits

Page 53 of 66

PM Environmental, Inc.
0604884
7876 Van Dyke - 22-692A

CLIENT:
Work Order:
Project:

Sample ID: 10ug/L LCS1
Client ID:

LCSS

QC SUMMARY REPORT
TestCode: SW_8260S

SampType: LCS
Batch ID: R5970

Analyte

TestCode: SW_8260S

Units: µg/Kg

Prep Date:

TestNo: SW8260B

Result

PQL

Analysis Date:

SPK value

SPK Ref Val

%REC

RunNo: 5970
5/1/2006

LowLimit

HighLimit

SeqNo: 88582
RPD Ref Val

%RPD

RPDLimit

Qual

1,2,3-Trichlorobenzene

540

50

500.0

0

107

70

130

1,2,3-Trichloropropane

490

50

500.0

0

98.1

70

130

1,2,3-Trimethylbenzene

470

50

500.0

0

93.3

70

130

1,2,4-Trichlorobenzene

530

250

500.0

0

105

70

130

1,2,4-Trimethylbenzene

500

50

500.0

0

99.2

70

130

1,2-Dibromo-3-chloropropane

470

50

500.0

0

93.1

70

130

1,2-Dichlorobenzene

510

50

500.0

0

102

70

130

1,2-Dichloroethane

540

50

500.0

0

109

70

130

1,2-Dichloropropane

500

50

500.0

0

99.8

70

130

1,3,5-Trimethylbenzene

490

50

500.0

0

97.7

70

130

1,3-Dichlorobenzene

500

50

500.0

0

100

70

130

1,3-Dichloropropane

520

50

500.0

0

105

70

130

1,4-Dichlorobenzene

530

50

500.0

0

106

70

130

2,2-Dichloropropane

790

50

500.0

0

158

70

130

2-Chloroethyl vinyl ether

ND

500

500.0

0

82.1

70

130

2-Chlorotoluene
2-Hexanone

520
ND

50
2,500

500.0
500.0

0
0

103
142

70
70

130
130

S

2-Methylnaphthalene

780

250

500.0

0

156

70

130

S

2-Nitropropane

420

200

500.0

0

84.8

70

130

4-Chlorotoluene

500

50

500.0

0

101

70

130

Acetone

ND

2,500

500.0

0

248

70

130

Acrylonitrile

530

250

500.0

0

105

70

130

Benzene

540

50

500.0

0

108

70

130

Bromobenzene

490

50

500.0

0

97.5

70

130

Bromochloromethane

580

50

500.0

0

116

70

130

Bromodichloromethane

450

50

500.0

0

89.1

70

130

Bromoform

400

50

500.0

0

80.5

70

130

Bromomethane

520

250

500.0

0

103

70

130

Carbon disulfide

540

250

500.0

0

109

70

130

Carbon tetrachloride

520

50

500.0

0

103

70

130

Chlorobenzene

510

50

500.0

0

102

70

130

Qualifiers:

E
ND
S

S

S

Value above quantitation range

H

Holding times for preparation or analysis exceeded

M

Manual Integration used to determine area response

Not Detected at the Reporting Limit

R

RPD outside accepted recovery limits

RL

Reporting Detection Limit

Spike Recovery outside accepted recovery limits

Page 54 of 66

PM Environmental, Inc.
0604884
7876 Van Dyke - 22-692A

CLIENT:
Work Order:
Project:

Sample ID: 10ug/L LCS1
Client ID:

LCSS

QC SUMMARY REPORT
TestCode: SW_8260S

SampType: LCS
Batch ID: R5970

Analyte

TestCode: SW_8260S

Units: µg/Kg

Prep Date:

TestNo: SW8260B

Result

PQL

Analysis Date:

SPK value

SPK Ref Val

%REC

RunNo: 5970
5/1/2006

LowLimit

HighLimit

Chloroethane

530

250

500.0

0

107

70

510

50

500.0

0

102

70

410

50

500.0

0

81.8

70

470

50

500.0

0

94.2

70

500

50

500.0

0

101

70

130

Dibromochloromethane

460

50

500.0

0

91.4

70

130

Dibromomethane

490

50

500.0

0

97.9

70

130

Dichlorodifluoromethane

340

50

500.0

0

68.1

70

130

Dichloromethane

540

250

500.0

0

108

70

130

Diethyl ether

520

250

500.0

0

103

70

130

Ethyl methacrylate

480

50

500.0

0

95.4

70

130

Ethylbenzene

500

50

500.0

0

99.1

70

130

Ethylene dibromide

490

50

500.0

0

98.0

70

130

Hexachlorobutadiene

580

250

500.0

0

116

70

130

Hexachloroethane

440

50

500.0

0

87.5

70

130

Isopropyl ether
Isopropylbenzene

560
530

250
50

500.0
500.0

0
0

112
106

70
70

130
130

m,p-Xylene

980

100

1,000

0

98.4

70

130

Methyl ethyl ketone

940

250

500.0

0

189

70

130

Methyl Iodide

470

250

500.0

0

94.5

70

130

Methyl isobutyl ketone

520

500

500.0

0

103

70

130

Methyl tert-butyl ether

1,000

250

1,000

0

105

70

130

Naphthalene

540

250

500.0

0

109

70

130

n-Butylbenzene

530

50

500.0

0

106

70

130

n-Propylbenzene

500

50

500.0

0

99.9

70

130

o-Xylene

490

50

500.0

0

97.6

70

130

p-Isopropyltoluene

500

50

500.0

0

100

70

130

sec-Butylbenzene

510

50

500.0

0

102

70

130

Styrene

490

50

500.0

0

98.8

70

130

2,500

2,000

2,500

0

99.9

70

130

520

200

500.0

0

104

70

Qual

130

cis-1,3-Dichloropropene

RPDLimit

130

cis-1,2-Dichloroethene

%RPD

130

Chloromethane

RPD Ref Val

130

Chloroform

SeqNo: 88582

130

t-Butyl alcohol tert-Amyl Methyl Ether
Qualifiers:

E
ND
S

S

S

Value above quantitation range

H

Holding times for preparation or analysis exceeded

M

Manual Integration used to determine area response

Not Detected at the Reporting Limit

R

RPD outside accepted recovery limits

RL

Reporting Detection Limit

Spike Recovery outside accepted recovery limits

Page 55 of 66

PM Environmental, Inc.
0604884
7876 Van Dyke - 22-692A

CLIENT:
Work Order:
Project:

Sample ID: 10ug/L LCS1
Client ID:

LCSS

QC SUMMARY REPORT
TestCode: SW_8260S

SampType: LCS
Batch ID: R5970

Analyte

TestCode: SW_8260S

Units: µg/Kg

Prep Date:

TestNo: SW8260B

Result

PQL

Analysis Date:

SPK value

SPK Ref Val

%REC

RunNo: 5970
5/1/2006

LowLimit

HighLimit

tert-Butyl Ethyl Ether

550

250

500.0

0

110

70

480

50

500.0

0

95.7

70

490

50

500.0

0

97.9

70

520

50

500.0

0

104

70

530

50

500.0

0

106

70

130

trans-1,3-Dichloropropene

520

50

500.0

0

104

70

130

trans-1,4-Dichloro-2-butene

560

50

500.0

0

111

70

130

Trichloroethene

500

50

500.0

0

99.4

70

130

Trichlorofluoromethane

530

50

500.0

0

107

70

130

Vinyl chloride

480

40

500.0

0

96.1

70

130

1,500

150

1,500

0

98.1

70

Qual

130

trans-1,2-Dichloroethene

RPDLimit

130

Toluene

%RPD

130

Tetrachloroethene

RPD Ref Val

130

tert-Butylbenzene

SeqNo: 88582

130

Xylenes, Total
Surr: 4-Bromofluorobenzene

2,800

2,500

111

70

130

Surr: Dibromofluoromethane

2,700

2,500

109

70

130

Surr: Toluene-d8

2,800

2,500

111

70

130

Sample ID: MBLK1 1.0mL
Client ID:

PBS

SampType: MBLK
Batch ID: R5970

Analyte

TestCode: SW_8260S

Units: µg/Kg

Prep Date:

TestNo: SW8260B

Result

PQL

1,1,1,2-Tetrachloroethane

ND
ND
ND
ND
ND
ND
ND
ND
ND

50

1,2,3-Trichloropropane

ND

50

1,2,3-Trimethylbenzene

ND

50

1,2,4-Trichlorobenzene

ND

Qual

50

1,2,3-Trichlorobenzene

RPDLimit

50

1,1-Dichloropropene

%RPD

50

1,1-Dichloroethene

RPD Ref Val

50

1,1-Dichloroethane

HighLimit

50

1,1,2-Trichloroethane

LowLimit

50

1,1,2-Trichloro-1,2,2-trifluoroethane

%REC

SeqNo: 88583

50

1,1,2,2-Tetrachloroethane

SPK Ref Val

5/1/2006

50

1,1,1-Trichloroethane

SPK value

Analysis Date:

RunNo: 5970

250

Qualifiers:

E
ND
S

Value above quantitation range

H

Holding times for preparation or analysis exceeded

M

Manual Integration used to determine area response

Not Detected at the Reporting Limit

R

RPD outside accepted recovery limits

RL

Reporting Detection Limit

Spike Recovery outside accepted recovery limits

Page 56 of 66

PM Environmental, Inc.
0604884
7876 Van Dyke - 22-692A

CLIENT:
Work Order:
Project:

Sample ID: MBLK1 1.0mL
Client ID:

PBS

QC SUMMARY REPORT
TestCode: SW_8260S

SampType: MBLK
Batch ID: R5970

Analyte

TestCode: SW_8260S

Units: µg/Kg

Prep Date:

TestNo: SW8260B

Result

PQL

1,2,4-Trimethylbenzene

ND
ND
ND
ND
ND
ND
ND
ND
ND

50

2,2-Dichloropropane

ND

50

2-Chloroethyl vinyl ether

ND

500

2-Chlorotoluene

ND

50

2-Hexanone

ND

2,500

2-Methylnaphthalene

ND

250

2-Nitropropane

ND

200

4-Chlorotoluene
Acetone

ND
ND

50
2,500

Acrylonitrile

ND

250

Benzene

ND

50

Bromobenzene

ND

50

Bromochloromethane

ND

50

Bromodichloromethane

ND

50

Bromoform

ND

50

Bromomethane

ND

250

Carbon disulfide

ND

250

Carbon tetrachloride

ND

50

Chlorobenzene

ND

50

Chloroethane

ND

250

Chloroform

ND

50

Chloromethane

ND

50

cis-1,2-Dichloroethene

ND

Qual

50

1,4-Dichlorobenzene

RPDLimit

50

1,3-Dichloropropane

%RPD

50

1,3-Dichlorobenzene

RPD Ref Val

50

1,3,5-Trimethylbenzene

HighLimit

50

1,2-Dichloropropane

LowLimit

50

1,2-Dichloroethane

%REC

SeqNo: 88583

50

1,2-Dichlorobenzene

SPK Ref Val

5/1/2006

50

1,2-Dibromo-3-chloropropane

SPK value

Analysis Date:

RunNo: 5970

50

Qualifiers:

E
ND
S

Value above quantitation range

H

Holding times for preparation or analysis exceeded

M

Manual Integration used to determine area response

Not Detected at the Reporting Limit

R

RPD outside accepted recovery limits

RL

Reporting Detection Limit

Spike Recovery outside accepted recovery limits

Page 57 of 66

PM Environmental, Inc.
0604884
7876 Van Dyke - 22-692A

CLIENT:
Work Order:
Project:

Sample ID: MBLK1 1.0mL
Client ID:

PBS

QC SUMMARY REPORT
TestCode: SW_8260S

SampType: MBLK
Batch ID: R5970

Analyte

TestCode: SW_8260S

Units: µg/Kg

Prep Date:

TestNo: SW8260B

Result

PQL

cis-1,3-Dichloropropene

ND
ND
ND
ND
ND
ND
ND
ND
ND

50

Hexachlorobutadiene

ND

250

Hexachloroethane

ND

50

Isopropyl ether

ND

250

Isopropylbenzene

ND

50

m,p-Xylene

ND

100

Methyl ethyl ketone

ND

250

Methyl Iodide
Methyl isobutyl ketone

ND
ND

250
500

Methyl tert-butyl ether

ND

250

Naphthalene

ND

250

n-Butylbenzene

ND

50

n-Propylbenzene

ND

50

o-Xylene

ND

50

p-Isopropyltoluene

ND

50

sec-Butylbenzene

ND

50

Styrene

ND

50

t-Butyl alcohol

ND

2,000

tert-Amyl Methyl Ether

ND

200

tert-Butyl Ethyl Ether

ND

250

tert-Butylbenzene

ND

50

Tetrachloroethene

ND

50

Toluene

ND

Qual

50

Ethylene dibromide

RPDLimit

50

Ethylbenzene

%RPD

250

Ethyl methacrylate

RPD Ref Val

250

Diethyl ether

HighLimit

50

Dichloromethane

LowLimit

50

Dichlorodifluoromethane

%REC

SeqNo: 88583

50

Dibromomethane

SPK Ref Val

5/1/2006

50

Dibromochloromethane

SPK value

Analysis Date:

RunNo: 5970

50

Qualifiers:

E
ND
S

Value above quantitation range

H

Holding times for preparation or analysis exceeded

M

Manual Integration used to determine area response

Not Detected at the Reporting Limit

R

RPD outside accepted recovery limits

RL

Reporting Detection Limit

Spike Recovery outside accepted recovery limits

Page 58 of 66

PM Environmental, Inc.
0604884
7876 Van Dyke - 22-692A

CLIENT:
Work Order:
Project:

Sample ID: MBLK1 1.0mL
Client ID:

PBS

QC SUMMARY REPORT
TestCode: SW_8260S

SampType: MBLK
Batch ID: R5970

Analyte

TestCode: SW_8260S

Units: µg/Kg

Prep Date:

TestNo: SW8260B

Result

PQL

trans-1,2-Dichloroethene

ND
ND
ND
ND
ND
ND
ND

%RPD

RPDLimit

Qual

40

Xylenes, Total

RPD Ref Val

50

Vinyl chloride

HighLimit

50

Trichlorofluoromethane

LowLimit

50

Trichloroethene

%REC

SeqNo: 88583

50

trans-1,4-Dichloro-2-butene

SPK Ref Val

5/1/2006

50

trans-1,3-Dichloropropene

SPK value

Analysis Date:

RunNo: 5970

150

Surr: 4-Bromofluorobenzene

2,800

2,500

113

70

130

Surr: Dibromofluoromethane

2,700

2,500

109

70

130

Surr: Toluene-d8

2,700

2,500

107

70

130

Qualifiers:

E
ND
S

Value above quantitation range

H

Holding times for preparation or analysis exceeded

M

Manual Integration used to determine area response

Not Detected at the Reporting Limit

R

RPD outside accepted recovery limits

RL

Reporting Detection Limit

Spike Recovery outside accepted recovery limits

Page 59 of 66

PM Environmental, Inc.
0604884
7876 Van Dyke - 22-692A

CLIENT:
Work Order:
Project:

Sample ID: 0604884-001BMS
Client ID:

SB-1 1-2'

QC SUMMARY REPORT
TestCode: SW_8270S

SampType: MS

TestCode: SW_8270S

Batch ID: 2825

Analyte

Units: µg/Kg-dry

Prep Date:

Result

PQL

SPK value

SPK Ref Val

%REC

RunNo: 5994

Analysis Date:

TestNo: SW8270C

5/1/2006
5/2/2006

SeqNo: 88963

LowLimit

HighLimit

1,2,4-Trichlorobenzene

1,600

370

1,873

0

83.0

50

1,700

370

1,873

0

88.4

50

1,600

370

1,873

0

85.4

50

1,700

370

1,873

0

90.7

50

130

2,4-Dimethylphenol

1,800

370

1,873

0

97.1

50

130

2,4-Dinitrophenol

ND

370

1,873

0

0

50

130

2,4-Dinitrotoluene

1,900

370

1,873

0

102

50

Qual

130

2,4-Dichlorophenol

RPDLimit

130

2,4,6-Trichlorophenol

%RPD

130

2,4,5-Trichlorophenol

RPD Ref Val

130

2,6-Dichlorophenol

ND

370

1,873

0

0

50

130

2,6-Dinitrotoluene

1,900

370

1,873

0

102

50

130

2-Chloronaphthalene

1,700

370

1,873

0

90.1

50

130

2-Chlorophenol

1,700

370

1,873

0

92.0

50

130

2-Methylnaphthalene

1,600

370

1,873

0

86.5

50

130

2-Methylphenol

1,700

370

1,873

0

92.4

50

130

2-Nitroaniline

1,800

930

1,873

0

95.7

50

130

2-Nitrophenol

1,800

370

1,873

0

94.4

50

130

3,3´-Dichlorobenzidine
3/4 Methylphenol

1,800
1,600

370
370

1,873
1,873

0
0

95.9
84.6

50
50

130
130

3-Nitroaniline

1,800

930

1,873

0

94.1

50

130

4,6-Dinitro-2-methylphenol

1,300

370

1,873

0

68.7

50

130

4-Chloro-3-methylphenol

1,800

310

1,873

0

97.7

50

130

4-Chloroaniline

1,700

370

1,873

0

92.1

50

130

4-Chlorophenyl phenyl ether

1,800

370

1,873

0

97.2

50

130

4-Nitroaniline

1,900

930

1,873

0

99.3

50

130

4-Nitrophenol

1,300

930

1,873

0

69.3

50

130

Acenaphthene

1,900

370

1,873

0

101

50

130

Acenaphthylene

1,800

370

1,873

0

94.3

50

130

Aniline

1,400

370

1,873

0

74.7

50

130

Anthracene

1,900

370

1,873

0

99.2

50

130

Benz(a)anthracene

1,700

370

1,873

0

90.1

50

130

Benzidine

1,400

370

1,873

0

76.6

50

130

Benzo(a)pyrene

2,000

370

1,873

0

107

50

S

130

Qualifiers:

E
ND
S

S

Value above quantitation range

H

Holding times for preparation or analysis exceeded

M

Manual Integration used to determine area response

Not Detected at the Reporting Limit

R

RPD outside accepted recovery limits

RL

Reporting Detection Limit

Spike Recovery outside accepted recovery limits

Page 60 of 66

PM Environmental, Inc.
0604884
7876 Van Dyke - 22-692A

CLIENT:
Work Order:
Project:

Sample ID: 0604884-001BMS
Client ID:

SB-1 1-2'

QC SUMMARY REPORT
TestCode: SW_8270S

SampType: MS

TestCode: SW_8270S

Batch ID: 2825

Analyte

Units: µg/Kg-dry

Prep Date:

Result

PQL

SPK value

SPK Ref Val

%REC

RunNo: 5994

Analysis Date:

TestNo: SW8270C

5/1/2006
5/2/2006

SeqNo: 88963

LowLimit

HighLimit

Benzo(b)fluoranthene

2,000

370

1,873

0

108

50

2,000

370

1,873

0

106

50

1,900

370

1,873

0

99.8

50

ND

3,700

1,873

0

0

50

130

Benzyl alcohol

ND

3,700

1,873

0

92.4

50

Qual

130

Benzoic acid

RPDLimit

130

Benzo(k)fluoranthene

%RPD

130

Benzo(g,h,i)perylene

RPD Ref Val

130

Bis(2-chloroethoxy)methane

1,800

370

1,873

0

94.6

50

130

Bis(2-chloroethyl) ether

1,600

110

1,873

0

87.0

50

130

Bis(2-chloroisopropyl) ether

1,600

370

1,873

0

87.9

50

130

Bis(2-ethylhexyl) phthalate

2,300

370

1,873

0

125

50

130

Butyl benzyl phthalate

2,000

370

1,873

0

107

50

130

Carbazole

1,900

370

1,873

0

104

50

130

Chrysene

1,900

370

1,873

0

103

50

130

Dibenz(a,h)anthracene

1,900

370

1,873

0

101

50

130

Dibenzofuran

1,800

370

1,873

0

98.8

50

130

Diethyl phthalate

2,100

370

1,873

0

110

50

130

Dimethyl phthalate
Di-n-butyl phthalate

1,800
2,000

370
370

1,873
1,873

0
0

96.2
109

50
50

130
130

Di-n-octyl phthalate

2,200

370

1,873

0

119

50

130

Fluoranthene

1,800

370

1,873

0

94.4

50

130

Fluorene

1,900

370

1,873

0

102

50

130

Hexachlorobenzene

1,800

370

1,873

0

94.6

50

130

Hexachlorobutadiene

1,600

56

1,873

0

83.6

50

130

Hexachlorocyclopentadiene

1,500

370

1,873

0

80.1

50

130

Hexachloroethane

1,700

340

1,873

0

88.8

50

130

Indeno(1,2,3-cd)pyrene

1,900

370

1,873

0

101

50

130

Isophorone

1,700

370

1,873

0

89.9

50

130

Naphthalene

1,700

370

1,873

0

91.5

50

130

Nitrobenzene

1,800

370

1,873

0

94.6

50

130

N-Nitrosodimethylamine

1,400

370

1,873

0

74.4

50

130

N-Nitrosodi-n-propylamine

1,700

370

1,873

0

93.0

50

130

N-Nitrosodiphenylamine

2,400

370

1,873

0

130

50

S

130

Qualifiers:

E
ND
S

S

Value above quantitation range

H

Holding times for preparation or analysis exceeded

M

Manual Integration used to determine area response

Not Detected at the Reporting Limit

R

RPD outside accepted recovery limits

RL

Reporting Detection Limit

Spike Recovery outside accepted recovery limits

Page 61 of 66

PM Environmental, Inc.
0604884
7876 Van Dyke - 22-692A

CLIENT:
Work Order:
Project:

Sample ID: 0604884-001BMS
Client ID:

SB-1 1-2'

QC SUMMARY REPORT
TestCode: SW_8270S

SampType: MS

TestCode: SW_8270S

Batch ID: 2825

Analyte

Units: µg/Kg-dry

Prep Date:

Result

PQL

SPK value

SPK Ref Val

%REC

RunNo: 5994

Analysis Date:

TestNo: SW8270C

5/1/2006
5/2/2006

SeqNo: 88963

LowLimit

HighLimit

Pentachlorophenol

1,400

370

1,873

0

74.6

50

1,900

370

1,873

0

102

50

1,700

370

1,873

0

90.7

50

1,800

370

1,873

0

96.5

50

130

Pyridine

1,000

370

1,873

0

55.6

50

Qual

130

Pyrene

RPDLimit

130

Phenol

%RPD

130

Phenanthrene

RPD Ref Val

130

Surr: 2,4,6-Tribromophenol

1,800

1,873

94.8

50

130

Surr: 2-Fluorobiphenyl

1,600

1,873

86.7

50

130

Surr: 2-Fluorophenol

1,700

1,873

88.9

50

130

Surr: Nitrobenzene-d5

1,700

1,873

88.8

50

130

Surr: Phenol-d5

1,700

1,873

90.5

50

130

Surr: Terphenyl-d14

1,600

1,873

87.1

50

130

Prep Date:

5/1/2006

RunNo: 5994

Analysis Date:

5/2/2006

SeqNo: 88964

Sample ID: 0604884-001BMSD
Client ID:

SB-1 1-2'

SampType: MSD
Batch ID: 2825

Analyte

TestCode: SW_8270S

Units: µg/Kg-dry

TestNo: SW8270C

Result

PQL

SPK value

SPK Ref Val

1,2,4-Trichlorobenzene

1,500

370

1,873

0

2,4,5-Trichlorophenol

1,600

370

1,873

0

2,4,6-Trichlorophenol

1,600

370

1,873

2,4-Dichlorophenol

1,700

370

2,4-Dimethylphenol

1,800

2,4-Dinitrophenol
2,4-Dinitrotoluene

LowLimit

HighLimit

RPD Ref Val

%RPD

RPDLimit

81.8

50

130

1,554

1.51

25

87.5

50

130

1,655

1.00

25

0

87.1

50

130

1,600

1.90

25

1,873

0

89.7

50

130

1,699

1.15

25

370

1,873

0

94.5

50

130

1,818

2.71

25

ND

370

1,873

0

0

50

130

0

0

25

1,800

2,6-Dichlorophenol

%REC

370

1,873

0

98.8

50

130

1,904

2.91

25

ND

370

1,873

0

0

50

130

0

0

25

2,6-Dinitrotoluene

1,900

370

1,873

0

100

50

130

1,918

1.97

Qual

S

25

2-Chloronaphthalene

1,700

370

1,873

0

89.8

50

130

1,687

0.311

25

2-Chlorophenol

1,700

370

1,873

0

91.9

50

130

1,723

0.131

25

2-Methylnaphthalene

1,600

370

1,873

0

86.8

50

130

1,619

0.369

25

2-Methylphenol

1,700

370

1,873

0

90.9

50

130

1,730

1.66

25

2-Nitroaniline

1,800

930

1,873

0

96.1

50

130

1,793

0.375

25

2-Nitrophenol

1,700

370

1,873

0

93.0

50

130

1,768

1.49

S

25

Qualifiers:

E
ND
S

Value above quantitation range

H

Holding times for preparation or analysis exceeded

M

Manual Integration used to determine area response

Not Detected at the Reporting Limit

R

RPD outside accepted recovery limits

RL

Reporting Detection Limit

Spike Recovery outside accepted recovery limits

Page 62 of 66

PM Environmental, Inc.
0604884
7876 Van Dyke - 22-692A

CLIENT:
Work Order:
Project:

Sample ID: 0604884-001BMSD
Client ID:

SB-1 1-2'

QC SUMMARY REPORT
TestCode: SW_8270S

SampType: MSD
Batch ID: 2825

Analyte

TestCode: SW_8270S

Units: µg/Kg-dry

Prep Date:

Result

PQL

SPK value

SPK Ref Val

3,3´-Dichlorobenzidine

1,900

370

1,873

0

3/4 Methylphenol

1,600

370

1,873

0

3-Nitroaniline

1,800

930

1,873

0

4,6-Dinitro-2-methylphenol

1,100

370

1,873

4-Chloro-3-methylphenol

1,900

310

1,873

4-Chloroaniline

1,700

370

4-Chlorophenyl phenyl ether

1,800

370

4-Nitroaniline

1,900

4-Nitrophenol

1,400

Acenaphthene

1,900

Acenaphthylene

1,800

Aniline

1,400

%REC

RunNo: 5994

Analysis Date:

TestNo: SW8270C

5/1/2006
5/2/2006

SeqNo: 88964

LowLimit

HighLimit

RPD Ref Val

%RPD

RPDLimit

100

50

130

84.6

50

130

1,796

4.52

25

1,584

0.0473

98.2

50

25

130

1,763

4.20

0

56.6

0

100

25

50

130

1,286

19.4

25

50

130

1,829

2.63

1,873

0

25

92.3

50

130

1,725

0.217

1,873

0

25

94.1

50

130

1,820

3.26

930

1,873

0

99.4

930

1,873

0

72.7

25

50

130

1,860

0.0805

25

50

130

1,297

4.85

370

1,873

0

99.8

370

1,873

0

94.6

25

50

130

1,891

1.24

25

50

130

1,766

0.381

370

1,873

0

76.2

25

50

130

1,399

2.07

25

Anthracene

1,900

370

1,873

0

99.2

50

130

1,857

0.0403

25

Benz(a)anthracene

1,700

370

1,873

0

92.5

50

130

1,688

2.58

25

Benzidine

1,500

370

1,873

0

77.7

50

130

1,435

1.40

25

Benzo(a)pyrene
Benzo(b)fluoranthene

1,900
2,000

370
370

1,873
1,873

0
0

104
109

50
50

130
130

1,997
2,027

2.70
0.810

25
25

Benzo(g,h,i)perylene

1,900

370

1,873

0

104

50

130

1,980

1.72

25

Benzo(k)fluoranthene

1,900

370

1,873

0

99.0

50

130

1,868

0.724

25

Benzoic acid

ND

3,700

1,873

0

0

50

130

0

0

25

Benzyl alcohol

ND

3,700

1,873

0

93.6

50

130

1,730

0

25

Bis(2-chloroethoxy)methane

1,700

370

1,873

0

91.1

50

130

1,772

3.79

25

Bis(2-chloroethyl) ether

1,600

110

1,873

0

86.8

50

130

1,630

0.276

25

Bis(2-chloroisopropyl) ether

1,600

370

1,873

0

85.5

50

130

1,646

2.81

25

Bis(2-ethylhexyl) phthalate

2,300

370

1,873

0

124

50

130

2,346

1.03

25

Butyl benzyl phthalate

2,000

370

1,873

0

109

50

130

2,007

1.67

25

Carbazole

2,000

370

1,873

0

105

50

130

1,945

0.844

25

Chrysene

1,900

370

1,873

0

103

50

130

1,930

0.272

25

Dibenz(a,h)anthracene

1,900

370

1,873

0

101

50

130

1,893

0.395

25

Dibenzofuran

1,800

370

1,873

0

95.9

50

130

1,849

2.96

25

Diethyl phthalate

2,000

370

1,873

0

107

50

130

2,069

3.65

Qual

25

Qualifiers:

E
ND
S

Value above quantitation range

H

Holding times for preparation or analysis exceeded

M

Manual Integration used to determine area response

Not Detected at the Reporting Limit

R

RPD outside accepted recovery limits

RL

Reporting Detection Limit

S

Spike Recovery outside accepted recovery limits

Page 63 of 66

PM Environmental, Inc.
0604884
7876 Van Dyke - 22-692A

CLIENT:
Work Order:
Project:

Sample ID: 0604884-001BMSD
Client ID:

SB-1 1-2'

SampType: MSD
Batch ID: 2825

Analyte

QC SUMMARY REPORT
TestCode: SW_8270S
TestCode: SW_8270S

Units: µg/Kg-dry

Prep Date:

Result

PQL

SPK value

SPK Ref Val

Dimethyl phthalate

1,700

370

1,873

0

Di-n-butyl phthalate

2,000

370

1,873

0

Di-n-octyl phthalate

2,300

370

1,873

Fluoranthene

1,800

370

Fluorene

1,900

Hexachlorobenzene
Hexachlorobutadiene

%REC

RunNo: 5994

Analysis Date:

TestNo: SW8270C

5/1/2006
5/2/2006

SeqNo: 88964

LowLimit

HighLimit

RPD Ref Val

%RPD

RPDLimit

93.0

50

130

1,801

3.34

25

107

50

130

2,043

1.93

25

0

122

50

130

2,231

2.29

25

1,873

0

93.5

50

130

1,768

0.979

25

370

1,873

0

99.0

50

130

1,903

2.55

25

1,700

370

1,873

0

92.9

50

130

1,772

1.88

25

1,500

56

1,873

0

82.5

50

130

1,565

1.30

25

Hexachlorocyclopentadiene

1,400

370

1,873

0

77.3

50

130

1,500

3.51

25

Hexachloroethane

1,600

340

1,873

0

86.8

50

130

1,664

2.28

25

Indeno(1,2,3-cd)pyrene

1,900

370

1,873

0

100

50

130

1,899

1.43

25

Isophorone

1,600

370

1,873

0

87.6

50

130

1,684

2.61

25

Naphthalene

1,700

370

1,873

0

90.4

50

130

1,713

1.14

25

Nitrobenzene

1,700

370

1,873

0

92.5

50

130

1,771

2.18

25

N-Nitrosodimethylamine

1,400

370

1,873

0

73.8

50

130

1,393

0.702

25

N-Nitrosodi-n-propylamine

1,700

370

1,873

0

92.1

50

130

1,741

0.951

25

N-Nitrosodiphenylamine
Pentachlorophenol

2,400
1,400

370
370

1,873
1,873

0
0

126
74.8

50
50

130
130

2,442
1,398

3.18
0.214

25
25

Phenanthrene

1,900

370

1,873

0

104

50

130

1,905

1.95

25

Phenol

1,700

370

1,873

0

91.0

50

130

1,698

0.352

25

Pyrene

1,800

370

1,873

0

96.2

50

130

1,807

0.332

25

Pyridine

1,000

370

1,873

0

1,041

56.0

50

130

0.788

25

Surr: 2,4,6-Tribromophenol

1,800

1,873

93.6

50

130

0

25

Surr: 2-Fluorobiphenyl

1,700

1,873

89.3

50

130

0

25

Surr: 2-Fluorophenol

1,700

1,873

89.5

50

130

0

25

Surr: Nitrobenzene-d5

1,700

1,873

90.6

50

130

0

25

Surr: Phenol-d5

1,700

1,873

93.2

50

130

0

25

Surr: Terphenyl-d14

1,700

1,873

92.6

50

130

0

Qual

25

Qualifiers:

E
ND
S

Value above quantitation range

H

Holding times for preparation or analysis exceeded

M

Manual Integration used to determine area response

Not Detected at the Reporting Limit

R

RPD outside accepted recovery limits

RL

Reporting Detection Limit

Spike Recovery outside accepted recovery limits

Page 64 of 66

PM Environmental, Inc.
0604884
7876 Van Dyke - 22-692A

CLIENT:
Work Order:
Project:

Sample ID: LCS-2825
Client ID:

LCSS

QC SUMMARY REPORT
TestCode: SW_8270S

SampType: LCS
Batch ID: 2825

Analyte

TestCode: SW_8270S

Prep Date:

PQL

SPK value

SPK Ref Val

%REC

5/1/2006

RunNo: 5994

Analysis Date:

TestNo: SW8270C

Result

2-Methylnaphthalene

Units: µg/Kg

5/2/2006

SeqNo: 88966

LowLimit

HighLimit

830

330

1,667

0

49.9

50

330

1,667

0

59.7

50

910

330

1,667

0

54.5

50

960

330

1,667

0

57.5

50

130

Benz(a)anthracene

900

330

1,667

0

54.0

50

130

Benzo(a)pyrene

1,000

330

1,667

0

60.6

50

130

Benzo(b)fluoranthene

1,100

330

1,667

0

63.2

50

130

Benzo(g,h,i)perylene

980

330

1,667

0

58.8

50

130

Benzo(k)fluoranthene

980

330

1,667

0

58.7

50

130

Chrysene

980

330

1,667

0

59.1

50

130

Dibenz(a,h)anthracene

880

330

1,667

0

53.0

50

130

Fluoranthene

950

330

1,667

0

57.2

50

130

Fluorene

980

330

1,667

0

58.9

50

130

Indeno(1,2,3-cd)pyrene

940

330

1,667

0

56.2

50

130

Naphthalene

880

330

1,667

0

52.7

50

130

Phenanthrene
Pyrene

990
960

330
330

1,667
1,667

0
0

59.2
57.6

50
50

Qual

130

Anthracene

RPDLimit

130

Acenaphthylene

%RPD

130

1,000

RPD Ref Val

130
130

Acenaphthene

S

Surr: 2,4,6-Tribromophenol

750

1,667

45.0

50

130

S

Surr: 2-Fluorobiphenyl

810

1,667

48.4

50

130

S

Surr: 2-Fluorophenol

840

1,667

50.2

50

130

Surr: Nitrobenzene-d5

850

1,667

51.3

50

130

Surr: Phenol-d5

840

1,667

50.4

50

130

Surr: Terphenyl-d14

880

1,667

52.8

50

130

Sample ID: MB-2825

SampType: MBLK

TestCode: SW_8270S

Prep Date:

5/1/2006

RunNo: 5994

Batch ID: 2825

TestNo: SW8270C

Analysis Date:

5/2/2006

SeqNo: 88967

Client ID:

PBS

Analyte

Result

PQL

2-Methylnaphthalene

ND
ND
ND

%REC

LowLimit

HighLimit

RPD Ref Val

%RPD

RPDLimit

Qual

330

Acenaphthylene

SPK Ref Val

330

Acenaphthene

SPK value

Units: µg/Kg

330

Qualifiers:

E
ND
S

Value above quantitation range

H

Holding times for preparation or analysis exceeded

M

Manual Integration used to determine area response

Not Detected at the Reporting Limit

R

RPD outside accepted recovery limits

RL

Reporting Detection Limit

Spike Recovery outside accepted recovery limits

Page 65 of 66

PM Environmental, Inc.
0604884
7876 Van Dyke - 22-692A

CLIENT:
Work Order:
Project:

Sample ID: MB-2825
Client ID:

QC SUMMARY REPORT
TestCode: SW_8270S
TestCode: SW_8270S

Batch ID: 2825

PBS

SampType: MBLK

TestNo: SW8270C

Analyte

Result

PQL

Anthracene

ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND

330

Naphthalene

ND

330

Phenanthrene

ND

330

Pyrene

ND

Qual

330

Indeno(1,2,3-cd)pyrene

RPDLimit

330

Fluorene

%RPD

330

Fluoranthene

RPD Ref Val

330

Dibenz(a,h)anthracene

HighLimit

330

Chrysene

LowLimit

330

Benzo(k)fluoranthene

SeqNo: 88967

330

Benzo(g,h,i)perylene

5/2/2006

330

Benzo(b)fluoranthene

RunNo: 5994

330

Benzo(a)pyrene

%REC

5/1/2006

Analysis Date:
SPK Ref Val

Prep Date:

330

Benz(a)anthracene

SPK value

Units: µg/Kg

330

Surr: 2,4,6-Tribromophenol

1,500

1,667

87.3

50

130

Surr: 2-Fluorobiphenyl
Surr: 2-Fluorophenol

1,800
2,000

1,667
1,667

111
118

50
50

130
130

Surr: Nitrobenzene-d5

1,800

1,667

109

50

130

Surr: Phenol-d5

2,000

1,667

118

50

130

Surr: Terphenyl-d14

2,000

1,667

122

50

130

Qualifiers:

E
ND
S

Value above quantitation range

H

Holding times for preparation or analysis exceeded

M

Manual Integration used to determine area response

Not Detected at the Reporting Limit

R

RPD outside accepted recovery limits

RL

Reporting Detection Limit

Spike Recovery outside accepted recovery limits

Page 66 of 66

Appendix E

Boring Log SB-1
Project No.: 22-692

Boring No.: SB-1

Project Name: 7876 Van Dyke

Date Drilled: 4/27/06

Facility ID#:

Drill Rig: 6610/2.125" MC

Logged By: BH

Sampling Method: Grab

PID (ppm)

No Well Installed

Ground Surface

CONCRETE
(Loose) SAND/GRAVEL (moist)
Brown, fine

(Medium) CLAY (moist)
2

Sample # &
Depth

Boring
Profile

Depth (ft.)
0

Description and Comments

Blow Counts

SAMPLE

SUBSURFACE PROFILE

Brown

0.0
SS-1
0.0
1.0-2.0'

0.0

0.0
4
0.0

(Stiff) CLAY (moist)
Brown

0.0

6
0.0

0.0
8
0.0

0.0
10

(Stiff) CLAY (moist)
Brown/Grey

0.0

0.0
12
0.0

0.0
14
0.0

16

Completion Notes: EOB @ 15.0'. Hole filled with soil cuttings/Bentonite.
1. The indicated stratification lines are approximate in situ.
The transitions between materials may be gradual.
2. Boring backfilled with natural soils unless otherwise noted.

Sheet: 1 of 1

Boring Log SB-2
Project No.: 22-692

Boring No.: SB-2

Project Name: 7876 Van Dyke

Date Drilled: 4/27/06

Facility ID#:

Drill Rig: 6610/2.125" MC

Logged By: BH

Sampling Method: Grab

PID (ppm)

Sample # &
Depth

Boring
Profile

Depth (ft.)
0

Description and Comments

Blow Counts

SAMPLE

SUBSURFACE PROFILE

No Well Installed

Ground Surface

CONCRETE
(Loose) SAND (moist)

0.0

Brown, fine
0.0
2

(Med Dense) SAND (moist)
Black/Grey, fine, with medium Clay

SS-1
0.0
2.0-3.0'

0.0
4

(Med/Stiff) CLAY (moist)
Brown/Grey

0.0

0.0
6
0.0

0.0
8
0.0

0.0
10

(Stiff) CLAY (moist)
Brown

0.0

0.0
12
0.0

(Stiff) CLAY (moist)
Grey

0.0

14
0.0

16

Completion Notes: EOB @ 15.0'. Hole filled with soil cuttings/Bentonite.
1. The indicated stratification lines are approximate in situ.
The transitions between materials may be gradual.
2. Boring backfilled with natural soils unless otherwise noted.

Sheet: 1 of 1

Boring Log SB-3
Project No.: 22-692

Boring No.: SB-3

Project Name: 7876 Van Dyke

Date Drilled: 4/27/06

Facility ID#:

Drill Rig: 6610/2.125" MC

Logged By: BH

Sampling Method: Grab

PID (ppm)

Sample # &
Depth

Boring
Profile

Depth (ft.)
0

Description and Comments

Blow Counts

SAMPLE

SUBSURFACE PROFILE

No Well Installed

Ground Surface

CONCRETE
(Loose) SAND (moist)

0.0

Brown, fine
0.0
2

(Med Dense) SAND (moist)
Black/Grey, fine

SS-1
0.0
2.0-3.0'

0.0
4
0.0

(Med/Stiff) CLAY (moist)
Brown

0.0

6
0.0

0.0
8
0.0

0.0
10

(Stiff) CLAY (moist)
Brown

0.0

0.0
12
0.0

0.0
14
0.0

16

Completion Notes: EOB @ 15.0'. Hole filled with soil cuttings/Bentonite.
1. The indicated stratification lines are approximate in situ.
The transitions between materials may be gradual.
2. Boring backfilled with natural soils unless otherwise noted.

Sheet: 1 of 1

Boring Log SB-4
Project No.: 22-692

Boring No.: SB-4

Project Name: 7876 Van Dyke

Date Drilled: 4/27/06

Facility ID#:

Drill Rig: 6610/2.125" MC

Logged By: BH

Sampling Method: Grab

PID (ppm)

Sample # &
Depth

Boring
Profile

Depth (ft.)
0

Description and Comments

Blow Counts

SAMPLE

SUBSURFACE PROFILE

No Well Installed

Ground Surface

CONCRETE
(Loose) SAND (moist)

0.0

Brown, fine
0.0
2

(Med Dense) SAND (moist)
Black/Grey, fine, with medium Clay

SS-1
0.0
2.0-3.0'

0.0
4

(Med/Stiff) CLAY (moist)
Brown/Grey

0.0

0.0
6
0.0

0.0
8
0.0

0.0
10

(Stiff) CLAY (moist)
Brown

0.0

0.0
12
0.0

(Stiff) CLAY (moist)
Grey

0.0

14
0.0

16

Completion Notes: EOB @ 15.0'. Hole filled with soil cuttings/Bentonite.
1. The indicated stratification lines are approximate in situ.
The transitions between materials may be gradual.
2. Boring backfilled with natural soils unless otherwise noted.

Sheet: 1 of 1

Boring Log SB-5
Project No.: 22-692

Boring No.: SB-5

Project Name: 7876 Van Dyke

Date Drilled: 4/27/06

Facility ID#:

Drill Rig: 6610/2.125" MC

Logged By: BH

Sampling Method: Grab

PID (ppm)

Sample # &
Depth

Boring
Profile

Depth (ft.)
0

Description and Comments

Blow Counts

SAMPLE

SUBSURFACE PROFILE

No Well Installed

Ground Surface

CONCRETE
(Med) CLAY (moist)
Brown, with trace fine Sand

0.0
SS-1
0.0
1.0-2.0'

2

0.0

0.0
4
0.0

(Stiff) CLAY (moist)
Brown

0.0

6
0.0

0.0
8
0.0

0.0
10

(Stiff) CLAY (moist)
Brown/Grey

0.0

0.0
12
0.0

0.0
14
0.0

16

Completion Notes: EOB @ 15.0'. Hole filled with soil cuttings/Bentonite.
1. The indicated stratification lines are approximate in situ.
The transitions between materials may be gradual.
2. Boring backfilled with natural soils unless otherwise noted.

Sheet: 1 of 1

Boring Log SB-6
Project No.: 22-692

Boring No.: SB-6

Project Name: 7876 Van Dyke

Date Drilled: 4/27/06

Facility ID#:

Drill Rig: 6610/2.125" MC

Logged By: BH

Sampling Method: Grab

PID (ppm)

No Well Installed

Ground Surface

CONCRETE
(Loose) SAND (moist)
Brown, fine, with trace Gravel

(Med Dense) SAND (moist)
2

Sample # &
Depth

Boring
Profile

Depth (ft.)
0

Description and Comments

Blow Counts

SAMPLE

SUBSURFACE PROFILE

Grey/Black, fine

0.0
SS-1
0.0
1.0-2.0'

0.0

(Med/Stiff) CLAY (moist)
Brown/Grey

0.0

4
0.0

0.0
6
0.0

0.0
8
0.0

0.0
10

(Stiff) CLAY (moist)
Grey

0.0

0.0
12
0.0

0.0
14
0.0

16

Completion Notes: EOB @ 15.0'. Hole filled with soil cuttings/Bentonite.
1. The indicated stratification lines are approximate in situ.
The transitions between materials may be gradual.
2. Boring backfilled with natural soils unless otherwise noted.

Sheet: 1 of 1

Boring Log SB-7
Project No.: 22-692

Boring No.: SB-7

Project Name: 7876 Van Dyke

Date Drilled: 4/27/06

Facility ID#:

Drill Rig: 6610/2.125" MC

Logged By: BH

Sampling Method: Grab

PID (ppm)

Sample # &
Depth

Boring
Profile

Depth (ft.)
0

Description and Comments

Blow Counts

SAMPLE

SUBSURFACE PROFILE

No Well Installed

Ground Surface

CONCRETE
(Loose) SAND (moist)

0.0

Brown, fine, with Gravel
0.0
2

(Med Dense) SAND (moist)
Grey/Black, fine

SS-1
0.0
2.0-3.0'

0.0
4
0.0

(Med/Stiff) CLAY (moist)
Brown/Grey

0.0

6
0.0

0.0
8
0.0

0.0
10

(Stiff) CLAY (moist)
Grey/Brown

0.0

0.0
12
0.0

0.0
14
0.0

16

Completion Notes: EOB @ 15.0'. Hole filled with soil cuttings/Bentonite.
1. The indicated stratification lines are approximate in situ.
The transitions between materials may be gradual.
2. Boring backfilled with natural soils unless otherwise noted.

Sheet: 1 of 1

Boring Log SB-8
Project No.: 22-692

Boring No.: SB-8

Project Name: 7876 Van Dyke

Date Drilled: 4/27/06

Facility ID#:

Drill Rig: 6610/2.125" MC

Logged By: BH

Sampling Method: Grab

PID (ppm)

No Well Installed

Ground Surface

CONCRETE
(Loose) SAND (moist)
Brown, fine

(Med Dense) SAND (moist)
2

Sample # &
Depth

Boring
Profile

Depth (ft.)
0

Description and Comments

Blow Counts

SAMPLE

SUBSURFACE PROFILE

Grey/Black, fine

0.0
SS-1
0.0
1.0-2.0'

0.0

(Med) CLAY (moist)
Brown

0.0

4
0.0

0.0
6

(Med/Stiff) CLAY (moist)
Brown

0.0

0.0
8
0.0

0.0
10

(Stiff) CLAY (moist)
Brown/Grey

0.0

0.0
12
0.0

0.0
14
0.0

16

Completion Notes: EOB @ 15.0'. Hole filled with soil cuttings/Bentonite.
1. The indicated stratification lines are approximate in situ.
The transitions between materials may be gradual.
2. Boring backfilled with natural soils unless otherwise noted.

Sheet: 1 of 1

Boring Log SB-9
Project No.: 22-692

Boring No.: SB-9

Project Name: 7876 Van Dyke

Date Drilled: 4/27/06

Facility ID#:

Drill Rig: 6610/2.125" MC

Logged By: BH

Sampling Method: Grab

PID (ppm)

Sample # &
Depth

Boring
Profile

Depth (ft.)
0

Description and Comments

Blow Counts

SAMPLE

SUBSURFACE PROFILE

No Well Installed

Ground Surface

CONCRETE
(Loose) SAND (moist)

0.0

Brown, medium
0.0
2
0.0

0.0
4
0.0

(Med Dense) SAND (moist)
Grey/Black, fine
6

SS-1
0.0
5.0-6.0'

0.0

0.0
8

(Med) CLAY (moist)
Brown

0.0

0.0
10
0.0

0.0
12

(Stiff) CLAY (moist)
Brown/Grey

0.0

0.0
14
0.0

16

Completion Notes: EOB @ 15.0'. Hole filled with soil cuttings/Bentonite.
1. The indicated stratification lines are approximate in situ.
The transitions between materials may be gradual.
2. Boring backfilled with natural soils unless otherwise noted.

Sheet: 1 of 1

Boring Log SB-10
Project No.: 22-692

Boring No.: SB-10

Project Name: 7876 Van Dyke

Date Drilled: 4/27/06

Facility ID#:

Drill Rig: 6610/2.125" MC

Logged By: BH

Sampling Method: Grab

PID (ppm)

Sample # &
Depth

Boring
Profile

Depth (ft.)
0

Description and Comments

Blow Counts

SAMPLE

SUBSURFACE PROFILE

No Well Installed

Ground Surface

CONCRETE
(Loose) SAND (moist)

0.0

Brown, fine
0.0

(Med Dense) SAND (moist)
2

Grey/Black, fine
0.0

(Med) CLAY (moist)

0.0

Brown/Grey
4

0.0
SS-1
0.0
5.0-6.0'

6

0.0

0.0
8
0.0

0.0
10

(Stiff) CLAY (moist)
Brown/Grey

0.0

0.0
12
0.0

0.0
14
0.0

16

Completion Notes: EOB @ 15.0'. Hole filled with soil cuttings/Bentonite.
1. The indicated stratification lines are approximate in situ.
The transitions between materials may be gradual.
2. Boring backfilled with natural soils unless otherwise noted.

Sheet: 1 of 1

Appendix F

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