...2. EXPERIMENTAL DETAILS 2.1 MATERIAL SELECTION Aluminium 2618 was used as the base material in this study. Two types of salt, namely K2ZrF6 & KBF4 were used to synthesize the ZrB2 reinforcement in addition to Si3N4 (Silicon Nitride), AlN (Aluminium Nitride).The chemical composition of the base material is shown in Table.1. Table.1. Chemical composition of Al2618 alloy in wt% Element Cu Mg Fe Ni Si Ti Al Wt% 2.30 1.60 1.1 1.0 0.18 0.07 Bal Aluminum 2618 is melted in a graphite crucible and a stirrer is used to stir the melt. When the temperature of the melt reaches 510°C, the dried K2ZrF6 and KBF4, Si3N4 and AlN salt powders with weight ratio x wt%(x=2,4,6,8) were added to the molten aluminum. The stirrer assembly consisted of a graphite turbine stirrer fixed to a steel rod. Approximately 1Kg of alloy was then melted at 820°C in the resistance furnace of stir casting setup. Preheating of Silicon Nitride, Aluminium Nitride, and Zirconium Boride mixture at 800°C was done for one hour to remove moisture and gases from the surface of the particulates. The stirrer was then lowered vertically up to 3 cm from the bottom of the crucible (total height of the melt was 9 cm). The speed of the stirrer was gradually raised to 800 rpm and the preheated Silicon Nitride, Aluminium Nitride, and Zirconium Boride particle was added with a spoon at the rate of 10- 20g/min into the melt. The speed controller maintained a constant speed, as the stirrer speed got reduced by 50-60 rpm due to the...
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...Melting Range Report Name: Date: Lab Section: |Selected Known Compounds | |Name |Structural Formula |Literature Melting Point | |Acetanilide |[pic] |114.3°C | | |C8H9NO | | |Fluorene |[pic] |116.5°C | | |C13H10 | | |Experimental Data | |Sample Composition | |1. |2. |3. |4. |5. |6. |7. | |100% |10% |25% |50% |75% |90% |100% | |...
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...Determinación de la carga de un electrón por electrólisis Químicos: * Solución de sulfato de cobre * Acetona * Ácido sulfúrico * Ácido sulfúrico diluido. Químicos: * Solución de sulfato de cobre * Acetona * Ácido sulfúrico * Ácido sulfúrico diluido. Objetivo: Determinar la carga de un electrón. Equipo: * Cubeta de electrólisis con armadura para conexión * Electrodos de cobre * Transformador * Conectores * Amperímetro * Cronómetro * Balanza electrónica * Probeta de 100 ml. Diagrama: Procedimiento: Se limpiaron los electrodos con lija, se sumergieron en ácido sulfúrico y una vez secos, se midió la masa de cada uno. Se armó el equipo como en el diagrama 1. Se agregaron 200 ml de solución de sulfato de cobre. Se conectó la fuente de energía durante 5 minutos y se midió la corriente cada 15 segundos, intentando mantenerla constante. Se enjuagaron los electrodos, primero con agua destilada y posteriormente con acetona. Se dejó secar por unos minutos y luego se volvió a medir la masa. Se repitió el proceso 2 veces más. Se calculó la corriente promedio que ha fluido por el circuito en los tres casos. Se calculó la carga eléctrica que ha pasado por el circuito, los mol de iones de cobre formados o reducidos, mol de electrones transferidos y por consiguiente la carga de cada electrón. Resultados: Tiempo en segundos (±1 s) | Corriente en A (± 0.05 A) | Masa inicial de Cu en g (±0.001...
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...1) Look up the chemical/health hazards for sulfur!. Main Routes of Exposure: Inhalation. • Inhalation: VERY TOXIC, can cause death. Can cause severe irritation of the nose and throat. At high concentrations: can cause life-threatening accumulation of fluid in the lungs (pulmonary edema). Symptoms may include coughing, shortness of breath, difficult breathing and tightness in the chest. A single exposure to a high concentration can cause a long-lasting condition like asthma. If this occurs, many things like other chemicals or cold temperatures can easily irritate the airways. Symptoms may include shortness of breath, tightness in the chest and wheezing. {Reactive Airways Dysfunction Syndrome (RADS)}. • Skin Contact: CORROSIVE. The gas irritates or burns the skin. Permanent scarring can result. Direct contact with the liquefied gas can chill or freeze the skin (frostbite). Symptoms of mild frostbite include numbness, prickling and itching. Symptoms of more severe frostbite include a burning sensation and stiffness. The skin may become waxy white or yellow. Blistering, tissue death and infection may develop in severe cases. • Eye Contact: CORROSIVE. The gas irritates or burns the eyes. Permanent damage including blindness can result. Direct contact with the liquefied gas can freeze the eye. Permanent eye damage or blindness can result. • Ingestion: Not a relevant route of exposure (gas). • Effects of Long-Term (Chronic) Exposure: May harm the respiratory system. Can irritate...
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...Torres 1 Luis A. Torres Group #11 USC Chemistry 322b Formal Lab Report 6th November 2015 I. II. Enzymatic Resolution of 1-Phenylethanol and Diastereomer Analysis Objective/Abstract Enzymatic transesterification reaction was performed to study the resolution of diastereomers using 1H-NMR analysis. The stereo-selectivity of acylase I, an enzyme, for a 50:50 racemic mixture of 1-phenylethanol was determined. In the first of a two-step reaction, 1-phenylethanol was reacted with vinyl acetate with the help of acylase I to form an ester, unreacted 1-phenylethanol, and vinyl alcohol. The unreacted 1phenylethanol was separated from the ester by column chromatography and confirmed by thin-layer chromatography (TLC). In the second reaction, the unreacted 1-phenylethanol was reacted with (R)-(-)-acetoxyphenylacetic acid to form a diastereomer ester. In the latter reaction, four different 1-phenylethanol samples were used in order to compare 1HNMR data of the resulting diastereomer esters and determine which enantiomer of the 50:50 racemic mixture was preferred by acylase I. Those four samples were: (1) racemic 1-phenylethanol, (2) unreacted 1-phenylethanol, (3) (R)-1-phenylethanol, and (4) (S)-1phenylethanol. After 1H-NMR analysis, it was found that the (S)-1-phenylethanol was preferred by acylase I. III. Introduction and Background Information Scheme 1: Reaction of 1-phenylethanol with vinyl acetate in the presence of the enzyme acylase I to produce 1-phenylethyl...
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...Introductory Chemistry Introduction Instructor: Dr. Tao Tao Course Section: CHEM1405.6013-6014 Meeting Time: TTh 6:00pm-9:10pm Bldg 13-629 Office Hours: TTh 5:30 pm-6:00 pm Contact: tao.tao@lonestar.edu Introductory Chemistry 2 Course Material Requirements • Textbook – Introductory Chemistry, by Nivaldo J. Tro 5th edition • Chapters 1-4, 6-10, 14 • Sections, 5.6-5.10, 12.4-12.8, 13.6-13.8 • Scientific Non-programmable Calculator • Safety Goggles for Lab • Lab Coat/Apron (Optional) Introductory Chemistry 3 Evaluation and Grade • Tests: 45%; 4 tests, best of 3, no make-up unless good excuses (documented, in advance notice) • Open-book Quizzes: 10%; best n-2, no make-up • Laboratory: 25% • Final Exam: 20% • Homework: Encouraged but not mandatory • Problem Set: Provides but not mandatory • Final withdrawal day: Nov. 10th, 2014 Introductory Chemistry 4 Lab Report/Grade Guideline • Pre-lab write-up (30%): Complete before lab starts, will be checked and signed for completeness – – – – Title/Date Aim/Purpose Introduction Procedures • Lab Performance and Quality of data (25%): will be checked and signed when leaving lab – Observations – Collect and record data • Post-lab (40%) – Result (Calculations, Graphs, Interpretations etc), – Discussions/Conclusions – Post-lab questions if any • Overall Report Neatness (5%) • Report due one week after the completion of experiment for full credit; after two weeks, no report will be accepted, and no credit...
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...In the 4th quarter of 9th grade science we continued our study of chemistry with a focus on chemical formulas, chemical reactions, and stoichiometry. Formative assessments included practice questions on how to write proper names and formulas for chemical compounds, balancing equations, converting between chemical units, and titration problems. The lab experiments for the quarter consisted of a freezing point experiment, chemical flame test comparison, the activity series of four metals, production of hydrogen, and the titration of an unknown concentration of acid. Summative assessments for the quarter were an evaluation of the freezing point experiment, written exploration of the flame test experiment, and two unit exams on chemistry topics. In 10th grade students will study science topics related to biology, environmental science, and some...
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...There are many ways to examine the subject of alchemy, including alchemy as a source of symbolism, psychology, and mysticism. It has also been an influence on the world view of various writers, artist, and musicians. The focus of this report is alchemy as a pre-chemistry, which gave a new impulse towards the preparation of medicinal remedies and also was a major influence on today's scientific investigations. Alchemy is an ancient art, practiced in the Middle Ages. The fundamental concept of alchemy stemmed from Aristotle's doctrine that all things tend to reach perfection. Because other metals were thought to be less perfect than gold, it was reasonable to believe that nature created gold out of other metals found deep within the earth and that a skilled artisan could duplicate this process. It was said that once someone was able to change, or transmute a "base" chemical into the perfect metal, gold, they would have achieved eternal life and salvation. In this way, alchemy turned into not only a scientific quest, but a spiritual quest as well. Although the purposes and techniques were often times ritualistic and fanciful, alchemy was in many ways the predecessor of modern science, especially the science of chemistry. The birthplace of alchemy was ancient Egypt, where, in Alexandria, it began to flourish during the Hellenistic period. Also at that time, a school of alchemy was developing in China. The writings of some Greek philosophers may be considered to be among the...
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...Lab Report Chemistry 341L: Preparation of Cyclohexene Introduction: The purpose of this lab was to prepare an alkene, cyclohexene, by the dehydration of an alcohol, cyclohexanol. In this experiment cyclohexanol is dehydrated to prepare cyclohexene, using phosphoric acid as a catalyst. Unsaturation tests are then done to ensure cyclohexene was prepared. Experimental Scheme: The procedure for the Preparation of Cyclohexene lab started with first having to add 10mL of cylcohexanol (clear liquid with strong odor), and 2.5mL of phosphoric acid (clear liquid) to a 50-mL round bottom flask. These liquids were mixed together well; a boiling stone was added to the flask in order to allow for a smoother and gentle boil. Below is the equation for the reaction that took place in this lab. Equation 1: Formation of the product cyclohexene, from the reactant cyclohexanol with the aid of a catalyst phosphoric acid4 Next a distillation apparatus had to be assembled, using a 25-mL round bottom flask as a receiving flask, this flask was then placed into a beaker of ice water refer to figure 1. Figure 1: Distillation apparatus5 Distillation is used in order to dehydrate the cyclohexanol. After the apparatus was assembled we circulated the cooling water in the condenser, while heating the mixture in the flask. The flask was heated until the product started to distill, and collect into the receiving flask in the ice water bath. We continued to heat the mixture...
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...Department of Chemistry College of Sciences University of Central Florida CHM 2046L Chemistry Fundamentals Laboratory (1 Credit) Course Syllabus Graduate Laboratory Instructor: Office: Phone: E-mail: Office Hours: | Instructor: Dr. Cherie YestrebskyOffice: CH 325Phone: 407-823-2135E-mail: cherie.yestrebsky@ucf.edu | University Course Catalog Description Illustration of chemical principles and introduction to the techniques of inorganic and physical chemistry. Course Overview The Chemistry Fundamentals Laboratory course is designed to give students an insight into the processes of experimental chemistry. The course provides a series of authentic, challenging, and relevant questions which students seek to answer through experimentation in a safe environment. Lab techniques like titration, spectroscopy, dilution, and measurement will be incorporated with critical thinking exercises to enhance the learning process and improve comprehension of fundamental concepts. An introduction to writing within the science discipline will be addressed each week. Course Objectives At the end of the semester, students will be able to: * Keep safety the first priority while working in the laboratory * Design a procedure to answer a key question * Model how writing is used in a variety of chemistry genres * Experiment with glassware & equipment in alignment with their intended function * Develop stronger critical thinking skills ...
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...Syllabus |Discipline Prefix: CHM |Course Number: 111 |Course Title: College Chemistry I | | |Course Section: D04B | | |Credit Hours: 4 |Lecture Hours: 3 |Clinical Hours: |Lab Hours: 3 | |Contact Hours: 6 |Studio Hours: N/A |Semester: Fall | |Meeting Days/Time/Location: Fridays/1:30pm-4:20pm/Science Building | Instructor Information Name: Dr. Shahin Maaref Office Location: JD-30 Office Hours: TRF 9:00am-11:00am, TR 4:30pm-5:30pm & by appointment Contact Information: 822-7692 Blackboard site: http://learn.vccs.edu Instructor email address: smaaref@tcc.edu Course Information Course Description Explores the fundamental laws, theories, and mathematical concepts of chemistry. Designed primarily for science and engineering majors. Requires a strong background in mathematics. Part I of II. Prerequisites and/or Co-requisites Prequisites - None Corequisites – None It is recommended to have H.S. chemistry or CHM01 as prerequisites and MTH 03 or MTE 06 level or higher. General Education Core Competencies Supported...
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...S W I S S G E R M A N U N I V E R S I T Y INORGANIC & ORGANIC CHEMISTRY LABORATORY REPORT | Subject | : Inorganic & Organic Chemistry Laboratory | Lecturer | : Hery Sutanto S.Si | Instructor | : Tabligh Permana S.Si., Dian Sukmayanda S.Si | Faculty/Class | : Life Science/LS 2 A | Date of Experiment | : 11 April 2012 | Date of Lab. Report | : 18 April 2012 | Semester | : 2 | Time of Experiment | : 14.00-17.00 | | | | | | | | | | | | | | | | Experiment: | Principle of Spectroscopy | NAME : Melisa Grace (14211043) Nur Ratih K. (14111005) Group : G | | Campus BSD CityBumi Serpong DamaiTangerang 15321 – Indonesia | Tel. +62 21 537 6221 Fax. +62 21 537 6201 sgu.info@sgu.ac.id www.sgu.ac.id | EXPERIMENT 5: Extraction of Caffeine From Tea Leaves 1. Objective: To demonstrate the extraction of Caffeine as natural substance by using organic solvent and distillation technique. 2. The Materials, Equipments and Procedures: A) Materials * K2CrO4(Potassium Chromate) * H2SO4 (Sulphuric Acid) * Aquades B) Equipments * Beaker * Volumetric flask (50 ml and 25 ml) * Glass rod * Spatula * Watch glass * Graduated pipette * Pipette * Scale * UV-Vis spectrophotometer * Cuvette C) Methods 1. Equipment and materials necessary for the experiment were prepared on the working table. 2. Calculation...
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...Experiment 34A: Hypochlorite Oxidation of Methyl Ketones by the Haloform Reaction: Benzoic Acid Objective: To practice the Haloform reaction as synthetic rout to form benzoic acid To understand the mechanis that provide chorine from NaOH To obtain the melting point and FTIR spectrum of benzoic acid Experimental Procedure: The procedure was followed as described in Mayo, pages 405 -406, with the modifications given on Blackboard. Additional modifications to the procedure included the following: * The filtered product was left on the Hirsch funnel for 1 5 min * The amount of Na2SO3 was increased from 15 to35 mg * The amount of Acetophenone was increased from 15 to35 mg * The amount of Na2SO3 was increased from 90 μL, from 60 μL. * The amount of Sodium hypoclorite was increased to 3.2 mg Reaction scheme Data and Results: Physical properties Compound | Formula | MW | Amount | mmol | Mp 0C | Bp 0C | d | nD | Acetophenone | C₆H₅COCH₃ | 120.16 | 90 μL. | 77 | 20.7 | 2.2.6 | 1.03 | 1.5372 | Aquous NaOCl | NaOCl | 74.442 | 3.2mL | | 18 | 101 | 1.11 | | Sodium sulfite | Na2SO3 | 120.6 | 35mg | | | 33.4 | | | Benzoic acid | C6H5COOH | 122.12 | 94mg | 77 | 121.0 | 249 | | | Chloroform | CHCl3 | 119.38 | 92mg | | | | | | Water | H2O | 18.015 | 1.5mL | | 32 | 100 | 1.00 | | Observations: * Acetophenone and NaOCl were clear liquids * Sodium Sulfite was a whote powder * A yellow greasy liquid was found at the...
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...*If I have to contact the class as a whole it will be through D2L email. Check regularly for notes and announcements.* Credit Hours: 4 Contact Hours: 5 Lab Hours: 2 Prerequisite(s): Math 1710 or equivalent. Required Text(s): 1. Chemistry: The Central Science, 12th edition, Brown, et. al., Prentice Hall, ISBN #978-0-321-78756-9 2. General Chemistry Lab Manual, Cengage Learning ISBN # 9781285127712 3. Register for Sapling Learning homework system ($29.99) See bottom of last page of syllabus for more information!!! Required Supplies/Material(s): Chemical Splash Proof Safety Goggles Recommended Supplementary Material(s): 1. Study Guide and Solutions Manual for Chemistry: The Central Science, 12th edition, Brown, et. al., 2. Scientific calculator Disabilities: A student with a disability who requires academic accommodations MUST contact Sonja Hood, director of disability services, to request an academic accommodation plan. Contact information: Simon Hall 129, (931) 393-1765, shood@mscc.edu Evaluation Plan (subject to revision): |Task |Weight | |Exam 1 (Chapters 10-12) |10% | |Exam 2 (Chapters 13-16) |10% | |Exam 3 (Chapters 17,19-21)...
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...CH 220C ORGANIC CHEMISTRY LABORATORY Spring, 2015 Section Page 1. General Information 2 2. Safety Information 2 3. Attendance 3 Make-Up Policy 3 4. Laboratory Protocol 3 Assigned Reading 3 Pre-Lab Quizzes 3 Lab Notebook 5 Chemicals 5 Due Dates for Reports 5 5. Orientation 5 In-Lab Information 5 Library Information 5 6. Check-In 6 7. Grading Procedure 6 8. Policy on Cheating 7 9. TA Office Hours 8 10. Faculty Course CoordinatorS 8 11. Course Web Page 8 12. Hints to Minimize Frustration IN ORGANIC CHEMISTRY 8 13. Work Schedule 10 Lab Report Due Date Schedule 10 Experiments 10 14. Supplements 17 A. Extraction of Unknown 17 B. Recrystallization of Unknown Products 18 C. Methyl Benzoate 19 D. Synthesis of Luminol 20 E. Azo Violet 23 1. GENERAL INFORMATION PRE- and CO-REQUISITES Pre- and co-requisites for CH 220C listed in the Course Schedule. Important: Because the lecture and laboratory courses are co-requisites of each other, dropping one of them requires that you drop the other as well, unless the drop occurs during ...
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