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Process Scale Up

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Submitted By Buddhs
Words 317
Pages 2
Product Name : DCBA
Stage code : ABCD

There are two reactions involved in the process. The first reaction is reaction between dhercdacetic and bromo amine. The reaction takes place at room temperature. To monitor the unreacted dhercdacetic and the product conversion there are few challenges because of which in process checks are not in place. After completion of the reaction, the bromoamine solution is distilled out and chased with water distillation to get the dhercdbromo in water. Here the active content of the dhercdbromo shall be checked which is only for information purpose. Even if lower content of dhercdbromo obtained also there is no corrective actions for the same to increase the active content.
Further more challenges are there in the process in the second reaction i.e BOC protection, where in unreacted dhercdbromo may not be possible to monitor. TLC method was tried to identify the same but not successful. Moving forward in the process there is pH adjustment for the BOC protected group. The more acid pH may cleave the BOC group and can go for yield loss in the aqueous layers. To quantify the yield loss or to quantify any of the aqueous layers there are challenges to establish any method. Finally the compound would be checked with TLC in the complete analysis to identify the structure.
Based on the chemistry point of view, both the reactions are straight forward reactions and there may not be any abnormalities in the formation of the product. Since there are no in-process checks to monitor the exact product conversions, it could be difficult to find out the failures after the completion of the batches if any.
Because of the time line pressure in meeting the customer requirement this process needs to be taken in to the plant with the known facts of the process. Future scalability point of view for this process needs to be revisited.

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