...By utalizing various methodologies including solid-liquid extraction, liquid-liquid extraction, recrystallization, IR spectroscopy, and TLC, the components of Excedrin were seperated, purified and analyzed/identified. Of the 4.0058 grams of excedrin powder 77.80% was recovered yielding 3.1167 grams. The amount of acetimanophen recovered was 1.6283 grams and the amount of aspirin recovered was 1.4884 grams. The solid-liquid extraction successfully extracted the acetaminophen and the melting point range was found to be 168.3ºC to 170.3ºC for the recrystallized substance compared to the 168.4ºC to 170.1ºC for a 50-50 mixture of pure and recrystallized acetimanophene. The calculated retention factor for acetaminophen was 0.273 and no secondary dots (which would indicate a mixture) were...
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